i •••-. fte.xtia^f t · ii ii ii ii ii i 5 = 35 6 33 to reference tocjeno()t 5636 contract...

.'t-i'-'v

.'^-'v"

.''-X'

' - J1 '

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xtia^ft

" •

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,••

002123

smartin

Poor Quality

5635 6%/W W %J W

LABORATORY RESPONSE TO RESULTS OF CCS (Continued)

SampleFC894 FC898 *FC899FD002 JFD004FBOll^

Fraction/VGA ^

4 BNA /PESTJ

'

FD003

FC898

FDOli

:

VGA

BNA

PEST

CriterionH

C

H

J

——— «

_ j - - . . -

CommentsThe concentration level of each of these six soil sampleswas indicated as medium level on its Organics Traffic Report.However, the results of GC/FID screening indicated that thesesamples needed to be extracted at the low level for the BNAand pesticide analyses. We also decided to run the VGAanalysis of these samples at the low level. The sampleconcentration level to be used for analysis must be deter-mined in the laboratory, and cannot be based on the fieldrecommendation.

As discussed in item 5 of the case narrative, Mr. WilliamLangley granted us interim permission for this case to usea medium level soil blank which was slightly contaminatedwith 2-butanone from the methanol used, The telephone recordlog from Mr. Langley is attached to this laboratory response.

More legible copies of pages 3-0091 and 3-0092 are attached.

This continuing calibration percentage difference problemwas fully addressed in item 1 of the case narrative.

1 .

2.

3.

002124

CON fRACT COMPLIANCE SCREFNtNG SUMMARY FOR ORGANtCS

CASE SAMPLES: DATE: LOG NO.LAB NAME: RECION/S(TC: PREPARED BY;

SampleMo.

feSft*fVSflsFC.TOrcmF&e**F£>®5F&»<ff«votoFOoll

VGA

AHold-ing

Time

B

Tun-Wfc

C

&EanS<

WC_

CaiibraeioaIni-tial

ECon-tinu-ing

'.

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i ; j

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5

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X

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Time

G C

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CdlibratiwO

Jm-tiat

——— ——— _ ——i fi

T~ I ——————— i ——— ' ——— lj; i

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.,_!— _ .-ji —*•e?f 1-

i— 1

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] Vj ehCoracmertts: Probtem Owle (Critefion Specifick £X -as -su -

NC -

KcsubmttSub«nuNoiK~omplianC

Criterion Code: A - Kt A - H, JStKt A f K refof (»sections in Screening

t5ting for cadifraction. ,*«,»(««

CO

002125

I

y JE > V

sr

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002126

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002127

f f [ ft M r. , (. K f t 1 N d f 0 R 0 h t C t/N/t

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MOC/M (

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002128

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oi

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002129

002130

002131

IIIIIII

5636 6 25In Reference to Case No(s):

Contract Laboratory ProgramREGIONAL/LABORATORY COMMUNICATION SYSTEM

Telephone Record LogDate of Call:

Laboratory Name:Lab ContactsRegion;Regional Contact:

Call Initiated By: __*^ Laboratory __ RegionIn reference to data for the following sample number(s):

v>/V.._ L 4&}_//__

Summary of Questions/Issues Discussed;

Summary of Resolution:

^

.o2LSignature

Distribution: (1) Lab Copy, (2) Region Copy, (3) SMO Copy

**<?/#. ~&e-.J)/j&!i\AtL

Date

002132

I

air/

6B'£J£0'9££'988-21I8'£l£0'2£0'2£0

B2

£8'2£0'2

80'@80*0

2161

an 3; £:*;;• 9f! SSD'S2

3D SIZ'£29fl 800'81*sn 000'Si? an 000 *@t> sn 000-0f

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6^6' 0

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an

/•: y AJ y Aa y GS y 8a y aa y AS y 88 UA8 y 88 U88 y

88 y Ktaw

£63'9'G'9'0'I1

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sei 2919£t

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88 y 6I6'0 9A3 y 666'S S

IONiOHIONiONIONION

=82 8831A8 y 666'@ S 83-32 8891

S9 y 828'0 S38 U fSI'I t?aa y £60-i P8A y 680-1 t?

•senanr.us ..")

£16-03WII

annod J.OH 821iCNiON10H691

^8:s98J£#S222.92|

I21

92

99

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CaIS

Zi 6h

002133

iffB 5 253

1545556

m 57

• 53• 59

S3

1616263€4

165666763

1 6979717?

1 737475

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73

1809132

111

w19:3720:8328:3129:532 1 : 8 1,72:4524 : 1324:5326:5329 : 1223: 1323:3823:2133:3931 :5331 :573~:3738:5939:0840:368:59

12:0516:4629:4428:12

6:388:22

10:2115 :6 118:5625:19

RfcTIQ RRT<L) RATIO1 .01 0.895 1,02

8.9420.3613.9?6

1.88 1 .C33 1 . 3 11 . 2 1 9

0.39 I. -3331 .08 1 . 1 6 31 .23 3.878

•6.9510.997

1 .20 0.999: . 8 128.99 1,0821 . 53 0 .9 19

8.9559.9590.9931 . 1 691 . 1 7 31 . 2 1 7

1 .98 1 .0901.98 1.3031 .86 1 . 888!.g9 1 .0831 .08 1.000!.ee 0.?24i.ea 0 .93 11 .00 0.8571 .80 6. 8361 .83 0 .9 1 31.68 8.898

1.331 .081 .03

1 .081 .831 .88

1 .081.881 .00: .381 .381 .C8I. SO1 .991 .331 .881.08

AWT9.99

3.2231.48

1 .969.95

9.480.460.98

40.0849.0048. £940. S340. C074.0373.3 1 .30.3434. 2 179.0642. *2

Artmu58.9850.8059.2030.0858. £8Jf3.S953. £053. S353. ' ,359.0353,^3S'TI i—p**

5"" ,'""i(T - -j.i - J- 1

e-j. ' :5-"•. 3-d.ae50. Q050.3048.2949.3048.29-3.23.^3.002-3 . e0

288. £0103. CO139.63200. 33108. C8

fi.FACa. 096

3.0851.3390.0230.337

0 . 3 1 3Q.??3H.CG3

i .9001 .0901 .8081.0091 .3383.4208.2S5*0.99!8.4129.3238.421

R.FfiCOJ0.3210 . 1 3 13. 1613.067I.-.56' . .3 161 .651.rv=g.'i43.^J79i . ;-44.-31. ;52. *7S

4.3601.7601 .9421 .5641 .6781 ,3381,3831 ,0801 ,3001 ,9031.3001 , 009: . i 330.6958.3811.2003 .05 13.990

RATIO9.02

0.00

9.633.023.92

8 .0 10.010.60

1 .00use1 03t v f **l

1.001.0©3.379.37•a. 308.349.403.43

6

10

002134

IIIIIIII

?35 6 29

LABORATORY RESPONSE TO RESULTS OPCONTRACT COMPLIANCE SCREENING (CCS)

Laboratory Name _ Southwest Research Institute

EPA Contract No. 68-01-7167Case No.

Sample Nos.

5636

FC894FC898FC899FB002IlFD003FD004FDOil

l *Only list sample numbers that require reconciliation.

Response DateOat« ScreeningResults Receivedat Laboratory

_May 5, 1986(VTSR + 38)

_ , 1986(VTSR + 38)

CCS Response should be receivedby EPA on May 6, 1986 (VTSR + 39)

l This form is used to identify materials sent in response to results of Contract ComplianceScreening (CCS). A separate form must accompany the response for each Case. Please indicate (onthe attached continuation form) which, fractions and which criteria correspond with your,resubmission. Response materials sent to CCS should also be copied to the Region and to EMSL/LV,each with the blue identification form.

002135

IIIIIII

LABORATORY RESPONSE TO RESULTS OFCONTRACT COMPLIANCE SCREENING (CCS)

Laboratory Name Southwest Research InstituteEPA Contract No.Case No.

Sample No*.*

68-01-7167

IIIc I

*Oniy list sample numbers that require reconciliation.

Response DateHate ScreeningResults Receivedat Laboratory

" • t , I -' - -,r

oi

- (

I Th,s form u wd to identify materials sent in response to resu.ts of Contract ComplianceScreemng (CCS). A separate form must accompany the response for each Case. Pteajj^indicate (on

tomaterials

each with the blue identification form.CCS

I

002136

IIII

5633 6LABORATORY RESPONSE TO RJ3UI.TS OF CCS (ConlnuU)

Commants

Pag of

iiiiiiiiiiiii

002137

' * f*t .-' t'__._. ";....____.. _^_ -~*

^ r,

__.— _ _• '. _j .

9

IIIIIIIIIIIIIIIIIII

002138

IIIIIIIIIII

5 = 35 6 33to Reference toC*jeNo(*)t

5636Contract Laboratory ProgramREGIONAL/LABORATORY COMMUNICATION SYSTEM

Date of Call iLaboratory Mamei

Telephone Record Lag5/20/S6SWRJ, San Antonio rTx

Herb Sehattenberg MM*

Region!Regional Contact:

VI- HoustonM.L. Ritter

RegionCall initiated Bvi .LaboratoryReturn^ Of earlier caTT by RegionIn reference to data for the iollowing sample numbeKs):

Case data for pesticides analysis; Samples FD003 and FD004

Summary of Questions/Issues Discussed:1. Case data for pesticides has problems; confirming column analysisusing DB~5 capillary GC is not producing good data as seen by thevalues for some compounds. Primary GC analysis also had some $D problems.

°2. Sample FD003 reported B-Bhfi at amount of3, Sample FD004 has posit£ve~hit for two pesticides on Form III ror

QC Summary, but results for thece w*,re negative in the sample analysis.

t Summary of Resolution:^ Pi, Lab is taking stepa _to Jjnproye data and recognizes pesticide analysis

problems..____ _____ ^2. False positive reported by Tab- wiYlT send corrections to Case data.3. Agreed-none found >n sample analysis or FDOO/*., but values were reportedon Form ill to make the "recoveries ilor tns jM^/Msi)~com0 out» LaD willsend corrections and/or explanation of_the data. Region position is that =if valuesare_npt reported in the aample, they cannot be_rgported in thejMS/M3D analyaia portion as positive for that sample^

Signature

Distribution.* '[(i)^Lab Copy, (2) Region Copy, (3) SMO Copy\^

Date /

002139

34

iiiiiiiiiiiiiii

Contract Laboratory ProgramREGIONAL/LABORATORY COMMUNICATION

Telephone R«»rd LogDate of Call* 5/19/^6, . „ SWRI, San Antonio ,TXLaboratory Nam«jLab Contacts David Camann (512)6$4-Region: VI-Hou ton

to Reference to Case NO(«)J5636

SYSTEM -"-F St» ju I-A-,S »"£<>/'.**j ' 4 . - r — * ^ ** *_ A , A **- 'C,v-^^ -,t lfc F!_; f~t*.-e•'?(•' ^UsS?"--"*^*:5c M & 7 T &** 6£ *&-HS u

-5111

ReRional Contacts >^ HITTER (713)954-6771CaU Initiated By: __ Laboratory • _ y_ Region

In reference to data for the following sample numbeKsJiFD003 and FD004.

Summary of Questions/Issues Discussed!1 A* FDOG3 Pesticide data reported on Form I the presence of J-BHC at 1500 ppfc

Raw GG data,p 3-0291 thru 3-0294, does not support B-BHC result and dataon g^3-0293 as confirmatory on DB5 GC run is not accepted.

B. FDG03 MS/MSD Pesticide data does not report B-BHC presence; see p5-0194and also p 5-020? to p 5-0210.

2. Sample FD004 is reported to have Aldrin and Dieldrin in the QC SuinmaryForm III, MS/MSD results, but GG raw data do«is not support th© numbersgiven of 4ppb and 2ppb in the sample , i . e ., looks like a typo error.Summary of Resolutions!• ft 2. Lab will review data and contact Region about results*

/>_ /lf\iL^L l£tt JS, X/ft/JVI Signature Date *

Distributions/(I) Xab Copy, (2) Region Copy, (3) SMO Copy

002140

iiiiiiiiiiiiii

5 5 3 5 6 3SOUTHU£ST BGSGARCH INSTITUTE

3 021Mo: FD003No: 5436

Antlytii Data Sh<s«t3)

Concentration: M*dtutaData Extr«ei*d/Pr*pAr«dJ 03/12/86Dale Anatr**d: 04/01/86Cono/Dil Factor; LOOP«ro«nl Moffftur* OfcwanUd): MA

CAS

P««ticid*/PCBtOPG Cleanup KO

V( i ) = voluac of e x t r a c t i n j ee tadM(S ) = Height of sas sp i e txtr«cted (g)VUJ * Valuae of total « < t r iLt <u l )

319-84-6319-85-7319-86-853-99-976-44-8309-00-21024-57-3059-98-8??-«-«72-20-8332 I3 -6S -972-S4-81 0 3 1 - 0 7 - 350-29-372-43-553-J94-70-557 .74-05001-35-2I2&74-U -21 1 104-28-2UlU-U-553469-2 1 -012672-29-61 1097-69- 1I I096-82-S

Alpha-f iHC8SU-8HC S*0* l t a -8HCG3*ia-8HC Uindane)Heptach l o rAMrinHeptachlor Epondc£ndosulfan IDie ldr i nCftdrinCndosuifan II4 , 4 ' - B 0 DEndosulfarj Su l f a t e4 , 4 * - O i D fHethoxych lo rEndr i n Ke t o n eChlordaneToraohenaAroc l o r - lOUAroeJ0r-122iAr j c l s r - 1232.Aroc l f l r - i242Ar o c l o r - 1248A r o c l o r - 1 254Aro c l o r - 1260

L36. fSU . s/1500 -J

136 , SOUI36 .80U1 36. SOUI 36. SOU136 .30U136 .80U*• - o • o y u^ ' o * o y y273. «OU273. 60U273. 60U273 . 60UUod.oou275 . ^OU

13«8.00U2^3o .OOU13 »8 .00UI j o d .HOUi : c . . -5ouloo. SOUl3 t » .8GU

2736 . OOU2?ja .OQl I

i V(s c r M / s ) 0 . 875 V ( t ) 10000 V ( i ) 5

Fors [

002141

If REPROCESS FILE « t>f ILE ; C s OAi^S

METHOD T ILE5 C iCAP i .

