Date Test No. Matrix Analytes Qty

01.09.09 02139F*φ Chicken Eggs # Coccidiostats 40g

01.09.09 0567F Minced Fish A number of compounds from List 1 50g

02.09.09 2766 Chocolate § Peanut, Peanut Protein 2 x 20g 03.09.09 1783 Spice Ochratoxin A 55g 08.09.09 1563F Lettuce Purée Nitrate 70g 08.09.09 2071F Meat Sulphur Dioxide 100g

09.09.09 1081 Sheep Feed Copper, Ash, Moisture, Total Oil & Protein 150g 10.09.09 1238 Food Simulant Phthlates 50mL 10.09.09 1353 Rum Alcoholic Strength, Ethanal (acetaldehyde), Methanol, Ethyl Acetate, Propan-1-

ol, 2-Methylpropanol, 2-Methylbutanol + 3-Methylbutanol (sum) & Ethyl Carbamate

200mL

11.09.09 1997 Orange Oil A number of compounds from List 5 25mL

14.09.09 1998F Peach Purée A number of compounds from List 3 100g

15.09.09 1486Fφ Mixed Fat Spread Cholesterol, Butyric Acid & Total Fat 50g

16.09.09 2259 Breakfast Cereal Deoxynivalenol (DON) 55g 17.09.09 388 Soft Drink Cyclamate, Sorbic Acid, Citric Acid, Saccharin, pH & Brix 150mL

18.09.09 7126 Cocoa Powder Cadmium & Lead (Both natural levels) 50g

21.09.09 2931F Fish Identification Three fish samples to be identified from the following list: Gadus morhua, (Linnaeus 1758)

Limanda limanda, (Linnaeus 1758) Melanogrammus aeglefinus, (Linnaeus 1758)

Merluccius merluccius, (Linnaeus 1758) Hippoglossus hippoglossus, (Linnaeus 1758)

Pleuronectes platessa, (Linnaeus 1758) Pollachius virens, (Linnaeus 1758)

Merlangius merlangus, (Linnaeus 1758)

10g of each fish

22.09.09 02140F* Honey # Aminoglycosides 20g

23.09.09 2767 Infant Cereal § Gluten 2 x 20g 23.09.09 4146 Milk Powder Aflatoxin M1 55g

25.09.09 164 Canned Meat Moisture, Ash, Total Fat, Nitrogen, Hydroxyproline 150g 28.09.09 1637F Apple Purée Patulin 60g 29.09.09 02141F* Honey # Macrolides 20g

29.09.09 04147F Almond Aflatoxins B & G &/or total 100g 30.09.09 642 Smoked Fish Pate PAHs 50g minimum 30.09.09 7127 Chilli Sugar Paste Lead 20g

06.10.09 2575F Chocolate Moisture, Total Fat, Butyric Acid & Total Sugars 150g 06.10.09 2161Fφ Fruit Juice Vitamin C 40mL

07.10.09 4148 Maize Aflatoxins B & G &/or total 55g 08.10.09 961 Wheat Flour A number of compounds from List 2 50g

13.10.09 02142F* Honey # Tetracyclines 20g

14.10.09 833 Orange Juice Brix, pH, Sucrose, Glucose, Fructose, Total Sugars & Citric Acid 250mL

20.10.09 7128 Canned Fish Arsenic (total), Cadmium, Mercury (total) & Cobalt(all natural levels) 150g

20.10.09 2072 Jam Sorbic Acid, Citric Acid, Benzoic Acid, pH & Brix 50g

21.10.09 1082 Pig Ration Ash, Crude Fibre, Moisture, Total Oil, Protein, Zinc & Vitamin E 150g 21.10.09 2768 Infant Cereal § Sesame, Sesame Protein 2 x 20g 22.10.09 1564 Meat Nitrate & Nitrite 25g 22.10.09 1485 Vegetable Oil Stigmastadienes 50mL

23.10.09 2436 Cereal Moisture at 130oC, Ash, Nitrogen & Total Dietary Fibre by AOAC 150g 27.10.09 02143F* Honey # Quinolones & Fluoroquinolones 40g

28.10.09 2260 Animal Feed Zearalenone (ZON) 55g 29.10.09 389 Cola Drink Caffeine, Total Sugars & Benzoic Acid 150mL

30.10.09 1784 Instant Coffee Ochratoxin A 55g

03.11.09 2162 Powdered Baby Food Vitamins A, B12, C & E 50g 04.11.09 2769 Cake Mix § Egg, Egg White Protein 2 x 20g 04.11.09 1487 Breakfast Cereal Total Fat, Saturates, Mono-unsaturates, Poly-unsaturates & Total Trans Fatty

Acids 50g

09.11.09 1999F Melon Purée A number of compounds from List 3 100g

09.11.09 19100F Citrus Juice A number of compounds from List 3 100g

11.11.09 1083 Poultry Ration Ash, Crude Fibre, Moisture, Total Oil & Protein 150g 11.11.09 1084 Poultry Ration Starch, Total Sugars, Calcium & Phosphorus 150g 12.11.09 1139 Plastic Film Overall Migration into Olive Oil by Total Immersion N/A 17.11.09 02144F*φ Bovine Liver # Avermectins 20g

17.11.09 2819F Honey Fructose, Glucose, Sucrose, Hydroxymethylfurfural (HMF) & Diastase 100g 18.11.09 4149 Spice Aflatoxins B & G &/or total 55g 19.11.09 1239 Food Simulant Total Primary Aromatic Amines >300mL 20.11.09 962 Rice A number of compounds from List 2 50g

23.11.09 2576F Butter Moisture, Non-Fat Solids, Total Fat, pH & Chloride 200g 24.11.09 04150F Dried Figs Aflatoxins B & G &/or total 100g 25.11.09 1354 Brandy Alcoholic Strength, Ethanal (acetaldehyde), Methanol, Ethyl Acetate, Propan-1-

ol, 2-Methylpropanol, 2-Methylbutanol + 3-Methylbutanol (sum) 200mL

26.11.09 165 Canned Meat Moisture, Ash, Total Fat, Nitrogen, Hydroxyproline 150g 27.11.09 1785 Wine Ochratoxin A 55mL

01.12.09 02145F*φ Pig Kidney # Sulfonamides 20g

02.12.09 4151 Rice Aflatoxins B & G &/or total 55g 04.12.09 2626 Soy Sauce 3-MCPD & 1,3 DCP 40g 08.12.09 7129 Seaweed Arsenic (inorganic), Arsenic (total) & Iodine 25g

08.12.09 7130 Soya Flour Aluminium, Arsenic (total), Cadmium, Lead & Mercury (total) (all high levels) 50g

09.12.09 2770* Cake Mix ▲Gluten, Milk and Egg screen 30g 09.12.09 568 Hydrogenated

Vegetable Oil A number of compounds from List 1 25g