traceability report soybean standard human … · 2018. 4. 13. · o gebana ge-02 • february 25th...

TRACEABILITY REPORT – SOYBEAN STANDARD HUMAN CONSUMPTION 追跡可能性報告書 - 人間消費用標準大豆

1

1. PRODUCT INFORMATION /産物情報

PRODUCT /産物

SOYBEAN / 大豆

ORIGIN /産地

PARANA ▪ BRAZIL / パラナ ▪ ブラジル

YEAR CROP /収穫年

2018

TYPE /種類

NON-GMO

ORGANIC? / 有機栽培

YES / はい ☐

NO / いいえ ☒

VARIETY /品種

GEBANA GE-02

SCREEN / ふるい

SIZE 4.5 MM / 網目... 4.5 MM ☐

SIZE 5.0 MM / 網目... 5.0 MM ☐

SIZE 5.5 MM / 網目... 5.5 MM ☒

SIZE 6.0 MM / 網目... 6.0 MM ☐

SIZE 6.5 MM / 網目... 6.5 MM ☐

LOT NUMBER / ロット番号

00120172018

PACKING / 梱包

VALVULATED PAPER BAG 30 KG / 弁付き 30 KG 入り紙袋 ☒

VALVULATED PAPER BAG 25 KG / 弁付き 25 KG 入り紙袋 ☐

STITCHED PAPER BAG 30 KG / 縫製 30 KG 入り紙袋 ☐

STITCHED PAPER BAG 25 KG / 縫製 25 KG 入り紙袋 ☐

NET WEIGHT / 正味重量

30 KG

SHELF LIFE / 有効期間

12/2019

2. GRAIN CHARACTERISTICS / 粒の特色

MOISTURE / 水分

9.84 %

OIL / 油

17.85 %

PROTEIN / たんぱく質

44.00 %

PROTEIN ON DRY BASE / 乾燥量基準のたんぱく質

48.80 %

PROTEIN 13% / たんぱく質 13％

42.46 %

PROTEIN SOLUBILITY (NSI) /タンパク質の溶解度(NSI)

90.2 %

SUCROSE / スクロース

2.00 %


2

SUCROSE ON DRY BASE /乾燥量基準のスクロース

2.22 %

100 SEEDS WEIGHT / 100 のタネの重量

14.2 G

LIPOXYGENASES / リポキシゲナーゼ

YES / はい ☒

NO / いいえ ☐

SIZE / サイズ

BIG / 大 ☐

MEDIUM TO BIG / 中〜大 ☐

MEDIUM / 中 ☒

SMALL TO MEDIUM / 小〜中 ☐

SMALL / 小 ☐

SKIN COLOR / 表皮色

WHITE / 白色 ☐

CLEAR YELLOW / 淡黄色 ☐

YELLOW / 黄色 ☐

CLEAR BROWN / 淡褐色 ☒

BROWN / 褐色 ☐

HILUM COLOR / 臍色

WHITE / 白色 ☐

CLEAR BROWN / 淡褐色 ☒

BROWN / 褐色 ☐

DARK BROWN / 濃褐色 ☐

BLACK / 黒色 ☐

3. COMPANY INFO / 会社概要

NAME / 会社名称 TRESBOMM AGRIBUSINESS / トレスボンン▪アグリブシネスス

BUSINESS NAME / 会社名

TRESBOMM COMERCIO E EXPORTACAO DE GRAOS LTDA

ADDRESS / 住所

RUA GETULIO VARGAS, N 959, SALA 09. CENTRO

PALOTINA – PARANA – BRAZIL - ZIP CODE 85.950-000

PHONE / 電話

+55 44 3649 1240 / +55 44 99988 9696

WEBSITE / ウェブサイト

WWW.TRESBOMM.COM.BR

EMAIL / Ｅ－メール

[email protected]

4. PRODUCTION INFO / 生産データ

FARM / 農場

FAZENDA TATURI (AGROPECUARIA MAREVA)