It s.rt t ime: J u .OOoui Values 574O Stop t ime:

Hi oh Value 35.OO

IIIIIii

5A ^ *^ «fe5oi 8 363 U293

Off se tJ oScale factor;

- 18.47

002142

MATRIX SPIES OP MEDIUM LEVEL SOILRB3£ARCH INSTITUTE 5 Ui94

Analyai* Data Sheetiiii

Concentration: MediumDate ExtrseUd/Pr«par«d: 03/14/86Date AmUy«d: 04/01/86Con<3/0ii Factor: 1.00

Moisture (DccanUd): NA

GPC Cleanup

i

i

CASNuaber

319-86-8Sa-8^-976-44-8309-00-21024-57-560-57-172-55-972-20-833213-65-972-54-SlQa l -07-950-29-372-43-553494-70-55 7 - 7 4 - 99001 -35 -21 2 6 7 4 - 1 1 - 2I 1 1 04 -2B -2534<> -5 -2 1 -012672-29-61 1097-69- 11 1096-82-5

Alpha -BHCSeta -SHCOeHa-9H66aoa-BHC (L i n d a n e )HeptachlorAidr inHeptach ior EpoxidsEndosuifan IDie ldr in4 , 4 ' - O D £Endosulfan II4 , 4 ' - D D D£ndosu l fan Su l fa t e4 , 4 ' - D D TMethoxych l o rEndrin Kfitor.eChlordaneToxapheneA r o c l o r - 10 16Aroc l d r - 1221A r o c l o r - 1242Aro c l o r - 1248Aro c l o r - 1254Aro c l o r - I2b0

1 36 .80U136 . 80U2 7 3 .273 , 60U2 7 3 . ^OU273 .60U

I368 .00U2 7 3 . 6 0 U

1368. OOU36. OOU

I 3 6 3 . 0 0 U1 ' & . SOU136 . SOU

2 / 3 6 . OOU273$ . GQU

V( s )

V( i ) -• Voluae of e x t r a c t iftj«ct«d (u l )= Voluas of water e x t r a c t e d (m l )- We igh t of saapie e x t r a c t e d ($}V( t ) - Vot'iae of total e x t r a c t (u l )

M( s ) 0 .87S VU) 10000 V ( i ) 5

002143

^ SOIL mm sriK/iuTin SPUE WPLICAIE KCOTHY £ e <? <* * o aO - «- 0 0 O 0Case Ho: & Ktoy Level: n

friction

VOASHOSAMPLE HO.FBB1I

8/HSHOSAHPLE NO.^D004

Ecoipouitd fM-ftichtaroftthtneTrkftittroftlftiAtChlorofeaflieasToItfMiiMZMtI,2,4-*nchlorobefi/eneActflipMheflft2,4-DinitrotolufinePirrefie

Contractor: Stilt!tfediui Level:

ddedfugAg) Result290 0m o290 0290 130290 0

Contact (to.: 68-01~7i£7

MS 2 gee m260 '0 260270 93 270310 107 300360 79 340300 103 300

3330 0 1940 58 14303330 £90 4190 105 2560

Zftee

93103n1034356

3330 0 1250 38 360 263330 500 1720 127 2S8GN-Niiroso-dH-propylmne 3330 0 1720 M 1260

1 ,4-OicniorcOftftzene 3330 0 1630 49 1270ACIDSKOSAHPLE MO.f&004

PESTSHOSAHPLE HO.FDQtH

* AsteriskedfiPD: VOAS:

8/H:Acid:Pest:

Pentachlorophenol 6670 0 > 160 62 3200Phenol 6670 0 4750 71 35402-Chiorophenol4-Cfcloro~3-i8thylphenol4-HitrophenoiLindansHeptatMorAldrinDieldrinEndrin4 ( 4 ' -ODT

values are outside OC liiits.0 out of tfi-* ;3 out Of 6 ;0 out of 5 ;0 out of 6 ;

6670 0 4380 ' 66 32406470 0 5420' 81 40506670 0 4&30 69 2940

35 035 JL^-r\

110 314 * 9172 296 » 61

35 /~^~ i 70 m ' 52

88 ( 2 J 92 132 7488 ^FtT38 0 >v

outside <JC liiitsoutside OC lintsoutside OC liiitseutside OC liiits /

110 125 3?110 125 85

Secovery: VOAs; S outS/N : 2 outAUd: 0 outPost: 6 out

6$3838485349£1

. 44

260-i?4137

829997

of :oof 12of 103( 12

flPD00300

3 0 *48 *

* 3755 *

* 31252629302945

* 19* 17* 30

2223?6

; outside; cuts ids;stitsidf•outside

OC Liiits*8PO Recovery22 SM7224 62-13721 60-13321 59-13921 oe-14223 38-10719 J1-II747 'R"893o 35- \\t38 41- 1262? 28-10447 17-109

•35 26-9050 25-10233 26-10350 1 1-H4SO 46-12731 35-13043 34-13238 31- 13445 42-i:«50 23-154

OC ::* itsuC li&itsOC liiitsOC lints

file FWS01 on disk 5636 Fora HI

002144

IIIII

i

563S 6In Reference to Case No(s)s

39

5636Contract Laboratory Program

REGIONAL/LABORATORY COMMUNICATION SYSTEM Jb

Date of Call;

Laboratory Name?Lab ContactsRegion:Regional Contacts

Call Initiated By:

Telephone Record LogMay 19 and May 20, 1986

Herb SchattenbergVIDr. Kelvin Ritter

Laboratory _%_._ RegionIn reference to data for the following sample numbeKs)s

FD003, FD004

Summary of Questions/Issues Discussed:!• The reported beta-BHC concentration of 1500 Ug/kg appears to be a false

positive, since^the confirmation run does not support the presence ofbeta-BHC.____ _

2* The aldrin and__dleldrln reported on Form III for FDQQ4 do not appear tobe supported by data (Form I, Form X).

Summary of Resolution:____We agree with Dr« Kitcar's intergretation regarding item lj__Forma I and____X will be reviaed for FD003 to exclude beta-BHC as a positive hit. Form

Ill for FppQ4__wlll be reyiaed to . j>roy id g an explanation of the need toinclude the aldrin and dialdrin results, The revised forma are attached

y^p tr. Jrt. t^L* rr-ir-'fugnature

Distributioni (1) Lab Copy, (2) Region Copy, (3) SMO Copy V dopy

002145

5636 6 401• SOIL KATRIl SPIKE/KATRII SPIKE DUPLICATE RECOVER*

«Ca$e f*o: 5636 Coo tractor: Sxftl Contract HeLow level: JCX . Hedisi Level:

™ Cone. Spilce Saiple Cone. Cone,fraction Coi^eond MdnHug/kg) Result HS I Ric K50 Z ftcc___ „__.. .__ ._ . . . . . _.. . . __ _

VGA

15*0SAKPLE NO.noii1•B j*|SHO

1SAMPLE NO.FS004

•AC 16"SHOSWtfLE NO.

•FD044"

•*EST

SHO^SAHFLE HO.•FD004

Bt Aster isved

RP6: VOAs:

I B/N:Acid :Pest:

IjS-Bic&lorosthsnffTricMoraetheneCMorobenzen*TolueneBenzene

1 ,2,4-Tfich larobenzeneAcenaflhthene2,4-DimtrototuenePvrsneH-Hitroso-di-n-propyUiiM1 ,4-I ich lorobenzeMPentacMorophenolPhenol2-CMoroohertol4-Chlflro-3-«ethylphenol4-NitrophsnolLindaneAldr ioCte iunnEndrin4, 4" -DOT

values are outside 3C litits0 out of 53 out of 60 out of 50 out of 6

290290290290290

33303330333033303330333066706670667066704670

353335888898

•(outside SC; outside QCi outside QC[Outside 0C

000

13000

6900

5000000000004200

hutshutsUnitshuts

260270310360300

19404190123047201720163041604750438054204630

HO727092no

1 10

9093

10779

103

5810538

12752496271668169

31420616910212S123

Recovery;

" 240 "270300340300

14302560360

2460126012703200354032404i>502940

* 91* 61* 52

748?85

VOAs; 0 out8/N : 2 outAcid; 0 outPest; 6 out

9093

19372

103435426&S38384853496144

260174137829f97

Of wof 12of 14of 12

2-QODt,jfeifftel $/3o/

M 68-81-7167

K lints*RP9 SPD Rec»«ry

00360

30 *48 *

* 375 5 *

* 3125262930

-2945

* 19( 17* 30

222326

{outsidej cut side; out side; outside

22 5V17224 6M3721 K-13321 59-11921 66-14223 38-10719 31-13747 3-8934 35-1423B 4H2627 21-10447 17-10935 26-9050 25-10233 26-10350 1 1 - 1 14

SO 46-12731 35-13043 34-13238 31-13445 42-U950 22-U4

X lintsX li.its£ luitsSC luits

;QW£MTS: Coeluting peaks ttere calculated as Aldrin and Duldrin even though Aldrin and Dieldnn uere sat se&fl in to*calusn. The calculated values nere retained in ordar to subtract the «>wo* the inUrferinf waif for cartelcalculation of the MS and MSB compounds.

- t i e FRH3SOI on disk 5636 tol IH

002146

IIIII

6 413-0211

SOUTHWEST RESEARCH INSTITUTESample Mo: PD003Case No: 5633

Grganics Analysis Data Sheet(Fage 3}

iiConcentration; MediumDate Extracted/Prepared: 03/12/86Date Analysed: 04/01/00Conc/Dtl Factor: 1.00Percent Moisture (Decanted): NA

Paaticide/PCBaGPC Cleanup NO

iii

CASNusber319-84-6319-85-73 19-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-5S3494-70-S57-74-98001-35-212674- 1 1 - 211104-28-2U141~U-553469-21 -912672-29-61 1097-69-111096-82-5

Alpba-BHC6eta-8HCDe l t a -8HCGaffisa-BHC (L i ndane )HeptaehlorAldrinHeptaehlor Epox ideEndosulfan IDieldrin4,4 ' -DO£Endrin£ndosulfan H4 ,4 '-ODDEndosulfan Sulfate4 ( 4 ' - D 0 rKethoxychlorEndrin KetoneChlordaneToxapheneAroc l o r - 1016Arocior-1221Aroclor-1232Aro c l o r - 1242Aroc l o r - 1248Aroc l o r - 1254Aroclor-1260

ug/ka136.SOU136,SOU136 .SOU136 .SOU136 .SOU136.SOU136 .SOU136 .SOU273.60U273 .60U273.60U273.60U273 .60U273.60U273.60U

1368.00U273.60U

1368.0GU2736.OOU1368.00U1368.00U136.SOU136 . SOU136 .SOU

2736.OOU2736 .OOU

V( s )

V(i) = Voluse of extract injected (ul)V( * j = Voluse of wa t e r extrac ted (s i)H fS ) = Weight of sample ex t ra c t ed (g)V(t) = Voiuae of total e x t r a c t (ui)

or H ( s ) 0 . 8 7 5 V ( t ) 10000 V ( i ) 5

Form I

002147

IIIII

5635 - oSfiPESTICIDE/PCSNo.:

Contract He.: &6-01-7167 U&oratQry! Svftl

Sa«ie1,9. Coluifi

RT of RT MiRdOKPasticide/ Tentative of Appropriate Cflftfiraation

PCS 1 .6. Standard ColuinRT on

ConfiriatoryColuin

RTStandard

6C/HSCon^irifi(Y or S!

No coipounds detected

iii

i

i

002148

I I I I I I I I I I I I I I

002149

QMftHHTTAL ^TOTECTTOTfcGEOffice of Enforcement CHAIN OF CUSTODY RECORD

First International BkJg,, 1201 Elm St.Dallas, Texas 75270

PROJ. NO. PROJECT NAME

D«e / Time Received by

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cn

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002150

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MONITORINGLABORATORYATTN DATA AUDIT STAFF

JLS*8"011 EXEC"tIVE CENTERVSGAS NV 39109

002154

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002157

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002158

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ENVIRONMENTAL PROTECTION AGENCYOff to« of Entforoerrwnt CHAIN OF CUSTODY RECORD

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002166

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002167

NumbermBEPET

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Date Rectt: jSample ConditionNumber ofContainers

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Sample LocationSurf ace WaterGround WaterL@achate

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002168

. -DPtiyNwt*REPORTSample NuppjserFC8£9

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Number ofContainersWater(Ebctractable)Water(VOA)


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Son/Sediment(Eatractable)Soil/Sediment(VQA)Other

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002169

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002170

T)CaseN


SAMPLE ODNCENTRimON(Check One)

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Number ofContainersWater(Extraetabie)Water(VGA)

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DateSample ConditionOft Beeeipt (e.g., broken, no jice, Chain-of-Custody, etc.) i

Soil/Sediinanfc

Name of CarrieirSoti/Sedtoent(VQA)Other

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Airbill Number:D Sample Location

Surf ace WaterGround WaterLaachate

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0334• a ? - 3 / x

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Special Handling Instructions:(a.g,, safety precautions, hazardous nature)

LAB COPY FOR RETURN TO SMO

002171

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Number ofContainersWater(Extra&tahle)Water(VGA)


"F) AnalymsLab;it

Date Hec'ASample ConditionOn Receipt (e.g., broken,ice, Chain-of-Cufltody, etc.)

iSK i i s i Inf oimation Scdl/Sedtoent(BbctractaMe)

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Date Shipped:

Airbill Number:on

Surf ace WaterGround WaterI-eachate

__ Mixed MediaJ^^! Solids__ Other (specify)

(e.g., safety precautions, hazardous nature)

LAB COPY FOR ROT8N TO SMO

002172

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(Namef

(FhorseJSampling Date:(Begin) (End)

S) SAMPLE CONCENtHATIOM

Low ConcenfcratiotvMedium Concentration

!|> SAMPLE MATRIX(Check One)

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ShipTo:.- * ^ *&tc :

® For each sample collected specify numberof containers used and mark volume level •-on each bottle.

Number ofContainers(Extractabld)Water(VGA)


4

Reo'd by:DateSampto Conditionon Receipt (e.g., broken, noice, Chain-ofCustody, etc.)

on Soil/Sediment

Name of GamerSoll/Sedliiient(VQA)Other

Date Shipped:

c//Airbill Number:

Sample Location_iX~ Surface Water __ Mixed Media__ Ground Water __ Solids—— L&achate -4^TOther (specify)


LAB CXDPY FOR REIUfRN TO SMO

002173

OHGANICS TRAFHG REPORTSompie Number

7 Case Number:


D SAMHJ: CONCENTRATION(Check One)ConcentrationMedium Concentration


__Water

3) Ship To:

Ship To:' 6 77

Sampling Personnel:For each sample collected specify numberof containers used and mark volume levelon each bottle.

Number ofContainersSampling Date:

Water(Extractable)

(Begin) (End)Water(VGA)


Analysis Lab;

DateSanq ld Condition0X1 Receipt (e.g., broken, n«sice, Chain-of-Cuatody, etc.)

® Shipping Information Soil/Sediment(Sxtractable)

Name of CarrierSoll/Sedtaenb(VOA)Other

Date Shipped:

Airbill Number:Sample Description_^ Surface Water

Ground Water

onMixed Media


LAB COPV FOR RETTUBN TO SMO

002174

iO

Hu-

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002175

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„. XSample Number SOUTHWEST RESEARCH INSTITUTE

Analysis Data Sheett uLaboratory Name: SwRtLab Sample No: T fC,Sample Matrix: SoilData Release Authorized By:

Case No:QC Report N<Contract No:Date Sample Received;

CASNuaber74-87-374-83 -97 5 - 0 1 - 475-00-375-09-267-64- i75- 15 -07S-35-475-34-3156-60-567-66-3107-06-278-93-37 1 -55 -656-23-5108-05-475-27 -4

Volatile CompoundsConcentration: Low0ate Extracted/Prepared: 3Date Analysed: 3 //.)*/ $(# fConc/Dil Factor: I pH \J>Percent Moisture (Not Decanted): iQ I.I

ug/kg CASChloroae thaneBroaoaethaneVinyl Ch lor i d eCh loroe thaneMethylene Chlor ideAce ton eCarbon Di su l f i d e1 * l -O i c h i o r o e t h e n e1 , 1 -D i c h l o r o e t h a n eTr a n s - l ,2-D i c h l o r o e t h e n eChloroforf ll »2 -D i c h l o r o e t h a n e2-Sutanorts1 , i , 1 -Tr i c h l o r o e t h a n eCarbon Tetrach lar idev iny l Ac e t a t eBroaod i ch l o romethane

10U10U10U10U-~&tr4£tf

5USU5U5U5U5U

10U5U5U

10U5U

78-87-510061 -0279-0 1 -6124-48- 179-00-571 -43-210061-011 10 -75 -875-25-259 1 -78 -6108- 10- 1127 - 18 -479-34-5108-88-3108-90-71 0 0 - 4 1 - 4100-42-5

1 ,2-Dich l o ropropane6 Tran s - I ,3-Oi c h l o r op r op e n e

Tr i ch loroe theneDibroff loch loromethanel , l ,2~Tr i c h l o roe t haneBenzene

5 Ci s - l ,3-Di ch l o ropropene2-Chloroe thy lv i ny l e therBrof l ioform4-Hethy i -2-Pen tanone2-HexanoneTetrach loroe thene1 , 1 ,2 ,2- r e t r a c h l o r o e t h a n eTolueneChlorobenzeneEthy lbenzeneStyrene

Xyienes

ug/k55555-5.5

10 *5!

I0tlOi

5<5 1.

5!5*5'

„ , .f t, ,. . . Data Reporting QualifiersValues If the rtMit is a value greater than or ewal to the detection lint, report the vskeU Indicates coipound ns analyzed for but not detected. Report the, , - - - - - - — .-.„..«,. ..«;*, . ,JI8

indicate in esti.ated value, fhis fla9 Is'«Sfid r £. MMM oncmm^ Zu^lftfr J*^ th8 Wl*'a 1:1 reswnse is assu.ed or «hen the MSS spectral data indicated the JS .} ~ f hi !/ ^ ^VS1'''^8 Mhere

criter a t the result i, Uss ta specified detection li.it bu a Th r * ° r I i f ! Jr^"*10 ug/I «d a concentration of 3 ug/i is calculated, »-«* « " 9< K If IliU flf detec^on isThis flag applies to pesticide paraiaters nhare the) = 10 ng/ul in the final fiitr.irt chnnM HO confined

spiked coipounds

002176

Sample No:Case Ho:i

SOUTHHBS T R&SZARCH XNS TI TUTE

Orgsnics Analysis Data Sheet(Page 4)

Tentatively Identified CompoundsPrac-Scan Estimated

Concentration

94 «/•

1

I

9I5"

002177

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Oat* Analyst*'0*1

I1

^;-l.H , " i^ _.. . . . . . . _ Cflrttin/^•4 ft

— iUZ_— CA*rBU*AOVFm AJ A'Q***Q819-85-7319-86-818-89 976-44.8309-00-21Q24-S7.3159-98-880-S7-172 55-972-20-8332 13 -85 -972-54-81031-07-850-29-372-43-553494.70-557-74-98001-35 212674- 1 1 .21 1 104-28-21 1 1 4 1 - 1 6 - 563469-21-9U672J9.8tioVr^l^1 1096 82 -5

Aio^i BHC8*ta SHCOtfta-iHCG*mmi|.8HCiL'nd»n«iH«o«CftierAtdnnM«et« iOf Eooaid*End<rtuH*rt lU'«tdnr\4 4 -ODEgndnn£rtdo*uH»n il4. 4 -000E*dO*ulf«rt $uH*te4 4 -DOTM»thO«VCf^lC'£hd"rt KiioftdChiopdanafOKCDH«n«Afocio^-1016Afeeio'-I22iAroclor-1232Aroeior-1242Aroe)6f-1248Ar$c lor-1254Afccio^ 1260

u$u* Liquid • Liquid £jrtf*ct7S» QYes

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002180

« i « uSample Number SOUTHUEST RESEARCH INSTITU

Laboratory Name: SwRILab Sample No: TSample Matrix SoilData Selea** Author By:

Analysis Data Sheet

QC 3 C 1

GASNumber74-67-374-83-975 -0 1 -475-00-375-09-267-64- i75- 15-075-35-475-34-3156-60-567-66-3107 -06 -278-93-37 1 - S5 -656-23-5108-05-47 5 - 2 7 - 4

Volatile CompoundsConcentration: Low -Date Extracted/Prepared: /AV Date Analyzed; J //£/ *?& /Conc/Dil Factor:^" PH Percent Moisture (Not Decanted); PS ) \7\J, L, /\

Chiorof te thaneViny l Chlor ideChloroe thaneHethy lene Ch l o r i d eAcetoneCarbon Di su l f i d e1 , 1 -D i c h l o r o e t h e n e1 . 1 -D i c h l o r o e t h a n er r a n s - l ,2-0 i c h l o r o e t h e n eCh l o r o f o rm1 .2 -O i c h l o r o e t h a n e2-Sutanone1 , 1 , 1 - r r i c h l o r o e t h an eCarbon Tet ra ch l o r i d eViny l Ac e t a t eBrof iod ich lor one thane

ug/kg10U10U10U10Uo -«rfl&etr5U5U5U5U5U5U

LOU5USU

10U5U

CASNutaber78-87-510061 -0279-01 -6124-48- 179-00-57 1 -43-21 0 0 6 1 - 0 1 -1 1 0 -75 -875-25-259 1 -78-6108- 10 - 11 27 - 18 -479-34-5108-88-3108-90-7100 -4 1 -4100-42-5

1 ,2-D i c h l o r op r opan e-6 Traf t s- l ,3-0ich loropropeneTr ich loroethene

Dibroff loch loro i f te thane1 , 1 ,2 -T r i c h l o r o e t h a n e*

5 C i s - l ,3-D i c h l o r o p r op e n e2-Ch l o r o e t h y I v i n yAe t h e rBrof l i o form4-Hethy i -2-Pen tanone2-Hexanon eTetrach l o roe thene1 , 1 ,2 ,2- f e t r a c h l o r o e t h a n etolueneChlorobenzeneEthy lbenzeneStyrene

Xylenes

ug/k555555;5

10t10(51SI•«515t5(51

Values(I

»k ,. . , Data R^portinsf Qualifiersthe result is a value greater than or equal to the detection liait, report the - -i(Jentlfied Cfllpounds

the identificationhllt of d««twft is1:1 response is assu.ed or «hen the as s r a i d rest III? l"J?criteria M the result is less than specified de Jion H a

S

r10 ug/t and a concenttation of 3 ug/1 is calculated, report as 3J 9<

This flay applies to pesticide parameters «her3 the identification has been confirmed bv cr/ns <iHfl ) . -)= 10 ng/ul in the final eitract should be confiraed by GC/HS confined by fiC/HS. Single cosponent pesticidesThis flan is used often the analyte is found in the blank as mil as a saiple it inrfir.fac „«.*! , „ ..and varns the data user to take appropriate action. IBdlMtw Possi6ie prflbable blaftii contaiinationspiked coipcunds

002181

— ' ^ ^ r > <•* 4 ^ *w\tofimftSample No:Case No:

0 oo

ICAS Compound NaraaNumber

Organics Analysis Data Sheet{Page 4}

Tentatively Identified CompoundsEstimatedFrac- Scan ConcentrationUon Number ug/%*****i*****t*****«**t, i|5r4ti4;,(:.

a

aa

002182

i

002183

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Case NoOrganic* Analyeia Data Shwt

3)

Number

Medium (Circle One)Date '*>r*&«red

i 'Oil FsetorMotCtur*

GPCSepiwory Funnel £Ktr»ctiOft 'P Y*sCoritmuout Liquid • Liquid £jrtfic*

CA4 (Circle OA«)Pi9-84.fi

76-44.630&.00-2

ISd-98-860-S7.172S5 -9

72-S4.833213-66-$

1031-07-850-29-372-43-5S3494. 70S57-74-S8001 -3& 212674.H-211 104-2821 1 14 1 - l g .S53469-21-912672-2»*61 1097.69-11 1 0 9 6 8 2 - 5

3MC8et«-6HC

AW? in

4 4 -ODE

4 4 -000

4 4 -DOT

Aroctor-1016

Aroetor-1232Areclor-1242Aroeior-1248

1 254U60

V( * Volume of »rtr«tt m|«cied (ullaxuaeied

> Weight of w^e'e aitrsctcd (gi* Volume & total «Btr«ct (uU

7 8S

002185

o — — J»

SOUTHWES T RESEARCH XNS T £ TU T£Sample Number

II

I

Laboratory Name: SwRII Lab Sample No: S

Sample Matrix; Soil

Organics Analysis Data Sheet(Page 1) *

Case No: QO Report No:Contract No: " O/V» - . i rff ~* /' W

Data Release Authorized By: Date Sample Received:

Volatile CompoundsConcentration: Medium riDate Extracted/Prepared: 3 /I /Date Analyzed: 3^1% (&Conc/Dil Factor: 4- pHPercent Moisture {Not Decanted):

CASNufiber74-87-37 4 - 8 3 - 97 5 - 0 1 - 475 -00-375-09-26 7 - 6 4 - 175 - 1 5 -07 5 - 3 5 - 475-34-31 5 6 - 6 0 - 567-66-31 0 7 - 0 6 - 278-93-37 1 - 5 5 - 65 b - 2 3 - 51 0 8 - 0 5 - 475-27-4

ChloromethaneBrof i ome t han eViny l Ch l o r i d eChlo roe t han eHethylene Chlor ideAce t o n eCarbon D i s u l f i d e1 , 1 -D i c h l o r o e t h e n e1 . 1 -D i ch l o roe t haneT r a n s - l , 2 -D i c h l o r o e t h e n eCh l o r o f o rm1 .2 -D i c h i o r o e t h a n e2-Butanone (S'OOCD1 , 1 , 1 -T r i c h l o r o e t h a n eCarbon Te t ra ch l ondeV i n y l Ac e t a t eBroaodich lorotne thane

us/kg1000UIOOOUIOOOUIOOOU

SOOU-t#at?tr500USOOUSOOUSOOUSOOU5QOUteefltr-500USOOU

IOOOUSOOU

CASNumber78-87-51006 1 -0279 -0 1 -61 24 -48 - 179-00-57 1 - 4 3 - 210061 -0 11 1 0 - 7 5 - 875-25-25 9 1 - 7 8 - 61 0 8 - 1 0 - 11 2 7 - 1 8 - 479-34-5108-88-31 0 8 - 9 0 - 71 0 0 - 4 1 - 4100-42-5

1 ,2-Dichloropropane•6 T r a n s - 1 ,3 -0 i c h l o r o p r o p e n e

Tr i c h l o ro e t h en eDibroaoch l o ro f l e t hane1 , 1 ,2-Tr i ch IoroYthaneBenzene

•5 Cis~ i ,3-D i c h l o r o p r op e n e2-Ch l o r o e t h y l v i n y l e t h e rBronofors4-Me i . lw l -2-Pen t a n o n e2-Hexano n eTet r a c h l o r o e t h e n e1 , 1 , 2 ,2 -T e t r a c h l o r o e t h a n eToluene o?3OOCh l o r o b e n z e n eE t h y l b e n z e n eStyrene

Xyl en e s'}

50015001500150015001500L5001

100015001

100011000L

500L5001500L

Data Reporting1 QualifiersValues If the result is a value greater than or equal to the detection liait, report the value.U indicates coipound tias analyzed for but not detected. Report the siniiua detection Uiit For the saiple mth the U

(e.g. 16U) based on necessary concentration dilution action (This is not necessarily the instrutent detection liiit). Thefootnote should bs read U coipound Has analyzed for but not detected. The rtmber is the fliniiui attainable liiit for the staple.