FARMER / 農業者

ILARIO EDGAR BOMM AND FAMILY


3

FARM LOCATION / 農場の位置

TERRA ROXA ▪ PARANA ▪ BRAZIL

ALTITUDE / 標高

300-600 M ☒

600-800 M ☐

800-1000 M ☐

> 1000 M ☐

FIELD(S) / 畑

▪ TALHAO 13

FIELD(S) COORDINATES / 畑の座標

▪ TALHAO 13

o GEBANA GE-02

• 24º 13’53.00”S / 54º 07’21.00”W

PREVIOUS CROP BY FIELD /畑ごとの以前の収穫

▪ TALHAO 13

o OAT

PLANTING DATES BY FIELD / 畑ごとの栽培時期

▪ TALHAO 13

o GEBANA GE-02

• OCTOBER 13TH 2017

PLANTING EQUIPMENTS BY FIELD / 畑ごとの栽培装置

▪ TALHAO 13

o GEBANA GE-02

• 1 X JOHN DEERE TRACTOR MODEL 6180J

• 1 X JOHN DEERE PLANTER 12 LINES

PLANTED AREA BY FIELD / 畑ごとの栽培エリア

▪ TALHAO 13

o GEBANA GE-02

• 15 HECTARES

SOYBEAN POPULATION BY FIELD /畑ごとの大豆の個数

▪ TALHAO 13

o GEBANA GE-02

• SPACE BETWEEN LINES: 50 CM

• SEEDS PER METER: 15.8

• DESIRED POPULATION: 316,000/HA

• FINAL POPULATION: 307,895/HA

USE OF FERTILIZERS /肥料の使用

PLEASE LOOK AT ITEM 5 FOLLOWING / アイテム 5 をご覧ください

SEED TREATMENT /種の処理


SPRAY OF CHEMICALS /化学薬品の散布


HARVESTING DATES / 収穫時期

▪ TALHAO 13

o GEBANA GE-02

• FEBRUARY 25TH 2018

HARVESTING EQUIPMENTS / 収穫装置

▪ TALHAO 13

o GEBANA GE-02

• 1 X JOHN DEERE HARVESTER S660


4

DID USE DRYER? / 乾燥機の使用

YES / はい ☐

NO / いいえ ☒

5. USE OF FERTILIZERS / 肥料の使用

6. SEED TREATMENT / 種の処理

7. SPRAY OF CHEMICALS / 化学薬品の散布

PRODUCT NAME BRAND ELEMENT TYPE QUANTITY/HA CONCENTRATION CONCENTRATION/HA

NITROGEN (N) 0.600 Ton 12.00 Kg/Ton 7.20 Kg/ha

PHOSPHORUS (P) 0.600 Ton 180.00 Kg/Ton 108.00 Kg/ha

POTASSIUM (K) 0.600 Ton 180.00 Kg/Ton 108.00 Kg/ha

USE OF FERTILIZERS

Date: October 13th 2017

2-18-18 HENRINGER SOLID

PRODUCT NAME BRAND ACTIVE INGREDIENT TYPE QUANTITY/KG CONCENTRATION CONCENTRATION/KG

FLUDIOXONIL 0.002 L/Kg of seeds 25 G/L 0.05 G/Kg of seeds

METALAXYL 0.002 L/Kg of seeds 37.5 G/L 0.08 G/Kg of seeds

FIPRONIL ALTA FIPRONIL SEED TREATMENT 0.002 L/Kg of seeds 200 G/L 0.40 G/Kg of seeds

APRON RFC SYNGENTA SEED TREATMENT

SEED TREATMENT

Date: October 13th 2017

PRODUCT NAME BRAND ACTIVE INGREDIENT TYPE QUANTITY/HA CONCENTRATION CONCENTRATION/HA

ZAPP QI 620 SYNGENTA GLYPHOSATE POTASSIUM HERBICIDE 1.250 L/Ha 100 G/L 125 G/Ha

IMAZETHAPYR 0.500 L/Ha 200 G/L 100 G/Ha

FLUMIOXAZIN 0.500 L/Ha 100 G/L 50 G/HaZETHAMAXX NUFARM HERBICIDE

1° SPRAY OF CHEMICALS

Date: October 12th 2017 - 1 Day Before Planting


BELT BAYER FLUBENDIAMIDE INSETICIDE 0.103 L/Ha 480 G/L 49 G/Ha

VENTURE ALTA HALOXYFOP-P-METHYL HERBICIDE 0.620 L/Ha 108 G/L 67 G/Ha


Date: November 13th 2017 - 31 Days After Planting


CLASSIC DUPONT CHLORIMURON-ETHYL HERBICIDE 0.019 L/Ha 750 G/L 14 G/Ha

FLEX SYNGENTA FOMESAFEN HERBICIDE 1.000 L/Ha 250 G/L 250 G/Ha




FLEX SYNGENTA FOMESAFEN HERBICIDE 0.500 L/Ha 250 G/L 125 G/Ha

NOMOLT BASF TEFLUBENZURON INSETICIDE 0.400 L/Ha 150 G/KG 60 G/Ha




5

8. LIST OF CHEMICALS /化学薬品のリスト

▪ Acephate ▪ Acetamiprid ▪ Azoxystrobin ▪ Bifenthrin ▪ Chlorimuron-Ethyl ▪ Cyhalothrin ▪ Cyproconazole ▪ Fipronil ▪ Flubendiamide