J Indicates an estiiated value, this flag is used either when estiiated a concentration for tentatively identified coipoimds Kherea 1:1 response is assuied or when the aass spectral data indicated the presence of a compound that neets the identificationcriteria but the result is less than specified detection liiit but greater than zero (e .g . 10J) . If liait of detection is10 ug/I and a concentration of 3 ug/1 is calculated, report as 3J.

C This flag applies to pesticide paraieters where the identification has been confiraed by 6C/HS. Single coaponent pesticides) : 10 rtg/ul in the final extract should be confined by GG/HS.8 This flag is used when the anaiyte is found in the blank as (tell as a saftple. It indicates possible probable blank conUunatiart

and warns the data user to take appropriate action.S spiked coipounds

002186

II[Sample No:Case No:

|CAS Compound NameNumber

r RESEARCH INSnrure

Organics Analysis Data Sheet(Page 4)

Tentatively Identified CompoundsEstimated

Frae- Scan Concentrationtion Number ug/|£<|

fc*********m****««*****«|lt***«

.- -c

3k-

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ret

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002187

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002188

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002189

Cas* No

Lowg Datt

Date• Cone'Oil

Or$anica Analysis Data(Page 3)

Numbor

3!4

GPC Cleanup QY*$S«e«r»terv f unn«i €Contmuou* Liquid • bquid^P

CA*Numb»f319-M-6

1985 -7319-86-ft

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1024-57-3

W-57-172-55-9'2-20-6

72-S4-81031-07-850-29-372-43-SS3494.70557-74-99001-3$ 212 *74. 1 1 -21 1 104-28-21 1U 1 - 18 -&63469-21-d12672 -29-*1 1 9 7 - 6 9 - 11 1096-82-1

8HC

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4 4 -ODE

4. 4 -ODDSu'Ute

4 4 -DOT

Afoc i o r - 1232

AroclOf-1246ArdClOf-1254

(ul)V. « Vo!um«o4 water extractedW§ «Weight ef

um«640,^5

«xtract«d (fl)V. tt Vo!um« «4 total extract

5"

7 85

002190

- ^ a * < £0 v 0 ^_Q

Sample NumberSOUTHW&Sr RBSKARCH INSriru

Organice Analysis Data SheetLaboratory Name; SwRI /Lab Sample No: T F DC°TSample Matrix: SoilData Helease Authorized By:

Case NQC Report No:Contract No:Date Sample Received: J/g

„. / n- / '

I

CASNumber74-87-374-83-975-01 -475-00-375-09-26 7 - 6 4 - 175- 15-075 -35 -475 -34 -3156-60-567-66-3107-06-278-93-371 -55 -656-23-5108-05-47 5 - 2 7 - 4

Volatile CompoundsConcentration: LowDate Extracted/Prepared:Date Analyzed: 3/l1/$(oConc/Dil Factor: gf pH ,Percent Moisture (Not Decanted);)^/, D , L , V >

Chloroae thanefiroflofltethaneViny l Ch lor i deChlo ro e t h an eMethy lene Ch l o r i d eAce ton eCarbon Di su l f i d e1 , 1 -D i c h l o r o e t h e n e1 . 1 -D i c h l o r o e t h a n eTra n s - l ,2 -D i c h l o r o e t h e n eCh lo r o f o r a1 .2-D i c h l o r o e t h a n e2-Butanone1 , 1 , 1 -Tr i c h l o r o e t h a n eCarbon Tetrach lor ideVinyl Ace t a t eSronod i c h l o r oa e t h an e

10UIOUIOUIOU

5U//D 4-etr5USU5USU5U5U

iOU5USU

IOU5U

CASNuaber78-87-5 1 ,2-Dich i o ropropane10061-02-6 Tran s - i ,3-0i ch l o rop ropen e79-0 1 -6 Tr ich loroethene1 24 -48 - 1 Dibro taoch i or ome thane79-00-5 1 , 1 ,2-Tr i c h l o r o e t h a n e71 -43 -2 Benz en e10061 -0 1 -5 Ci s - l ,3-D i c h I o r op rop e n e1 10 -75 -8 2-Chloroe thy lv i f i y l e the r75-25-2 Broff lofora59 1 -78-6 4-Methy l -2-PenUnon e108- 10 - 1 2-HeKanone127- 18 -4 Tstrach loroe thene79-34-5 1 , 1 ,2 ,2-Te t r a c h l o r o e t h a n e108-88-3 Toluene108-90-7 Chiorobenzene100-4 1 -4 Ethy lbenzane100-42-5 Sty r e n e <

Xylenes

C•*<55C

555

105

1010

55

--55

Data Reporting QualifiersValues If the result is * value greater than or equal to the detection liait, report the value.U Indicates COIPOUM) was analyzed for but not detected. Report the lirtiiuj detection halt for the saiple with the U

(e.g. IOU) based on necessary concentration dilution action (This is not necessarily the instruaent detection lint). Hiefootnote should be read U coipound Has analyzed for but not detected. Hie nuiber is the etnuu* attainable liiit for theJ Indicates an estiiated value. This flag is used either when estisated a concentration for tentatively identified coipounds wherea hi response is assuied or vim the sass spectral data indicated the presence of a compound that fleets the identificationcriteria but the result is less than specified detection liBit but greater than zero (e.g. 1(U). If liiit of detection is10 ug/l and a concentration of 3 ug/1 is calculated! report as 3J,C This fU$ applies to pesticide paraieters nhere the identification has been confined by GC/HS. Single coiponent pesticides} ^ 10 ng/ul in the final 01trac t should be conftraed by GC/HS.B This flag is used when the analyte is found in the blank as nsll as a saiple. It indicates possible probable blank contaminationand Hams the data user to take appropriate action.$ spiked coipounds

002191

i •1 '-'27

Sample No:No:

SOUTHHES T RESEARCH INS TI 1'UTE

30 4I Organics Analysis Data Sheet

(Page 4}Tentatively Identified Compounds

EstimatedAS Compound Name Frac. Scan ConcentrationNumber tion Number ug/kjft* * * * * * * * * * * * * * * * * * * * * * * * * *t** * * * *«*** * * * * * * *t** * * * * * * * * * *t** * * * * *^) (^^fS-Pu^>v^w- ^'^ ^ fc ^ f5oc3o

M53 PC6J

i

"1

002192

I

I

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/yf

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I

GAd

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M-751ai-i-oi i i .f i-i1 20-83-120-U-1 1 2

. .

002193

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002194

II3 130.

Labor story NameCas* No

Analysis{Page 3)

$ampt« Number

IIDtt*

yaw Mtdium (Circla Or*|'^*t»ared ——?M~Lrf,———————

Cane'OiP«fC*f«t

GPCS*par«lorv Punrt«lConimuou* Liquid • Liquid

(daeamtdt

I

CA$319-84-6519-8S-7319-86-858-4 *976.44.9309-00-21024.SY.355998 A80-57-172 5S-S72-20-8332 ^3 -65972-M-81 031 -07-850-29-372-43-S53494-70557-74-96001*35 112674- 1 1 . 21 1 104-28 21 1 1 4 ^ . 1 8 - 5$3469-21 -912672-29-61 1097-69. t1 1096 82-5

Aiona-SHC8#ia-BHC0«(ta-8HCG*f«fTi»'8HC (Lmd«n*iM«0t*eniarAtdfinH4CJt*ChlO/ eoo«i<3«£r^o«ui(an iDi«ldfm4 4 -OOE£ndnn6ndOiuK«n n4 4 -000gndoxjlfi* SuHate4 4 -DOTMcthoiveft'tirgndrm Katon«Chtordan«ToK4oh«*«Arc£lor-10l6AfdC(0'-122iAroc lo r- 1232Aroelor-1242AroctOr-U48Aroclor-12544r&ClO' 1260

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002195

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Ii Organic^ Analysis Data SheetLaboratory Name: SwRI Case No: "Lab Sample No: F Ot£ i (6 (JC Report No:Sample Matrix: Water Contract No: C.-£ ct*Data Release Authorized By: Date Sample Received:

c-l

Volatile CompoundsConcentration: LowDate Extracted/Prepared: 3/uDate Analyzed: "3/n /6c-Cone/Da Factor: I pHPercent Moisture (Not Decanted):

Ch l o r om e t h a n eBrowo r a e t h a n eViny l Ch lor i d eCh l o r o e t h a n eHethy l ene Chlor ideAce t o n eCarbon Disu l f ide1 , 1 -D i c h i o r o e t h e n e1 . 1 -D i c h l o c o e t h an er r a n s - l ,2-D i c h l o r o e t h e r i eCh l o r o f o r m1 .2 -D i c h l o r o e t h a n e2-Bytanone1 , 1 , 1 -Tr i c h l o ro e t haneCarbon Te t r a c h l o r i d eVinyl AcetateSro sod i c h l o r oa e t han e

IftB

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1805U5U5U5U5U5U

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CASNumber7 8 - 8 7 - 51 0 0 6 1 - 0 279-0 1 -61 2 4 - 4 8 - 179-00-57 1 - 4 3 - 210061-011 1 0 -75 -875-25-259 i -78- t >108- 10- 11 2 7 - 1 8 - 479-34 -5108-88-5108-90-7100-4 1 -4100-42-5

1 ,2-D i c h l o r o p r o p a n e-6 Tr a n s - 1 ,3-D i c h l o r a p r o p e n e

Tr i c h l o r o e t h e n eDi b r omo c h lor one-thane1 , 1 , 2 ~T r i c h l o r o e t h a n eBen z e n e

5 Cis- l ,3 *Dich loropropene2-Ch l o r o e t h y l v i n y i e t h e rBrofl ioform4-Me t h y l -2 -P e n t a n o n e2-HexanoneTe t r a c h i o r o e t h e n e1 , 1 ,2 ,2 -T e t r a c h l a r o e t h a n eTolueneChlorotenzeneEthylberizeneSty r e n e

Xytenes

5555555

10'5

1010

5555555

j Data Reporting Qualifierslvalues If the result is a value greater than or equal to the detection luit, report the value.U Indicates compound was <malmd for but not detected. Report the liniiua detection inn for the saiple *Hh the UI (e .g . IK)) based on necessary concentration dilution action (This is not necessarily the instrument detection Unit) . Hiej footnote should be read U compound was analyzed for but not detected. The nuiber is the liniiu* attainable litit for the saaple.PJ Indicates an estieated value. This flag is used either when estiaated a concentration for tentatively identified compounds where

a 1:1 response is sssoud or when the «ass spectral data indicated the presence of a compound that ieets the identificationI criter ia but the result is less than specified detection lilit but greater than zero (e.g. 10J) , If liait of detection isI 10 tig/1 and a concentration of 3 ug/1 is calculated, report as 3J.C This flag applies to pesticide paraieters where the identification has been confiraed by 6C/HS. Single coaponent pesticidesB ) = IO ng/ul in the final eitract should be co.ifireed by GC/HS.f This flag is used when the analyte is found in the blank as well as a saaple. It indicates possible probable blank contaminationand warns the data user to take appropriate act ion..3 spiked coipoitnds

002196

I•Sample No:Case Ho: :ii

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SOUTHUEST RESEARCH INSTITUTE

Orjfanica Analysis Data Sheet(Page 4)

Tentatively Identified CotnpoundsJAS Compound NameNumber

I

III

EstimatedFrac- Scan ConcantratiorNumber

I

002197

IIIIIII

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Orgaaica Analyaic Data Sheet. . (P«tf« 1)**¥?*** Waffle: SwRI Ca86 No. 5fcl6sLab Sample No: • F0«n Gc n..-^ „ . ,-2,Sample Matrix: Soil <***!£?***,* r^-it< *Data Release Authorized By: KS±S?» ?", : , Iuate Sample Received:..? /;?

Volatile CompoundsConcentration: LowDate Extracted/Prepared; 3 /Date Analyzed: ^ /, /^Cone/mi Factor: £~ pH *Percent Molature (Not Decanted): IS

CASNunber74-87-374-83-975-01 -475-00-375-09-267-64- i75- 15 -075-35-475 -34 -3156-60-567-66-3107-06-2?8-93-371-55-656-23-5100-05-475-27-4

ChloroiethaneSroao *QthaneVinyl Chlor ideChloroe than sMethy lene Ch lo r i d e -^ •Acetone 7 ' "Carbon Disu lf ide1 , 1 -Dieh l o roe th snei , I -D i ch l o roe t haneTran s - I ,2-Di c h l o ro e t h e f t eChlorofor i1 ,2-Dich l o roe thane2~8utanonal f 1 , 1 - f r i c h l o ro s t han eCarboit Tetrachlor idsVinyl Ace t a t eSroaiod ich lor ose thane

ug/fcgIOUIOUIOUIOU3 Stfa -Wtfsusu5U5U5USU

IOU5USU

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CASNutber78-87-510061-0279-01 -6124-48- 179-00-571 -43-210061-011 10 -75-875-25-2591 -78-6108- 10 - 1127- 18 -479-34-5108-88-3108-90-71 00 -4 1 -4100-42-5

1 ,2-Dich loropropane•6 r r3f t s - l ,3-Di ch l o ropropenoTr i ch lo roe thene

Oibronoch loronethane1 , 1 .2-Tr i ch lo r .oe thaneBenzene

5 Ci s- l ,3-Dich lo ropropene2-Chloroethy iv iny i e therSroaofor s4-Hethy I -2-Pef t t anone2-HexanoneTetrachloroethene1 , 1 ,2 ,2-Te t r a c h l o r o e t h a n eToluene ^^ChlorobenzeneEthy lbenzeneStyreneXylenos

It

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002198

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SOUTHWEST RESEARCH INSTITUTENo: F O ££ ! 1

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AS Compound NameriEstimated

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002199

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Laboratory Name: SwRI_ Case No: Or '- ('oILab Sample No: rlr-v^ MS Qc Repo^t No. 5fe A**(Sample Metrix; Water Contract No: ( - = • £ - ' - i • 1Data Release Authorized By: Date Sample Received- -->

Volatile CompoundsConcentration: LowDate Extracted/Prepared: 3Date Analyzed: -i/u /p?^Conc/Dil Factor: I pHPercent Moisture (Not Decanted):

•CASNuaber

17 4 - 8 7 - 3 Ch1oro«e thane7 4 - 8 3 - 9 8ro ( soae thane7 5 - 0 1 - 4 V i ny l Ch l o r i d e

17 5 - 0 0 - 3 Ch l o r o e t h a n e7 C - 0 9 - 2 He thy l e n e Ch l o r i d eo7- t .4- l A c e t o n e7 5 - 1 5 - 0 Carbon D i s u l f i d e

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Xy lenes

I Data Reporting Qualifiers/aiues If the result is a value greater than or equal to the detection liiit, report the valueU indicates coipmind -as analyzed for but not detected. Report the ftiftiiua detection li.it for the swle *ith the u! ' •? ' ?3^K°n n?nSary c°Ttrat i°? dilyti°n 3Ctioft (rliis is m n8C8SS8ri1^ «• ^truient detection lliit)footnote should be read U coipound «as analyzed for but not detected. The nuiber u the tiniaui attainlh 1. li« t f«i indicates an esti.ated value. This fla. is used either »hen estiiated a concsntral o o t t

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002217

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Sample NumberSOUTHWEST RESEARCH INSTITUT£

Orgamcs Analysis Data Sheet(Page 1)

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5iO1055>5-55

I Data Reporting Qualifierswaiues If the result is 3 value greater than or equal to the detection Ilait, report the value.u indicates coepound was analyzed for but not detected, tepcrt the fiiniiui detection liiit for th« sample mth the U

(e.g . IOU) based on necessary conegfitrition dilution action (This is not necessarily the instruient detection liiit). Thefootnote should be read U coipound was analyzed for but not detected. The nuiber is the ainicui attainable liiit for the saaple.

Ij Indicates an estiiatcd value. This flag is used either when estiaated a concentration for tentatively identified toipourids Hherea 1:1 response is assueed or when the id$s spectral data indicated the presence of a coipound that teets the idsntificUionI criteria but the result is less than specified detection liiit but greater than zero (e.g. IOJ) . If lint of detection is[ 10 ug/1 and a concentration of 3 ug/1 is calculated, report as 3J.C This flag applies to pesticide parameters where the identification has been confiraed by 6C/HS. Single component pesticidosI MIO ng/ul in the final eitract should be conf irmed by GC/HS.

[B This flag is used whea the analyte is found in the blank as well as a sasple. It indicates possible probable blank contaiination1 and warns the data user to take appropriate action.S spiked coapounds

002218

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Laboratory Name: SwRILab Sample No: <0 fiD0// /*£Sample Matrix: Soil0at* S*le**e Authorised By:

Analyst* Data Sheet(Pag* 1) Caee No:

QC Report NContract No:Date Sample

CASNuaber74-87-374-83-975-01-475-00-375-09-267-64- i75- 15 -075-35-475-34-3156 -60-567-66-3107-06-278-93-371 -55-656-23-5108-05-475-^7-4

Volatile CompoutidaConcentration; LowDate Extracted/Prepared: ?Date Analyzed: 5///^Conc/Dil Factor: & pHPercent Moiature (Not Decanted): /

ChloroaethaneBrosoaet luncVinyl ChlorideChioroe thaneHethylene Chlor ideAcetoneCarbon Bisulf ide1,1-Dichloroethene1 . 1 -Di ch lo roe thanef r a n s - I ,2-Oi c h l o r o e t h e n eChlorofora1 .2-D i c h ! o r o e t h a n e2-Butanorit ;1 , 1 , 1-Tr ich loroethar i f lCarbon Tetrach lor ideVinyl AcetateBroff l od i ch l o romethane

ug/kg10UIOUIOUIOU

'V3 >tfft ietj5U

-S 5tfSUSU5U5U

IOUSUSU

IOU5U

CASNusber78-87-510061-0279-01-6124-43- 179-00-571-43-210061 -0 1HO-75-875-25-259 1 -78-6108-10- 11 27 - 18 -479-34-5108-88-3108-90-7100-41 -4100-42-5

l ,2-0ich loropropar i e6 Trans- l ,3-Dich lo ropropeneTr'ichloroethefteDib ro rao ch l o rOAethane

1 , 1 ,2-Tr i c h l o rQe t h a n eBenzene•5 Ci s- l ,3-Dich lo roprapene

2-ChloroethylvinyletherBros iofora4-Hethy i -2-Pen tanone2-HeKfinoneTetrach loroethene1 , 1 ,2 ,2-Te t e a c h l o r o e t h a n eTolueneChlorobenzeneEthylbenzeneSty c e n e

Xylene s

sr

Data Rapoi'tinjValues If the result is a value greater than or equal to the detection liiit, report the value.U Indicates compound Has analyzed for but not detected. Report the linisui detection liiit for the saiple M. t h the (i(e.g. IOU) based on necessary concentration dilution action (This is not necessarily the instruient detection licit). Thefootnote should be read it coapound was analyzed for but not detected, rhe nuiher ,'s the siniiui attainable lisit for tfioJ IndicaUs an sstieatsrf value. This flag is used either when estimated a concentration for tentatively identified coipounds uhera 1:1 response is assuaed or when the lass spectral data indicated the presence of a compound that ssets the identificationcriteria but the result is less than specified detection liait but greater than zero (e.g. IOJ). If liiit of detection is10 ug/1 and a cencentratian of J ug/1 is calculated, report as JJ.C this flag applies to pestkide paraaeters where the identification has been confined by fiC/fu. single component pesticidesJ- IO ng/ul in the final extract should be confiraed by 6C/NS.8 This flag is used Hhen the atalyte is fmmd in the blank as xell as a saiple. It indicates possible probable blank contaiinatiacand uarns the data use/ to take appropriate action.

002230

I1I

i

I

xSample Number SOUTHW&Sr RESEARCH ZNSrx rare'

LaboratorrLab Sample No:Sample Matrix: SoilData Release Authorised By:

Organics Analysis Data Sheet(Patfe 1)

Caw No:QC Report No:Contract No:Date Sample Heceived:

CASNudber74-87-374-83-975-0 1 -475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108 -05 -475-27-4

Volatile CompoundsConcentration: LowDate Extracted/Prepared: 3Date Analysed: j?//f/J&Cone/Oil Factor: £~ pHPercent Moisture (Not Decanted): \J I L 9 f\

ChloroaethaneBrottoaethaneVinyl Chlor ideChlo ro e t han eHethylene Chlor ideAcetoneCarbon Disulfide1 , 1 -D i c h l o ro e t h en e1 . 1 -D i c h l o ro e t han etrans- l ,2"Dich ioroethen6Chlorofori1 .2-D i c h l o r o e t h a f t e2-6utanoneI , l , l -Tr i ch loro6thaft @Carbon fetrachlorideViny l Ace t a t eBroaod i ch loromethane

5

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5U^SU5U5U5U

IOUSUSU

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CASNuaber78-87-510061-0279-01-6124-48- 179-00-571-43-210061-011 1 0 - 7 5 - 875-25-2591-78-6108-10-11 2 7 - 1 8 - 479-34-5108-88-3108-90-7100-4 1 -4100-42-5

1 ,2-Di ch l o rop ropane6 Trans-l,3-0ichloropropene

TrichloroetheneDibroraoch l or o«e thaneI , l i2-Trich loc .o _ethaneflenzene

5 Cis-l ,3-Dichloropropene2-Chlocoe thy I .v i ny l e therSroflofora•t-Hethyl-2-Pentanone2-Hexanonefetrach loroethensI t 1 ,2 ,2-Ts t r a c h i o r o e t h a n efoiueneChiorobenzene£ thy lben/eneStyr sne

Xylenes

,5-

K;KU

Data Reporting QualifiersValues If the result is a value greater than or equal to the detection liiit, report the value.U Indicates cospoumf was analyzed for but not detected. Report the liniiua detection litit for the saipU with the (J(e .g . iOUl based on necessary concentration dilution action (This is not necessarily the insfcruBent detection liait). Thefootnote should be read U coipound xas analyzed for but not detected. The number is the aifliaui attainable liait for the saeple.J Indicates an estieaUd value. This flag is used either when estiiated a concentration for tentatively identified coipounds wherea hi response is assuisd or Khen the aass spectral data indicated the presence of a compound that teett tha identificationcriteria but the result is (ess than specified detection liiit but greater than zero (e.g. !OJ). If Lisit of detection is10 ug/1 and a concentration of 3 ug/1 is calculated, ropart as JJ.C This flag applies to pesticide paraeeters where the identification has been confused by GC/HS. Single co^onettt pesticides>--i(i ng/ul in the final eitract should be confined 6y GC/HS.8 This flag is used when the analyte is found in the blank as well as a sagple. It indicates possible probable blank contaminationand warns the data user to take appropriate action.S spiked coipound$

002231

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002233

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Organice Analysis Data SheetLaboratory Name: SwRLab Sample No: 3Sample Matrix: SoilData Relaaae Authorized By:

Case No: <w iQC Report Nor^"& Contract No: &$ - 01Date Sample Received: J /g /

rt // 77 ' '

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CASNucber7 4 - 8 7 - 37 4 - 8 3 - 97 5 - 0 1 - 475-00-375-or-z6 7 - 6 4 - 175- 15 -075-55-47 5 - 3 4 - 315 * > - bC-567-66-3107-Ot*-27 8 - 9 3 - 37 1 - 5 5 - 656 -23 -51 0 8 - 0 5 - 475 -2 7 -4

Volatile CompoundsConcentration: MediumDate Extracted/Prepared: 3Date Analyzed: J //7/^6> /Conc/Dil Factor: if pH (/Percent Moisture (Not Decanted):

Chloroae thaneSroff loae thaneViny l Ch lor i deChloroethaneHethy l ene Chlor ideAcetoneCarbon Di su l f i d el , I~Dichloroethene1 . 1 -D i c h l o r o e t h a n eT r a n s - 1 ,2 -D i c h l o r o e t h e n eCh l o r o f o rm1 .2-Dich loroethane2-Butanone1 , 1 , 1 -T r i c h l o r o e t h a n eCarbon fe t rach lor i deV i n y l Ace t a t eBro«od i ch loroff i8thane

ug/kgIOOOUIOOOUIOOOUIOOOU£ -&eotrojjmtrsoouS soou—soousooui &eey-

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CASNuaber78-87-51006 1 -0279-0 1 -61 24 -48 - 179-00-571-43-210061 -0 11 10-75-875-25-2591 -78-6108-10-1127- 18 -47 9 - 3 4 - 5108-88-3108-90-7100-41-4100-42-5

l ,2-0ich l o ropropane-6 T r a n s - 1 ,3 -D i c h l o r o p r o p e n e

Tr i ch l o roe theneOibroatoch loro i f i e thanel , l ,2 -Tr i c h l o?a e t h a n eBenzen e

-5 Ci s - l ,3-0i c h l o r op rop en e2-Chloroethy iv iny l e therBromofona4-He t h y i -2-Pen t a n o n e2-HexanoneTetrachloroetheneI , l t 2 ,2 -T e t r a c h l o r o e t h a n eTolueneCh lo robenz en eE t hy l b e n z e n eStyr en e

Xy iene s

SOt5QC> set50(50!1 «ffl501

lOOf501

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Data Re porting QualifiersValues IF the result is a value greater than or equal to the detection liiit, report the value.U Indicates coipotifid was analyzed for but not detected, deport the liniiui detection liiit for the saiple uith the u

(e.g. 10U) based an necessary concentration dilution action (This is not necessarily the instrument detection liiit). Thefootnote should be read U eoipound was analyzed for but not detected. The nuaber is the tiniaufi attainablg lieit for the saiple

J Indicates an estimated value. This flag is used either uhen cheated a concentration for tentatively identified coipounds uhena i;l response is assuied or when the lass spectral data indicated the presence of 3 coipotind that leets tha identificationcriteria but the result is less than specified detection iiiit but greater than zero (e.g. 10J ) . IF liiit of detection is10 us/1 and a concsntration of 3 ug/1 is calculated, report as 3J.C This flag applies to pesticide paraaeters where the identification has been confined by 6C/HS. Single exponent pesticidesMID ng/ul in the final cUract should be confined by (SC/HS.B This flag is used Khen tha analyte is found in the blank as «ell as a saipie. It indicates possible probable blank contannatioiand warns the data user to take appropriate action.S spiked cospounds

002240

. . 0SOUTHWEST RESEARCH INSTITUTE

Sample No:Case tio:

II

QrgamcB Analysis Data Sheet(Page 4)

Tentatively Identified Compounds/tAo « j « EstimatedGAS (impound Name Ppac_ Scan concentratiot:Number tion Number utf/fc***********************t*********t*********t****w^^

002241

II

I

Uttertte»y Warn*

002242

IEwMvnM

«...*• MMMHUMMi

V* •MMMMMan KK

«-

ie.