▪ Fludioxonil

▪ Flumioxazin ▪ Fomesafen ▪ Glyphosate

▪ Haloxyfop

▪ Imazethapyr Ammonium ▪ Metalaxyl ▪ Picoxystrobin ▪ Teflubenzuron


EVOS ALTA AZOXYSTROBIN FUNGICIDE 0.290 L/Ha 150 G/L 44 G/Ha

PERITO UPL ACEPHATE INSETICIDE 0.750 G/Ha 970 G/KG 728 G/Ha


Date: December 11th 2017 - 59 Days After Planting


EVOS ALTA AZOXYSTROBIN FUNGICIDE 0.290 L/Ha 150 G/L 44 G/Ha


KAISO UPL LAMBDA-CYHALOTHRIN INSETICIDE 0.080 G/Ha 250 G/L 20 G/Ha


Date: January 04th 2018 - 83 Days After Planting


PICOXYSTROBIN 0.200 L/Ha 200 G/L 40 G/Ha

CYPROCONAZOLE 0.200 L/Ha 80 G/L 16 G/Ha

NOMOLT BASF TEFLUBENZUROM INSETICIDE 0.103 L/Ha 150 G/KG 15 G/Ha


ACETAMIPRID 0.103 G/Ha 250 G/KG 26 G/Ha

BIFENTHRIN 0.103 G/Ha 250 G/KG 26 G/HaSPERTO UPL INSETICIDE



APPROACH DU PONT FUNGICIDE


PICOXYSTROBIN 0.330 L/Ha 200 G/L 66 G/Ha

CYPROCONAZOLE 0.330 L/Ha 80 G/L 26 G/Ha

BELT BAYER FLUBENDIAMIDE INSETICIDE 0.136 L/Ha 480 G/L 65 G/Ha


ACETAMIPRID 0.132 G/Ha 250 G/KG 33 G/Ha

BIFENTHRIN 0.132 G/Ha 250 G/KG 33 G/HaSPERTO UPL INSETICIDE



APPROACH DU PONT FUNGICIDE


6

9. PICTURES OF PLANTING / 栽培の写真


7

10. PICTURES OF CROP CONDITIONS / 作物の状態


8

11. PICTURES OF HARVESTING / 収穫の写真


9

12. HISTORY OF PRECIPITATION (mm)/ 降水量データ(mm)

13. HISTORY OF AIR HUMIDITY (%) / 湿度データ(%)

14. HISTORY OF AIR TEMPERATURE (Cº) / 気温データ(Cº)


10

15. HISTORY OF SUN RADIATION (Watts/m²) /日射遮蔽データ(W/m²)

16. HISTORY OF WIND SPEED (Km/h) / 風速データ(Km/h)

I on behalf of TRESBOMM COMERCIO E EXPORTACAO DE GRAOS LTDA hereby declare that all the information contained in

this traceability report is true of my best knowledge and represents the exact conditions of how this crop was

conducted from planting to harvest.


Marco Aurélio Riedi Bomm

International Trade Director


FARM LOCATION IN BRAZIL / ブラジルの農場の位置


FARM LOCATION IN PARANA / パラナの農場の位置


THE FARM / 農場


PLANTING DATE IN THE FIELD “TALHAO 13” / 栽培時期


SOYBEAN VARIETIES IN THE FIELD “TALHAO 13” / 大豆の品種


PLANTING SPEED (KM/H) IN THE FIELD “TALHAO 13” / 栽培速度 (KM／H)


FINAL POPULATION (1,000 PLANTS/HA) IN THE FIELD “TALHAO 13” / 合計個数（1000 の植物／HA）


HARVESTING DATE IN THE FIELD “TALHAO 13” / 収穫時期


HARVESTING SPEED (KM/H) IN THE FIELD “TALHAO 13” / 収穫速度(KM/H)


SOYBEAN MOISTURE WHEN HARVESTING THE FIELD “TALHAO 13” / 収穫時の大豆の水分


YIELD (60 KG/HA) OF FIELD “TALHAO 13” / 畑の収量 (60 KG/HA)

20/03/2018

691-2018-00039643Sample code Nr.

Analytical Report Nr. DateAR-18-GB-035902-01Page 1/2


Í%Rm;ÂÂC7eVÎ

Marco Aurélio Riedi [email protected]

R GETULIO VARGAS 959, CENTRO

BRASIL

85.950-000 PALOTINA

Soja em grãos

GE-02, LOT 00120172018, CROP 2018

Sample described as:

Grains in a plastic packingConditioning:

Your purchase order reference: 001/201813/03/2018Your purchase order date:

Sample reception date: 16/03/2018 23:06:05

Analysis starting date: Analysis ending date:20/03/2018 20/03/2018

GMO Matrix Soya beans Amount 2727g

Molecular biology Results

GBA75 GB 35S Promoter Quantification (Soy) Method: POP-BM001/5, Real-time PCRResult of Quantification 35S Promoter / Soy <0,1* % Standard deviation -- % pLOQ: practical limit of quantification 0,1 %

GBA86 GB AgroBorderII Quantification (Soy) Method: POP-BM001/5, Real-time PCRquantitative <0,1* % Standard deviation -- % pLOQ: practical limit of quantification 0,1 %

Comments and Conclusions:

Análises OGM: Os seguintes resultados foram obtidos através da detecção qualitativa (presença/ausência) e/ou percentual (análise

quantitativa) de seqüências de DNA características de Organismos Geneticamente Modificados (OGMs) utilizando a técnica da Reação da

Polimerase em Cadeia (PCR ou PCR em Tempo Real). O resultado percentual representa a relação entre o número de genomas modificados

em relação ao número total de genomas da espécie. LOD: Limite de detecção do método é de 0,01% determinado com material proveniente de

DNA de farinha pura e não processada. LOQ: Limite de Quantificação específica para cada amostra.

GBA75: The test performed determines the number of copies of DNA sequence characteristic of the 35S Promoter, which is present in the

genetic constructs of the following events approved in Brazil: A2704-12, A5547-127, GTS-40-3-2, among other events of soybean. The

percentage calculation is determined by the ratio of the number of copies of the 35S Promoter to the copy number of a specific soybean DNA

sequence determined by quantifying Gene Lectin

GBA86: The test performed determines the number of DNA sequence copies characteristic of the genetically modified events of the MON family.