-"

7 85

002243

' .79

III

No\/<*d

I

V,

ict Analysis Dtta Shwit3)

S«mpt«

Low Mudium (CireltOntj

'Liquid * Liquid f stfftetrfffrSYes

Numter319M-6

319-86-818 899305-00 -21024-S7-3&S9-98810-57.172 55-972-20-833213 -65 -97254-81031 -0-7-850-29-37243-553494.70-S57-74-98001-35 212674- 1 1 - J1 1 104-28-21 1 1 4 1 - 1 6 - 563489-21 -912672-29-6

1 1096 62 5

AI0** 8HCSflta-SHC

4 -ooe

4 4 .000

4 A -ODT

Aroc iOf- 1232ArMlor.1242

1260

c

s

V, * Volume af **u*ct mjscitti tuHV8 > Vafums cf watar astrscted (ml)W& " W«ight of ssmpit tfcuacud (g)V( * VoJuma of total attract (ull

V. .,

7 85

002244

" S OSample Number

SOUTHWESr RESEARCH XNSriruretflfrfri^ 3?'^ ^

Or^anics Analysis Data Sheet(Page 1)

Laboratory Name: SwRI . Case No:Lab Sample No: S fQ CO3 » H. QC ReportSaaple Matrix: Soil Contract No: (^Ot " ''Data Release Authorized By: fete Sample Received: 3 / $ /

GASNuflber7 4 - 8 7 - 374-33-97 5 - 0 1 - 475-00-375-09-2b7-&4- l7 5 - i S - O75 -35 -47 5 - 3 4 - 3156-&0-567 -66 -3107-06-27 8 - ^ 3 - 3

1 0 8 - G 5 - 47 5 - 2 7 - 4

Volatile CompoundsConcentration: MediumDate Extracted/Prepared: 3Date Analyzed: 3 /fl / & /Cone/Dil Factor: 4 PH (j>Percent Moisture (Not Decanted):

Chlaros te thaneGroaoaethaneViny l Ch lor i deChloroethaneHethy lene Ch lo r i d eAcetoneCarbon D i s u l f i d ei , 1-Dich loroethene1 , l -D i c h l o r o e t h a n eTrans- 1 ,2-Dich loroe thensCh l o r o f o rm1 ,2-Dich loroethane2-Bu t a no n e1 , 1 , 1 -Tr i c h l o ro e t han eCarbo n Te t r a c h l o r i d eVinyl AcetateBro iod i c h l o ro f f l e t hane

ug/kg1000U1000U1000U1000Usoou

)-HJ60y-500U5--§60trsoousoousoousoou^tesmr500Usoou

1000Usoou

GASNumber78-87-510061-0279-01 -6124-48-179-00-571 -43-21006 1 -0 11 10-75-87S -25 -2S91-78-6108 - 10 - 1127- 18 -479-34 -5108-88-3108 -90-7100-4 1 -4100 -42 -5

u v L-, \ \1 ,2-D i c h l o r op ropan e

6 Trans-1,3-DichloropropeneTr i ch lo roe theneDibrofitcchioroffiethane1 , 1 ,2-Tr i c h l o r o e t h a n eBenzene

•5 C i s - l ,3-D i c h l o r op r op e n e2-Ch1oroethy 1vinylether

500500

4-Hethy l-2-Pentanone2-HexanoneTetrach loroetheneTolueneCh lo rob en z en eEthyibenzeneStyreng

Xylenes

500so:*

50C1000

500100G1000

500500• sec

Data Reporting Qualifiersvalues If the result is a value greater than or equal to the detection liiit, report the value.U Indicates coipound tias analyzed for but not detected. Deport the liniiui detection lint for the saipie filth the u

(e.g. 10U) based on necessary concentration dilution action (This is not necessarily the insistent detection Haiti, fhefootnote should be read U coipmrad uas analyied for but not detected, fha nuioer is the ainiiui attainable lint for the saaple..1 Indicates an cstiaated value. This flag is used either Khen estieated a concentration for tentativelr identified cowunds Mherea 1:1 response is assuicd or when the lass spectral data indicated the presence of a coipotind that seels the identificationcriteria but the result is less than specified detection Hut but greater than zero (e.g. 10J). If liiit of detection is10 ug/1 and a concentration of 3 ug/1 is calculated, report as JJ.

C This flag applies to pesticide paraieters where the identification has been confined by GC/H5. Single coaponent pesticides) : IO ng/ul in the final eitract should be confined by SC/HS.S This flag is used uhen the analyte is found in the bland as well as a saiple. It indicates possible probable blank ctifttaainationand warns the data user to take appropriate action.S spiked coipounds

002245

ii SOUTHWFST RESEARCH INBTITUTESample No: F D CO 3 fTl^ 0Caae No: 5636

CAS Compound NameNumberi

Organics Analyaia DaU Sheet(Paffe 4)

Tentatively Identified CompoundaEatiaatad- Scan Concentration

tion Number ug/j&x*********ts*»sft»«*«t

i

002246

IIII

I

7 3S

002247

(flu «niti/an)w.

"01

n

«t

"U

B

I

Cr*

002248

D-.LaboratoryCtst No -K ies Analytis Data(Pag« 3)

S«mfil* Number

IMoicturc

GAS3 1 93 1 9 * 5 - 7

306-00-21024-57-3959-98-880-57-t72 55-972-20-6332U-85-972-54-81031-07-8SO-29-372-43-5S3494-70-S57-74-9S001-33 21 2674 . 1 1 -21 1 104.28-21 1 1 4 1 - 1 8 - 563469-21 -«12672-23-61 1097.6A-11 1036 82 S

SHC

Alarm

4 4 -ODEIndnn

4 4 -OOD

4 4

Aroelor-1232Ardclar-1242

CIWAUO QY«« QNe , ,Punntl grtrscnon Q Yes

Commuout Liquid • Liquid Extraction

Aroclor-1248

UfiO

^^-—

V( *of *atr«ei lull

(ml)a Wfttght of umplt «Rtr«CtBd (01

total aairact Ml

POTm 7 85

002249

-.It-

9 989S

002250

r/85

002251

5636 6

"Iff*

002252

Contractor s.a" c^l ' 9/Jy '

WATOtfl m&r.to CQWfOOWO tH&L.fftC OR tJMtffOWtl co»c. twit* 0*0*.

3 I 2 7

~i / 3 7~ —;—^ y

Jl

cnCosnmonfs:

FORM IV 7/85

002253

o

Q ,fV

0!

fc01-3ooCl

5636 69

^O-9,(DO(X*

5^

5.*a-3l

m<t>«>fcK.iOu.

002254

5636 6 G'ample Number TI TUTB

iboratory Name: SwRI,ab Sample No: " 7!0(g^c

Organics Analysis Data Sheet(Page I)

Case No:"Sample Matrix: Water ' ^ I /

Release Authorized By:contract No: C- ft - c i • T t c, >

Date Sample Received: * /«

CA

Volatile CompoundsConcentration: LowDate Extracted/Prepared: " /\\ /- L.Date Analyzed: ""' . /n /B-,-Conc/Dil Factor: I pH (#Percent Moisture (Not Decanted): ^

4 - 3 7 - 3 Ch l o r o a e t h a n e' 4 - 9 3 - 9 B r o s c s e t h a n e' 5 - 0 1 - 4 V i n y l Ch l o r i d e5 - 0 0 - j Ch l o r o e t h a n e5 - 0 ^ - 2 Me t h y l e n e C h l o r i d e7 - 6 4 - 1 Acetone

' 5 - 1 5 - 0 Ca r b o n D i s u l f i d e5 - 5 5 - 4 1 , 1 -D i c h l c r o e t h e n e' 5 - 3 4 - 3 1 , 1 -D i c h l o r o e t han e5 f c - * 0 - 5 T r a n s - ! , 2 -D i c h l o r o e t h e n e

. 7 - 0 6 - 3 C h l o r o f o * a0 ^ - 0 6 - 2 I t2-D i c h l o r o e t h a n e' 9 - ^ 3 - 3 J -8 u t a n o n e" I - 5 5 - » ? l , l , i - T r i c h i o r o e t h a n et ^ - 2 3 - 5 Carbon Te t r a c h lor He. 0 8 - 0 5 - 4 V i n y l A c e t a t e' 5 - 2 7 - 4 B f o n o d i c h l o r o m e t h a n e

IOUIOUIOUiOU

5U5U5U5U5U5U:ou5U5U

IOU5U

C A SNyiber7 8 - 8 7 - 51 0 0 6 1 - 0 2 -7^ -0 1 -61 2 4 - 4 8 - 17 3 - 0 0 - 57 1 -43 -2i ao t , i -o i -I I O - 7 5 - 8^5 -25-2591 -78- t ,

^ - • 4 - 5l d ' J -38 -3| Q9 _ gQ -71 0 0 - 4 1 - 41 0 Q - 4 2 - 5

f\ D,Lug/1

l ,2 *D i c h l o r o p r o p a n eT r a n s - l ,3 -D i c h l o r o p r o p e n eTrichloroethene1 , 1 , 2 -T r i c h l o r o e thaneBenzene

5 C i s - 1 ,3-Di ch l o rop ropen e2-Ch lo roe thy I vinyl e the r4-He thy l -2-Pen t a non e2-HexanoneTetcachioroetheneI t 1 , 2 , 2 -T e t r a c h l o r o e t h a n eTolueneChlorobenzene^ t h y l b e n z e n eSty r e n evylenes

c~J5c

1C101C

5

Data Reporting QualifiersValues If the result is a value greater than or equal to the detection hut, report the valueI indicates cMpoufld «as «nairzed for but not detected, deport the HIUIUB detection liiit far tto SWU Hith the UI e.g. IOU) based on necessary concentration dilution action (This is not necessarily the instruient detection li.it) The

, |CTI? "J? ~hwd/or J"1 B0t dettcted- rhe •*» « «• •wi«" ^tamable liiit fo^ the satple.h

rtl?h

fl11 1S USB e!1 W Mhe"estiMtfl<) a coBcantraHon for tentatively identified compounds Lta hi response is assuied or xhen the lass spectral data indicated the presence of a coipound that icets the identificationcr iter ia but the rssult is less than specified detection liiit but greater than zero (e.g. 1DJ ) . If U.it of detection is10 ug/1 and a concentration of 3 ug/1 is calculated, report as U.This flag applies to pesticide paraieters -here the identification has been confined by fiC/HS. Single exponent pesticides> = I8 ng/«l in the final eitract should be confined br 6C/HS.This flag is used Bhen the analyte is found in the blank as * * 1 1 3S , sagpie. it indicates possible probable blank contaunationand narns the data user to take appropriate act ion.spiked coipnynds

002255

ISample No: -. t/~ '•"Case Mo: .-. ^ .,.

Ir

5636 6SOUTHWEST RESEARCH INSTXTUTE

Or^anica Analysis Data Sheet(Pajfe 4)

Tentatively Identified CompoundsCAS Compound NameNumber

- B>i Estimated- Scan Concentratior

i C i fc:

002256

iiiiiiiiiiiiiiii

SaaipU Number

c l 5636 6SOUTHUE3T RESEARCH INSTITUTE

'"•^ Ce t L cic' L^: Jel VU -^

^2

3wRILaboratoryLab Sample Wo: 0 £SaapU MatrU: SoilPaU lUUaM Authorltad By:

Orfanica AnAlr*i< Data 5ha«t(P«tf« UHo: •

DaU flaapi* Itooalrad: " / • /%

VoIatiU Compound!Co«c«ntr«tlon; LowtitraoUd/Pr«par«d: ? / I /^Analysad; ^ /H A" vConc/0U Factor: / * pH ^Percent Motttura (Hoi DaaaaUd); f> iU. L,

CASNu«btr7 4 - 0 7 - 374-83-97 5 - 0 1 - 475-00-J75-09-26 7 - 6 4 - 175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-37 1 -55 -656-Z3-5108 - a5 -47 5 - 2 7 - 4

ChloroiethantIroaoaathanaVinyl Chlor ideChloroethaneNethylene Chlor ideAcetoneCarboa BisulfideKl-Oich ioroethene1 . 1 -D i ch l o roe t hanefrans-l ,2-0ichioroethaneChlorofora1 .2-Dictt lorde thane2-lutanofta1 . 1 , 1 -Tr i ch loroc thaneCarbon TetrachlortdeViny l Ace t a t e

10Utou10UiOU

CASmiaber78-87-5 1 ,2-Oich Ioropropana10041*02-4 tran«-l,3-eichloropropana79-0 1 -6 Trichlorotthane79-00-571-43-2

i.l .2-TrUhloroethanelafticne

5Usu5U5U

IOUSUsu

IOUsu

I IO-75-75-25-2 2-CMoroethyUiftr latharIroaoforalOfi-10-1127- 19-479-34-5108-88-3108-40-7100 *4 1 -4100-42-5

2-Nctaajoncrttrachloroathent1 , 1 ,2,2-Tatrach loroathana

Slyrtftt

DaU Raportlntf Quali/lsraIf Ui rtsalt is i viiti araaiir Uaa or «<*ul ta Ui fttactias lint, riaart UalAdic«tM caiaevftd us aaalyiad for tat Mt 4fttttad. ftaaart tit liaiM «ttacttaa liiit far UM MIP!« aiU tha tfU.fl. 10B) tuad aa »»cr$ta/T caacaatratiaa dilaliai «li» (Tkis is nat mttssarilr U* i*str«nt *tactiaa hut). n»afaotaala rtwld ta read tf caiamd NS mirtaa1 for tat wt attattad. Tta antar is tta iiaiaa ittaiartli lint far tta u»UtndicitH ta astiiatad valaa. Tkis flat is «sed fitaar AH attiiatad 4 caaciatrttiaB far taatitinlr iavatifiad cwaaidsi 1:1 rataooss if «taitd ar ihaa tfta i«i twttril «aU Udieatad U» arasaaca af t caipaaad tftat wu tfta idntificitiaRcriurit act IM rasaU is last Uta SBtcifitd avtactiaa liiit tat «TNUr tftia m* (*.<. I8J). if lint af aataftiaa 1$10 «/l aa4 t caKBHrJtian of ) tg/1 ts cilcalitadt r«wrt n U.nils fl«9 wpli«s ta us tic! to winters ritri ae idantificitiaa Ms MH canfirHd by tt/«. SiafU caipaaant pastuidas):IO fif/al ifl tfta fi/ul attnet staid ta cufirud by «/W.This fl<4 is and aften Ul wilrl* U faafid ia taa »Iaak u nil is i stapla. It iadiaUs WKI»!< araoa^la altak«id WM tfia data anr U lala wrapriati miaa.caimtds

002257

IJSnmple No; . CACa*« No: -iIf*riiiiiiiiiii

5636 6RESEARCH T N S T I r a r e

Organic* AruUy«t« DmU Shevt4)

TenUtively Identified Compound*:AS Compound NAIMNumber Pr«c- Scan Concentration

ttttt

I

002258

I5636 6 '".t.

r RESEARCH INSTiTUTESample Number

IIIIIIIIIIIIIII

Laboratory'Wame: 3*RfLab Sample No; SData Relee.ee Authorised By:

Sheetae No: -^Saport No: i >&^^

Contract No: £?? ' °*Date Sample Received: 3

Volatile Compound*Concentration: MediumDate Extracted/Prepared: 3Date AnmlyMd; ,?/|7/St>Conc/Dtl Factor:* pHPercent Moietur* (Hoi Decanted):

• ' S - O i - 4- -

5 - 1 5 - 05 - 3 5 - 4

Chlo ro e e t han eBroeoieefhaneVi f t y i c h l o r i d eChloroethane" e t h v l e n e Ch l o r i d eAce t o n e cCarbon D i s u l f i d ei , " • n t ^ ' f t r r t f ' ^O r r lO ^ i o4 t A i/ 1 !- I " i IJ * "J V V ' ' V ' ' t

1 , \ -DicMoroe thane' r a n s - 1 , 2 - D i c f i tor oe theneCniorofore1 . 2 -D i c h i o r o e t h a n e. -8 ' j t a n o n e1 , 1 . 1 - T r i c h l o r o e t h a n eCa r t o n T o f r a c M o - : deV i n y l A c e t a t e8roeod i c n l o r o « e t h a n e

ug/kg1000UIOOCU1000U1000Usoou

CASNuaber' 8 - 8 7 - 5100^ 1 -02-

500U500U500U500U5QQUSOOU

1 , 2 -D i c h l o r o p r oP a n eTr ans-1 ,3-Du.h loropropeneTruh l o ro e t h e n *Dibroeoch loro iethane1 . 1 , 2 - T r

i - 4 ^ -2 Ben z e n * *i ooft i-o i-5 c i s- i . :1 1 0 - ^ 5 - 3 2-Ch l o r c e t h y l v i n y l e t h e r7 5 -25 -2 firctofori

1 2 4 - 4 8 - 1" ' - O C - 5

SOOUsoou

108- 10 - 11 2 7 - 1 8 - 479 -34 -51 0 8 - 3 8 - 3

soou 1 0 0 - 4 1 - 41 0 0 - 4 2 - 5

To lu en eCh l o r ob e n z e n eEthv lbenreneStyr en e

500SOO500500500500500

1000'500

1000:i GOO-

500500'500500'500'500500'

Data Reporting1 QualifiargIf tfce rrsilt is * vtlw grtitcr thaa or teul U tHe detection lint, report ttie value.Indicites coipwW MS i*«lr;e^ for but not dttKted. tt»ort tie iifliwi dtttctiM lint for tfte saipie »itft the u. e . g . lOUi tastd «» wceswrr coacratritioa diletiw Klioa (Pus is not rtecKsarily tlte iftstrymt VrrtiM linti . ',ieFootnote shwid b« read U co00ttftd MS Mahzed for tat Mt dtUcttd. rNf wnocr is tte linnui atUmabie liiit for th* saiple.Indicates M estimated valM. This fin is «s*d titter i*wn tstiutfd a coAtHtratiOA for teatituetr identified ceipot»t4s ifterea 1:1 resMftse is tssutd or «hea Us HSS spectral daU iftdicaUd tte 0r«S8nce of a coifWAd that ieets the io>ntiftcationcriteria bit tfct restlt it ttss tfcafl specified detection lint Ut jreater than lero (e.g. IOJK If luit of detection is10 flf/l and a cwicwtmiw of 3 rt/l is caicwUted, report as 3J.Tltis fl*g applies to pestirj^ ptraieters Hhere the identification has been confined by fiC/NS. Single coiponent pesticides> : 1C fig/ul in the ftwt ettract shoo Id he confined 6r &C/HS.nil fiat is aserf sftea the aMlrte is found iff the Hank is wit as a saiple. It indicates possible probable blank contannationand (tarts the data user to take appropriate action,spiked coiBOunds

002259

IIcIImptoNo:

Caae No:

*AS Compound NameNumber

5636 6SOUTHU£Sr RESEARCH TNSTITUT£

Organic* Analyse Data Sheet(Patfo 4)

Tentatively Identified Compound*Estimated

Prac- Scan Concentrationtion Number "(/$&:»««t**tx*ttj6ttt*ti**********tt*t*tAttJ*t

IIIIII

002260

iiii

N«m« ' _ ^ *

OfgtAfeft AMlyafs Data ShMt

_**"•***«*«

4Uatfum (OrcttOni) ">/>

CAJI

11*44*4

1C4-W-I

MM 3

i irit-i130-33-2116-iMt•1.17-4

1

0< •

fMOA<yeA«•

Ma nMhKmc»tia«itftf MH *•! . 4

7 as

002261

5636 6

Ieotifio

I

10..11..12..13..

17..It.If

St..

M.

? 85

002262

5636 6 8CM* No V / A nic* Analysis Data 3h**t

3)

Low / M«dium One)

'OilPsream Moisture

GPC Cleanup QY*« EWo . ,Sipacaiory Funnel 6«fietien {3 Yes/ \Continuous Liquid • liquid detraction

6A*319-6A-S31585-7

78-44-fi30* -00- 2

e o s i72-58-972-20-S332U-65-972-S4.81031-07-850-29-372-43.fi53 *94-70357-74.0S001-3S212074- 1 1 -21 1 104-26-21 1U 1 - 16 5

1 109682-S

SHC

4 -ODIEndrin

4. 4 -000

4 4 -ODtgndrm

Aroc lar-1232

1360

V( s Valuta 0* ARirici mjeettd (uUVg * Vetuma sf water «Kiracifid imiWft «W*ight of umglt «Mraetad (Ql

aitraci (ul)

OfW.

form 1 7 85

002263

5636 6 2 rCBOUTHWES r RESEARCH INS TI T U

Sample No: \Case No: ^-

3 1 7 <lr C

Organica Analysis Data Sheet(Page 4)

Tentatively Identified CompoundsCAS Compound NameNumber

EstimatedFrac- Scan Concentrationtion Number

002264

r RESEARCH INS rx TUTE:5636 6 201

Laboratory Name: SwRILab Sample No: TSample Matrix: SoilDaU Release Authorized By

e o : > ? .Report No: 630 ^ntract No: 6tf ~^'~'''at« Sample Received: 3

CASNumber7 4 - 8 7 - 374-83-97 5 - 0 1 - 47 5 - 0 0 - 375-09-267-64- 175-15-07 5 - 3 5 - 475-34-3156-60-567 -66 -31 0 7 * 0 6 - 278-93 -37 1 - 5 5 -&5 6 - 2 3 - 5108 -05 -47 5 - 2 7 - 4

Volatile CompoundsConcentration: LowDate Extracted/Prepared: 3 /Date Analyzed: 3 /H/% (0Conc/Dil Factor: / pHPercent Moisture (Not Decanted): Nff D . L ,

Chl or oae thaneBroaoffle thaneViny l Ch lor i deChloroe thaneMethy l enc Ch lo r i d eAce ton eCarbon Disulf ide1 , 1 -D i ch l o roe t h ene1 . 1 -D i c h l o r o e t h a n eTran s - l ,2-D i c h l o r o e t h e n eCh lo ro fo ra1 .2 -D i c h l o r o e t h a n e2-Bu t a n o n el , i f l -Tr i c h l o r o e thaneCarbon Te t r a c h l o r i d eVinyl Ace ta t eBroaod i c h l o roae thane

/NIOUIOUIOUIOU

5UIOU

5Usu5U5U5U5U

IOU5U5U

IOU5U

CASMuaber78-87-510061-0279-01 -61 24 -48- 179-00-571-43-210061-011 10 -75-875-25-2591 -78-6108-10- 11 27 - 18 -479-34-5108-88-3108-90-7100-41 -4100-42-5

ug/l1 ,2-Di ch l o rop ropane

•6 Trans-l,3-DichloropropeneTr i ch l o roe theneDibroAOChloroae thaneK1 .2-Tr i c h l o ro e t han eBenzene

•5 Cis-1 ,3-Oichloropropsnt2-Ch lo roe thy l v i ny l e t h e r4-Hethy l -2-Pen tanon e2-HexanoneTetrach loroethene1 , 1 ,2 ,2 -T e t r a c h l o r o e t h a n eTolueneCh l o rob en z c n eEthyIbenzeneSty r e n e

Xylenes

105

10to5c-s555-j5

Data Reporting QualifiersValues If the result is a value greater than or equal to the detection liiit, report the value.u Indicates coipound nas analyzed for but not detected. Report the liniiui detection lint for the saipie mth the u

(e .g . i(Hi) based on necessary concentration dilution action (This is not necessarily the instryieot detection liiit}. Thefootnote should be read U coipound was anaiyied for but not detected. The nuibsr is the ainiaus attainable liiit for the saapU

J Indicates an estiuted value. This flag is used either «h«n estiMted a concentration for tentatively identified coapounds where3 1:1 response is assuied or when the aass spectral data indicated the presence of a coipound that aeets the identificationcriteria but the result is less than specified detection liiit but greater than zero (e.g. 107). If liiit of detection is10 ug/1 and a concentration of 3 ug/1 is calculated, report as 3J.C Fhis flag applies to pesticide paraieters where the identification has been confined by SC/HS. Single cosponent pesticides) = 10 ng/ul in the final estract should be confused by GC/HS.ft This flag is used when the analyte is found ic the blank as well as a saipie. It indicates possible probable blank contaainationand warns the data user to take appropriate action.S spiked toapouncs

002265

IJample No:Case No:

I1

5636 6SOUTHWES r RESEARCH INSTITUTE

Organica Analjrris Data Sheet(Page 4)

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COnGWWtflKX1 UOW wwaium i\»irciv vr*V| «i-U V-- ' 7 .' • -ftejt iitrtcw? 'P'*p*'*4 .„. „„„ ----- — -.. _ S»pf

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ivanup LJ'V* uitory Funnel £xtuouc Liquid • Lil«lA *->'m.'/- OM(J/

CA6 uQ/ leru$''KgNumbtar (Cirtite OR^>3 1 9 S 4 - 61 19-85-7319.86-6$ 8 8 9 978.44-830»-00'21024-57-3i ssse-660-57-172-55-972-20-833213-65-972-54-61031 -07-850-29-372-43-553494-70157-74-S8001-35 212674- 1 1 -21 1 104-29-51 1 1 4 1 - 1 6 - 553469-21 -d12672-29-61 10)9^-49-11 1096 82-5