The percentage calculation is determined by the ratio of the number of copies of Agroborder II to the number of copies of a soybean specific

DNA sequence determined by quantification of Gene Lectin.

Signed eletronically according to the "Medida Provisória 2.200-2" of 24/8/2001visit http://www.eurofins.com.br/assinaturadigital to download a verification key

SIGNATURE

José Belarmino Da Silva Neto and/or Lia Mara Palermi Do Prado De Carvalho and/or Gustavo Salerno

Business Unit Manager Technical Manager - Biology Technical Manager - Chemistry

www.eurofins.com.br

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20/03/2018

691-2018-00039643Sample code Nr.


EXPLANATORY NOTE

* = Below Limit of Quantification

This document can only be reproduced in full ; it only concerns the submitted sample.

Results have been obtained and reported in accordance with our general sales conditions available on request.The tests identified by the two letters code GB are performed in laboratory Eurofins do Brasil Análises de Alimentos.

Only the signed hard copy or its duplicate is authentic

Technical contact for your orders: [email protected]

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10/04/2018

691-2018-00038555Sample code Nr.



Í%Rm;ÂÂDFwBÎ

Marco Aurélio Riedi [email protected]

R GETULIO VARGAS 959, CENTRO

BRASIL

85.950-000 PALOTINA

Soja em grãos

GE-02, LOT 00120172018, CROP 2018

Sample described as:

Grains in a plastic packingConditioning:

Your purchase order reference: 001/201816/03/2018Your purchase order date:

Sample reception date: 16/03/2018 09:45:21

Analysis starting date: Analysis ending date:20/03/2018 04/04/2018

Amount 2727g

Results

SF8UN SF Chlorimuron-Ethyl Method: LA-LCMS-007, LFGB L 00.00-113Chlorimuron-Ethyl <0.01* mg/kg

SF8UL SF Flubendiamide Method: LA-LCMS-007, LFGB L 00.00-113Flubendiamide <0.01* mg/kg

SF8T4 SF Fomesafen Method: LA-LCMS-007, LFGB L 00.00-113Fomesafen <0.01* mg/kg

SF00B SF Glyphosate, Glufosinate, AMPA in food Method: In-House method, LC-MS/MSAminomethylphosphonic acid (AMPA) <0.01* mg/kg Glufosinate <0.01* mg/kg Glyphosate <0.01* mg/kg

ZVP04 ZV Quantitative screening GC-MS TQ Method: CEN/TR 16468, mod.Screened pesticides Not Detected mg/kg

ZVP05 ZV Quantitative screening LC-MS Method: CEN/TR 15641, mod.Screened pesticides Not Detected mg/kg

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691-2018-00038555Sample code Nr.


List of screened molecules (LOQ = limit of quantification)Quantitative screening GC-MS TQ (LOQ mg/kg)ZVP04 ZV

1,4-dimethylnaphthalene 0.01 1-Naphthol 0.01 2,4,6-Trichlorophenol (2) 0.01 2,4-DDD 0.01 2,6-Dichlorobenzamide 0.01

2-Phenylphenol 0.01 3,4-dichloroaniline 0.02 4,4 -DDD + 2,4 -DDT 0.01 4,4 -DDT 0.01 4,4-DDE 0.01

Acibenzolar-s-methyl 0.01 Aclonifen 0.01 Acrinathrin 0.01 Alachlor 0.01 Aldrin 0.01

Allethrin 0.02 Ametryn 0.01 Aminocarb 0.01 Amitraz 0.02 Amitraz (sum) 0.02

Anthraquinone 0.01 Azinphos-ethyl 0.01 Azoxystrobine 0.02 Barban/Chlorbufam/Chlorpropham (as 3-Chloroaniline0.05 Benalaxyl 0.01

Bendiocarb 0.01 Benfluralin 0.01 Benfuracarb 0.01 Bifenazate 0.05 Bifenox 0.01

Bifenthrin 0.01 Biphenyl 0.01 Bitertanol 0.01 Bromacil 0.01 Bromocyclen 0.01

Bromophos-ethyl 0.01 Bromophos-methyl 0.01 Bromopropylate 0.01 Bromuconazole 0.02 Bupirimate 0.01

Buprofezin 0.01 Butralin 0.01 Cadusaphos 0.01 Captafol 0.05 Captan 0.01

Captan/THPI (Sum calculated as Captan)0.01 Carbaryl 0.01 Carbofuran 0.01 Carbofuran (Sum) 0.01 Carbofuranphenol 0.01

Carbophenothion 0.01 Carbophenothion-methyl 0.01 Chinomethionate 0.01 Chlorbufam 0.01 Chlordane (total) 0.02

Chlordane, cis- 0.01 Chlordane, oxy- 0.01 Chlordane, trans- 0.01 Chlorfenapyr 0.01 Chlorfenson 0.01

Chlorfenvinphos 0.01 Chlorfenvinphos cis 0.01 Chlorfenvinphos trans 0.01 Chloridazone 0.05 Chlorobenzilate 0.01

Chloroneb 0.01 Chlorothalonil 0.01 Chlorpropham 0.01 Chlorpropham (Sum) 0.01 Chlorpyrifos (-ethyl) 0.01

Chlorpyrifos-methyl 0.01 Chlorthal-dimethyl 0.01 Chlorthiamid 0.2 Chlozolinate 0.01 Clefoxydim 0.05