Aio* »-8MCS«la-8HC0«ita 8«CGammc-BHC (LmdaAciH«otSGhlorAtdftftKeptacnior looxid*Endo<uif*n IDi«idnrt4 4 -ODEErtd'inE^doiiji'Sfi tl4 4 -000Endoftulfm SuH*te4 4 -DOTMeihasvc^iio'Sndf'ft Ktto^*Chlordan*Touio^*n«AfKlw-1016AroclO'-122lArae ior . 1232Aroctor-124;Aroeid '-1248ArocJof ?2S4AroClO' 1260

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002275

Sample Number

5 5 3 5 63°"THHe3T KES£ARCH INSTITUTE

Organic* Analyaia Data Sheetf . (Patfe 1)Laboratory Name: SwRI Q™ Mo. ^/ ^/Lab Sample No: T V 1 T^4- QC^LSrt M ti -/ '>Sample R^trix: Soil ^STJ? f / a ,fData Release Authorized By: SE^B^'J

CASNumber7 4 - 8 7 - 374-83-97 5 - 0 1 - 475 -00 -37 5 - 0 9 - 26 7 - 6 4 - 175- 15 -075-35-475-34-3156 -60-567-66-31 0 7 - 0 6 - 278-93-37 1 - 5 5 - 656-23 -51 0 8 - 0 5 - 47 5 - 2 7 - 4

Volatile CompoundsConcentration: LowDate Extracted/Prepared: 3/ill Sk ,--—•"""Date Analyzed:,^ //;VSu /-Cone/Oil Factor: | PH (£ -. ,Percent Moiature (Not Decanted): IQ £ D L A

ChloroaethaneBro ioae thaneViny l Ch l o r i d eCh io r o e t h a n eHethy lene Ch lo r i d eAcetoneCarbon Di su l f i d e1 . 1 -O i c h l o r o e t h e n e1 » 1 -O i c h l o r o e t h a n eTra n s - l ,2 -D i c h l o r o e t h e n eCh lorofore1 .2 -D i c h l c r o e t h a n e2-Bu t a non el t 1 , 1 -T r i c h l o r o e t h a n eCarbon Te t r a c h l o r i d eV i ny l Ac e t a t efl r oaod i c h i or o s t - t hane

ug/kg10U10U10U10U

fa -Stf:>8 uxr5U5U5U5U5U5U

10U5U5U

10U5U

CASNuiber78-87-510061-0279-01-6124 -48- 179-00-571-43-210061-011 10 -75 -875-25-2591-78-6108 - 10 - 11 27 - 18 -479-34-5108-88-3108- ^0-71 0 0 - 4 1 - 4100-42-5

1 ,2-Di c h l o rop ropan eTran s - l ,3-Di ch l o rop ropen srr ich loroethene1 , 1 ,2-Tr i c h l o r o e t h a n eBen z e n e

5 Ci s- l »3-Dich l o ropropene2-Ch lo ro e t hy l v i n y l e t h e rBroff lofora4-He t h y l -2-Pen t a n o n e2-HexanoneTet rach lo roe thene1 , 1 , 2 ,2 -T e t r a c h l o r o e t h a n eTolueneCh lo robenzeneEthy lbenzeneStyfene

Xy lene s

55555

105

1010

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Valuesu

Data Reporting Qualifiersf the result is a value srttter than or equal to the detects liiit. report the valueindicates coipound vas anaiwd for out not detected. Report the siniaui -.1 the result is («* than specified detection li.it but greater'ihan m (rriojr'iri^rnf^u^nn"0"10 ug/i and a concentration of 3 ug/l is calculated, report as 3J. 9< K IF ll(llt of (tetectlon ls

This flag applies to pesticide paraseters nhere the i<) = 10 ng/ul in the final extract should be confinedThis flag is used Hhen the awlyte is found irt the blank as xeli as a saiple It indict nft«,M« W(lh,Ki. k. i * - -and warns the data user to take appropriate action. 6S POSSlMe probable bianb "«*«•"«wn' coipounds

002276

C r H /*oo3o 6SOUTHWEST RESEARCH INSTITUTE

-2.4-3

Sample No:Cave No:ICAS Compound NameNumber

Org;aiuc« Analysis Data Sheet(Page 4)

Tentatively Identified CompoundeEstimatedFrac- Scan ConcentrationUon Number ug/j&

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Form 1 7 85

002280

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Jample Number sournwesr RESEARCH INSriTUTE

I Organics Analysis Data Sheet(Page 1)Laboratory Name: SwRI Caae No. -.=£. i vc

tab Sample No: -^ ^ ^ QC R6po;t Ro. ^3Vample Matrix: Water Contract No: i-V '~Data Release AuthoHzed By: Date Sample Received: 'i

Volatile CompoundsConcentration: LowData Extracted/Prepared: 3/I t /£Date Analyzed: 3 /h /6C-Conc/Dil Factor: i pHPercent Moisture (Not Decanted):

- 2 7 - 4

Chlo ro« e t ha . - ; eBro t a o u i e t h a n eVi n y l Ch l o r i d eCh l o r o e t h a n eHetny l e n e C h l o r i d eAc e t o n e '2Carbon D i s u l f i d e1 , 1 -D i c h l o r o e t h e n e1 , 3 -D i c h l o r o e t h a n eT r a n s - l , 2 -D i c h l o r o e t h e n eT h l o r o f o r m1 . 2 - D i c h l o r c e t h a n e2-B u t a n o n e1 , 1 , I - T r i c h i o r o e t h a n eCa r b o n r e t r a c h i o r i d eV i n y l A c e t a t eB r o fD o d i c h l o r c a e t h d n e

ug/ 1IOUIOUIOU

r, IOU

5U5U5U5U5U

IOU5U5U

IOU5U

CASNumber7 8 - S 7 - 51 0 0 6 1 - 0 27^ -0 1 -61 2 4 - 4 8 - 17 9 - 0 0 - 57 1 - 4 3 - 21 0 0 b . l - 0 i -1 1 0 - 7 5 - 3' 5 -25 -25 9 1 - 7 8 - 61 0 8 - 1 0 - 11 2 7 - 1 8 - 47 9 - 3 4 - 5108 -88 -31 0 8 - ^ 0 - 71 0 0 - 4 1 - 41 0 0 - 4 2 - 5

i\L1 , 2 -D i c h l o r o p r o p a n e

• b T r a n s - 1 ,3 -D i c h l o r o p r o p e n eTr i c h l o r o e t h e n eDib ro to ch l o come t l i a n e1 , 1 , 2 -T n c h l o r o e t h a n eBe n z e n e

• 5 C i s - i , 3 -D i c h l o r o p r o p e n e2-Ch l o r o e t h y l v i n y l e t h e rBromo f c r i t4 -M e t h y i - 2 -P e n t a n o n e2-Mex a n c n eTe t r a c h l o r o e t h e n e1 , 1 ,2 ,2 -T e t n c h l o r o e t h a n eTo l u e n eCh l o r o b e n z e n eE t h y l b e n : e n eS t y r e n e

x y l e n e s

ug/1

5c5555

105101 0

5

lalues Data Reporting QualifiersIf the ^esuit is a value greater tnan or equal to the detection liait, report the valwrndicates coipound ws analyzed fcr but not detected. Report the •inuui detection hut for thi saaple «-th the ULL f l V" Tfry conrtratl°? lm 3CtIM Uhis 1S ftot nEC6SHri1^ tke ^^trusent d tect i nfootnote should be read U coipound was analyzed for but not detected The nuaoer is the tinum* Ath i » * h i i i , -.,>radicates an esti^ed value, rhis flag is used either «he* esti, ed o a o o t t

a 1 = 1 response is aSS»,ed or «hen the .ass spectral data indicated the presence ? ^sr •""" to » «*• ™h3s been conf-ed * SC/HS-spiked conpounds

002281

(Sample No:Case No: -

5 6 3 3 6SOUTHUES T RESEARCH INSTITUTE

Organics Analysis Data Sheet<Page 4)

Tentatively Identified Compounds

r;.8

AS Compound NameNumberEstimated

Frac- Scan Concentrationtion Num ber ug /I

'V c

002282

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002284

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Organist Analyais Data Shaet3)

Sample

tow Medium

'Oil FactorPercent M&fture

o

P*cticide/PCS*(Circla One) GPC Cle&nup QYe* QNo_k____«™ Sepiriwry Funnel Extueiion tlY*s«_______ Commuous LiQuid - Liquid E*tf*ction

On*}1 19-84.63 19 15 -7319-86-85 8 6 9 9

-44.6309-00-21024-5? 3

SO-57-1?2 55-972-20-83 3 2 1 3 - 6 5 - 972-54-81031-07-8£0-29-372-43-553494-70-557-74-98001 .36 212674*1 1 .2H 104-28 21 1 1 4 1 . 1 6 - 5

1 2 6 7 2 9 - 81 1097-69.111096 82 5

8*?*-BHC0«ita

EnckitutUn i

4 4 .ODEEndrm

4 4 -000

4 4 -DOT

1 2 3 2

Aroelor-1248

1260

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7 85

002285

5638 6Sample Number

SOUTHWEST RESEARCH INSTITUTS

.<-!

Laboratory Name: SwfttLab Sample No: 6Saaple Matrix: Soil

Organic* Analysi* Data Sheet(Pa*e 1)

Case No:QC Report No:Contract No: " ' <«Data Release Authorized By: Date Sample Received; ? /t-

Volatile CompoundaConcentration: LowDat* Extracted/Prepared: •'Date Analysed: 3 /K /€fcConc/Dil Factor: I pHPercent Moiature (Not Decanted): - D.i.i, /-

CAS74-87-374-83-975 -0 1 -475-00-375-09-267-64- 175 - 15 -075-35-475-34-3156-60-S67-66-3107-06-278-93-371 -55 -656-23-5103 -05 -475-27-4

Chloro ietbaneBroaotethaneViny l Ch lor i deChloroethaneMethylene Chlor ideAcetoneCarbon Disu l f ide1 , 1 -D i c h l o r o e t h e n e1 . 1-Oich loroethaneTrans- i t2-Dich loroetheneChlo ro fo r i1 .2-D i c h l o r o e t h a n e2-Butsnone1 , 1 , 1-Tr ich loroethaneCarbon Tet ra ch l o r i d eViny l Ace ta t eBroiodichloroaethane

Ag10U10U10U10U5tf1^0SUSUSUSUSU5U

10U5U5U

10U5U

CASNuaber78-87-510061-02-79-01 -6124-48- 179-00-571-43-210061 -0 11 10 -75-875-25-2591-78-6108- 10- 1127 - 18 -479-34-5108-88-3108-90-71 0 0 - 4 1 - 4100-42-5

1 ,2-Dich loropropane•6 Trans-l,3-Dicnloropropene

Tr ich loroetheneOibroaoch lor oae thane1 , 1 .2-Tr i c h l o ro e t haneBenzene

5 Ci s - l t3-Di c h l o r op rop e n e2-CNloroe thy lv i ny l e t h e r8ro«ofors4-Hethyl-2-Pentanone2-Hexanon eTs t rach lo roe thene1 , 1 ,2 ,2-Tet ra ch l o roe t haneChlorobenzeneEthy l b en?eneStyrene

XyUnes

10&oj

1010

55>5555

Data Reporting QualifiersValues If the result is a valw greater that) or equil to tfis detection lint, report the value.U Indicates eoipound was analyzed for but not detected. Report th« iiniaua detection liflit for the saiple with the U(e.g. 10U) based on necessary concentration dilution action (This is not necessarily the instruient detection lint). Htefootnote should be read U ccipound was analyzed for but not detected. The nuiber is the *iniiut attainable litit for the saspte.j Indicates an estimated vilue. fhis flag is used either uhen estitated a concentration for tentatively identified coipounds wherea 1:1 resoonea is assuied or when the idss spectral data indicated the presence of a coipound that fleets the identificationcriteria but the result is less than specified detection Hiit but greater than mo (e.g. IOJ). If liait of detection is10 ug/1 and a concentration of 3 ug/l is calculated, report as 3J.C This flag applies to pesticide paraaeters (there the identification has been confined by 6C/HS. Single component pesticides) : 10 ng/ut in the final extract should be confined by 6C/HS.9 This flag is used when the analyte is found in the blank as veil as a $*iple. a indicates possible probable blank contestation

and warns the data user to tab appropriate action.S spiked coipounds

002286

5 6 3 6 6

ample No:Caac No: *=r

SOUTHWEST RESEARCH INSTITUTE

OrganicB Analysis Data Sheet(Page 4)

Tentatively Identified CompoundsI Estimated

Prac- Scan Concentrationtion Number ug/f

AS Compound NameNumber

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. , 1Detd tafacwJ 'Pr«partd — ,',-. "" . .

antes Anaiyai* Data(Pag« 3)

1* Or*) GPC C<t*nar

ee^Artaiywd —— :____ ———————————— Contir/ TS !_•* Lf*rtfV 'f^il PltP^rt^ (JifcTC^fr1

PfffCt'M M0'*'y'» <d«i?*nt^) «„.„!.„ ———— ——— P "-i. *? ^^"Otor /o ——— t* ——— ***

319-84-63 1 9 8 S - 7319-86-65 8 6 9 9?8-44.8309-00-21024-S7-3g$9-96-@80-57-172 55-972-20-833213-6S-972-54-81031-07-8SO- 29- 372-43-553494-705[57-74-98001-35 212674- 1 1 -21 1 104-21-21 1 1 4 1 - 1 6 -553469-21-912672-29-61 1097-69. 11 1096 62-5

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i •••-. fte.xtia^f t · ii ii ii ii ii i 5 = 35 6 33 to reference tocjeno()t 5636 contract...