Clodinafop 0.01 Clomazone 0.01 Cloquintocet-mexyl 0.01 Coumaphos 0.01 Cyanazine 0.01

Cyanofenphos 0.01 Cyanophos 0.01 Cycloate 0.01 Cyfluthrin 0.01 Cyhalothrin 0.01

Cyhalothrin, lambda- 0.01 Cypermethrin 0.01 Cyphenothrin 0.05 Cyproconazole 0.01 Cyprodinil 0.01

DDT (total) 0.01 Deltamethrin 0.01 Demeton-O 0.01 Demeton-S 0.01 Demeton-S-methyl 0.01

Desmetryn 0.01 Diazinon 0.01 Dichlobenil 0.02 Dichlofenthion 0.01 Dichloranilin-3,5 0.02

Dichlorobenzophenone, p,p-0.01 Dicloran 0.01 Dicofol, p,p- 0.01 Dieldrin 0.01 Dieldrin (Sum) 0.01

Diethofencarb 0.01 Difenoconazole 0.01 Diflufenican 0.01 Dimethoate 0.01 Dimethoate/Omethoate (sum)0.01

Dimethylaminosulphotoluidide (DMST)0.02 Diniconazole 0.01 Diphenamid 0.01 Diphenylamine 0.01 Disulfoton 0.02

Disulfoton (sum) 0.02 Disulfoton-sulfon 0.01 Disulfoton-sulfoxide 0.01 Ditalimfos 0.01 Endosulfan (total) 0.01

Endosulfan sulphate 0.02 Endosulfan, alpha- 0.01 Endosulfan, beta- 0.01 Endrin 0.01 EPN 0.01

Epoxiconazole 0.01 EPTC 0.01 Etaconazole 0.01 Ethion 0.01 Ethofumesate 0.01

Ethoprophos 0.01 Ethoxyquin 0.01 Etofenprox 0.01 Etridiazole 0.02 Etrimfos 0.01

Famoxadone 0.05 Fenarimol 0.01 Fenazaquin 0.01 Fenfluthrin 0.01 Fenitrothion 0.01

Fenobucarb 0.01 Fenothrine 0.01 Fenoxycarb 0.05 Fenpiclonil 0.01 Fenpropidin 0.01

Fenpropimorph 0.01 Fenpyroximate 0.02 Fenson 0.01 Fensulfothion 0.01 Fenthion 0.01

Fenthion (sum) 0.01 Fenthion-sulfoxide 0.01 Fenvalerate & Esfenvalerate0.01 Fipronil 0.005 Fipronil (sum) 0.005

Fipronil-sulfone 0.005 Fluazifop-butyl 0.01 Fluchloralin 0.01 Flucythrinate 0.01 Fludioxonil 0.01

Fluquinconazole 0.01 Flurprimidol 0.01 Flusilazole 0.01 Flutolanil 0.01 Folpet 0.01

Folpet/PI (Sum calculated as Folpet)0.01 Fonofos 0.01 Formothion 0.01 Fuberidazole 0.01 Furalaxyl 0.01

Halfenprox 0.01 Haloxyfop-2-ethoxyethyl 0.01 HCH (sum) 0.02 HCH, alpha- 0.01 HCH, beta- 0.01

HCH, delta- 0.01 Heptachlor 0.01 Heptachlor (sum) 0.01 Heptachlor epoxide, cis- 0.01 Heptachlor epoxide, trans-0.02

Heptenophos 0.01 Hexachlorobenzene (HCB)0.01 Hexachlorobutadiene 0.01 Hexaconazole 0.01 Hexazinone 0.01

Imazethapyr 0.05 Iodofenphos 0.01 Iprobenfos 0.01 Iprodione 0.01 Isazophos 0.01

Isocarbofos 0.01 Isodrin 0.01 Isofenphos 0.01 Isofenphos-methyl 0.01 Isofenphos-oxon 0.01

Isoprocarb 0.01 Isoproturon 0.01 Isoxadifen-ethyl 0.01 Kresoxim-methyl 0.01 Lenacil 0.01

Leptophos 0.01 Lindane (gamma-HCH) 0.01 Malaoxon 0.01 Malathion, fyfanon 0.01 Malathion/Malaoxon (sum)0.02

Mecarbam 0.01 Mepanipyrim 0.01 Mephosfolan 0.02 Mepronil 0.01 Metalaxyl 0.01

Metazachlor 0.01 Methabenzthiazuron 0.01 Methacriphos 0.01 Methidathion 0.01 Methiocarb 0.01

Methiocarb (sum) 0.02 Methoprotryne 0.01 Methoxychlor 0.01 Methyl Parathion 0.01 Metobromuron 0.01

Metolcarb 0.01 Metrafenone 0.01 Metribuzin 0.01 Mevinphos 0.01 Mirex 0.02

Molinate 0.01 Myclobutanil 0.01 Naphthalene Acetamide 0.05 Napropamide 0.01 Nitrapyrin 0.01

Nitrofen 0.01 Nitrothal-isopropyl 0.01 Norflurazon 0.01 o,p'-DDE 0.01 Ofurace 0.01

Oxadiazon 0.01 Oxadixyl 0.02 Oxydemeton-methyl (sum)0.01 Oxyfluorfen 0.01 Paraoxon 0.01

Paraoxon-methyl 0.01 Parathion 0.01 Parathion-methyl (Sum) 0.01 Penconazole 0.01 Pencycuron 0.02

Pendimethalin 0.01 Pentachloranisole 0.01 Pentachloroaniline 0.01 Pentachlorobenzene 0.01 Pentachlorophenol 0.05

Permethrin-cis 0.01 Permethrins (sum) 0.02 Permethrin-trans 0.01 Perthane 0.01 Phenkapton 0.01

Phenothrin 0.02 Phenthoate 0.01 Phosalone 0.01 Phosfolan 0.02 Phosmet 0.01

Phosmet (Sum) 0.02 Phthalimid (PI) 0.01 Picoxystrobin 0.01 Piperonyl butoxide (PBO) 0.01 Pirimicarb 0.01

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Quantitative screening GC-MS TQ (LOQ mg/kg)ZVP04 ZV

Pirimicarb, desmethyl- 0.01 Pirimicarb, desmethyl-formamido-0.01 Pirimiphos-ethyl 0.01 Pirimiphos-methyl 0.01 Procymidone 0.01

Profenofos 0.01 Profluralin 0.01 Promecarb 0.01 Prometryn 0.01 Pronamide 0.01

Propachlor 0.01 Propanil 0.01 Propargite 0.02 Propazine 0.01 Propetamphos 0.01

Propham 0.01 Propiconazole 0.01 Propoxur 0.01 Propoxycarbazone 0.05 Prosulfocarb 0.01

Prothioconazole 0.01 Prothioconazole-desthio 0.01 Prothiofos 0.01 Pyraflufen-ethyl 0.01 Pyrazophos 0.01

Pyridaben 0.01 Pyridaphenthion 0.01 Pyrifenox 0.01 Pyrifenox (E-) 0.01 Pyrifenox (Z-) 0.01

Pyrimethanil 0.01 Pyriproxyfen 0.01 Quinalphos 0.01 Quinoxyfen 0.01 Quintozene 0.01

Quintozene (sum) 0.01 Quizalofop ethyl 0.01 Ronnel 0.01 S 421 0.05 Screened pesticides

Silthiofam 0.01 Simazine 0.01 S-Metolachlor 0.01 Spiromesifen 0.01 Spiroxamine 0.01

Sulfotep (2) 0.01 Sulphur (S) 0.2 Sulprofos 0.01 tau-Fluvalinate 0.01 Tebuconazole 0.01

Tebufenpyrad 0.01 Tecnazene 0.01 Tefluthrin 0.01 Telodrin 0.01 Terbacil 0.01

Terbumeton 0.01 Terbuthylazine 0.01 Terbuthylazine-Desethyl-2-hydroxy0.01 Terbutryn 0.01 Tetrachlorvinphos 0.01

Tetraconazole 0.01 Tetradifon 0.01 Tetrahydrophthalimide (THPI)0.01 Tetramethrin 0.01 Tetrasul 0.01

Tolclofos-methyl 0.01 Tolylfluanid (Sum) 0.02 Transfluthrin 0.01 Triadimefon 0.01 Triadimenol 0.01

Triadimenol/Triadimefon (sum)0.02 Triallate 0.01 Triazamate 0.01 Triazophos 0.01 Trichloronat 0.01

Trifloxystrobin 0.01 Triflumizole 0.01 Trifluralin 0.01 Trinexapac-ethyl 0.01 Vinclozolin 0.01

Quantitative screening LC-MS (LOQ mg/kg)ZVP05 ZV

1,2,4-triazole 0.1 1-Naphthylacetic acid 0.05 2,4,5-T 0.01 2,4,6-Trichlorophenoxyacetic Acid0.01 2,4-D 0.01

2,4-D butyric acid (2,4-DB)0.01 2-Naphthyloxyacetic acid 0.01 3-Hydroxycarbofuran 0.01 3-ketocarbofuran 0.01 4-CPA 0.01

6-Benzyladenine 0.01 6-Chlor-3-phenylpyridazin-4-ol0.01 Abamectin 0.01 Acephate 0.01 Acequinocyl 0.01

Acetamiprid 0.01 Alanycarb 0.01 Aldicarb 0.01 Aldicarb (sum) 0.01 Aldicarb-sulfone 0.01

Aldicarb-sulfoxide 0.01 Ametoctradin 0.01 Aminopyralid 0.25 Amisulbrom 0.01 Amitraz 0.01

Amitraz (as 2,4-Dimethylaniline)0.05 Amitraz (sum) 0.01 Amitraz DMF 0.01 Amitraz DMPF 0.01 Amitrole 0.5

Anilazine 0.05 Asulam 0.01 Atrazine 0.01 Avermectin B1a 0.01 Avermectin B1b 0.01

Azaconazole 0.01 Azadirachtin 0.01 Azamethiphos 0.01 Azimsulfuron 0.01 Azinphos-methyl 0.01

Azoxystrobine 0.01 Barban 0.01 Beflubutamid 0.01 Benoxacor 0.01 Bentazone 0.01

Benthiavalicarb, isopropyl-0.01 Benzovindiflupyr 0.01 Bitertanol 0.01 Bixafen 0.01 Boscalid 0.01

Bromoxynil 0.01 Bromuconazole 0.01 Bupirimate 0.01 Buprofezin 0.01 Butafenacil 0.01

Butocarboxim 0.02 Butocarboxim-sulfoxide 0.01 Butoxycarboxim 0.01 Buturon 0.01 Caffeine 0.05

Carbaryl 0.01 Carbendazim 0.01 Carbendazim/Benomyl (sum)0.01 Carbetamide 0.01 Carbofuran 0.001

Carbofuran (Sum) 0.001 Carbosulfan 0.01 Carboxin 0.01 Carfentrazone 0.01 Carpropamid 0.01

Chloorthiofos 0.01 Chloramben 0.1 Chlorantraniliprole 0.01 Chlorbromuron 0.01 Chlordecon 0.01

Chlordimeform 0.01 Chlorfluazuron 0.01 Chlorothalonil-4-hydroxy 0.01 Chlorotoluron 0.01 Chlorthiofos-sulfone 0.01

Chlorthion 0.01 Cinerin I 0.01 Clethodim 0.01 Clethodim/Sethoxydim (Sum)0.01 Climbazole 0.01

Clofentezine 0.01 Clopyralid 0.5 Clothianidin 0.01 Crimidine 0.01 Cyantraniliprole 0.01

Cyazofamid 0.01 Cyclanilide 0.01 Cycloxydim 0.01 Cyflufenamid 0.01 Cyflumetofen 0.01

Cymoxanil 0.01 Cyproconazole 0.01 Cyprodinil 0.01 Cyromazine 0.02 Cythioate 0.01

Daminozide 0.01 DEET (Diethyltoluamide) 0.01 Demeton-S-methyl sulfoxide (= oxydemeton-methyl)0.01 Demeton-S-methyl-sulfone0.01 Desmedipham 0.01

Diafenthiuron 0.01 Dicamba 0.05 Dichlofluanid 0.01 Dichlorophen 0.01 Dichlorprop P 0.01

Dichlorvos 0.01 Diclobutrazol 0.01 Dicrotophos 0.01 Diethofencarb 0.01 Difenoconazole 0.01

Diflubenzuron 0.01 Dimethenamid 0.01 Dimethirimol 0.01 Dimethoate 0.01 Dimethoate/Omethoate (sum)0.01

Dimethomorph 0.01 Dimethylaminosulphotoluidide (DMST)0.01 Dimethylphenylsulfamide (DMSA)0.01 Dimoxystrobin 0.01 Diniconazole 0.01

Dinocap 0.01 Dinotefuran 0.01 Dipropetryn 0.01 Dithianon 0.01 Diuron 0.01

Dodemorf 0.01 Dodine 0.01 Emamectin, benzoate- 0.01 Epoxiconazole 0.01 Ethiofencarb 0.01

Ethiofencarb-sulfone 0.01 Ethiofencarb-sulfoxide 0.01 Ethiprole 0.01 Ethirimol 0.01 Ethoxysulfuron 0.01

Ethylene thiourea (ETU) 0.5 Etofenprox 0.01 Etoxazole 0.01 Famophos 0.01 Famoxadone 0.01

Fenamidone 0.01 Fenamiphos (sum) 0.01 Fenamiphos-sulfone 0.01 Fenamiphos-sulfoxide 0.01 Fenarimol 0.02

Fenazaquin 0.01 Fenbuconazole 0.01 Fenbutatin oxide 0.01 Fenhexamid 0.01 Fenoprop 0.01

Fenoxycarb 0.01 Fenpropidin 0.01 Fenpropimorph 0.01 Fenpyrazamine 0.01 Fenpyroximate 0.01

Fenthion 0.01 Fenthion (sum) 0.01 Fenthion-oxon 0.01 Fenthion-oxon-sulfone 0.01 Fenthion-oxon-sulfoxide 0.01

Fenthion-sulfone 0.01 Fenthion-sulfoxide 0.01 Fipronil 0.01 Fipronil (sum) 0.01 Fipronil-sulfone 0.01

Flazasulfuron 0.01 Flonicamid 0.01 Flonicamid (Sum) 0.01 Florasulam 0.01 Fluazifop 0.01

Fluazifop-P-butyl 0.01 Fluazinam 0.01 Flubendiamide 0.01 Flucycloxuron 0.01 Flufenacet 0.01

Flufenoxuron 0.01 Flumioxazin 0.01 Fluopicolid 0.01 Fluopyram 0.01 Fluotrimazole 0.01

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Quantitative screening LC-MS (LOQ mg/kg)ZVP05 ZV

Fluoxastrobin 0.01 Flupyradifurone 0.01 Fluquinconazole 0.01 Flurochloridone 0.01 Fluroxypyr 0.02

Fluroxypyr (Sum) 0.01 Fluroxypyr-Methylheptyl 0.01 Flusilazole 0.01 Fluthiacet-methyl 0.01 Flutolanil 0.01

Flutriafol 0.01 Fluxapyroxad 0.01 Forchlorfenuron 0.01 Formetanate 0.01 Fosetyl-aluminium 0.5

Fosthiazate 0.01 Furalaxyl 0.01 Furathiocarb 0.01 Furmecyclox 0.02 Halofenozide 0.01

Haloxyfop 0.01 Hexaconazole 0.01 Hexaflumuron 0.01 Hexythiazox 0.01 Hymexazol 0.1

Imazalil 0.01 Imazamox 0.01 Imazaquin 0.01 Imibenconazole 0.01 Imidacloprid 0.01

Indoxacarb 0.01 Iodosulfuron methyl 0.01 Ioxynil 0.01 Iprovalicarb 0.01 Isocarbofos 0.01

Isoprothiolane 0.01 Isopyrazam 0.01 Isouron 0.01 Isoxaben 0.01 Isoxaflutole 0.01

Isoxathion 0.01 Jasmolin I 0.01 Kresoxim-methyl 0.01 Lenacil 0.01 Linuron 0.01

Lufenuron 0.01 Malathion (Sum) 0.01 Malathion, fyfanon 0.01 Maleic hydrazide (MH-30)0.5 Mandipropamid 0.05

MCPA 0.01 MCPA/MCPB (sum) 0.01 MCPB 0.01 Mecoprop 0.01 Mefenacet 0.01

Mefenpyr-diethyl 0.01 Mepanipyrim 0.01 Mephosfolan 0.01 Mepronil 0.01 Meptyldinocap 0.01

Mesosulfuron-methyl 0.01 Mesotrione 0.02 Metaflumizone 0.01 Metalaxyl 0.01 Metaldehyde 0.01

Metamitron 0.01 Metconazole 0.02 Methamidophos 0.01 Methidathion 0.01 Methiocarb 0.01

Methiocarb (sum) 0.01 Methiocarb-sulfone 0.01 Methiocarb-sulfoxide 0.01 Methomyl 0.01 Methomyl/Thiodicarb (sum)0.01

Methoxyfenozide 0.01 Metobromuron 0.01 Metosulam 0.01 Metoxuron 0.01 Metsulfuron-methyl 0.02

Milbemectin (sum) 0.1 Milbemectin A3 0.1 Milbemectin A4 0.1 Monocrotophos 0.01 Monolinuron 0.01

Monuron 0.01 Myclobutanil 0.01 Naled 0.01 Neburon 0.01 Nicosulfuron 0.01

Nitenpyram 0.01 Nitralin 0.01 Novaluron 0.01 Nuarimol 0.01 Omethoate 0.01

Oxadixyl 0.01 Oxamyl 0.01 Oxasulfuron 0.01 Oxycarboxin 0.01 Oxydemeton-methyl (sum)0.01

Paclobutrazol 0.01 Paraoxon-ethyl 0.01 Paraoxon-methyl 0.01 Parathion-methyl (Sum) 0.01 Pebulate 0.01

Penconazole 0.01 Pencycuron 0.01 Penflufen 0.01 Penthiopyrad 0.01 Phenamiphos 0.01

Phenisopham 0.01 Phenmedipham 0.01 Phorate 0.01 Phorate (sum) 0.01 Phorate-sulfone 0.01

Phorate-sulfoxide 0.01 Phosalone 0.01 Phosmet 0.01 Phosmet (Sum) 0.01 Phosmet-oxon 0.01

Phosphamidon 0.01 Phoxim 0.01 Picaridin 0.01 Picloram 0.1 Picolinafen 0.01

Picoxystrobin 0.01 Pinoxaden 0.01 Piperonyl butoxide (PBO) 0.01 Pirimicarb 0.01 Pirimicarb, desmethyl- 0.01

Prochloraz 0.01 Prochloraz (Sum) 0.01 Prochloraz-desimidazole-amino0.01 Prochloraz-desimidazole-formylamino0.01 Profenofos 0.01

Prohexadione Calcium 0.05 Propamocarb Hydrochloride0.01 Propaquizafop 0.01 Propiconazole 0.01 Propoxur 0.01

Propyzamide 0.01 Proquinazid 0.01 Prosulfocarb 0.01 Prosulfuron 0.01 Prothiocarb 0.01

Prothiocarb hydrochloride 0.01 Prothioconazole 0.01 Prothioconazole-desthio 0.01 Pymetrozine 0.01 Pyracarbolid 0.01

Pyraclofos 0.01 Pyraclostrobin 0.01 Pyrazophos 0.01 Pyrethrins 0.01 Pyrethrins (Total Isomers) 0.01

Pyridaben 0.01 Pyridalyl 0.01 Pyridaphenthion 0.01 Pyridate 0.01 Pyridate (Sum) 0.01

Pyrifenox 0.01 Pyrimethanil 0.01 Pyrimidifen 0.01 Pyriproxyfen 0.01 Pyroxsulam 0.01

Quinclorac 0.01 Quinmerac 0.05 Quizalofop 0.01 Rimsulfuron 0.01 Rotenone 0.01

Saflufenacil 0.01 Screened pesticides Sethoxydim 0.01 Silafluofen 0.01 Simazine 0.01

Spinetoram 0.01 Spinosad (Sum) 0.01 Spinosad A 0.01 Spinosad D 0.01 Spirodiclofen 0.01

Spirotetramat 0.01 Spirotetramate (Sum) 0.01 Spirotetramat-enol 0.01 Spirotetramat-enolglucoside0.05 Spirotetramat-ketohydroxy0.01

Spirotetramat-monohydroxy0.01 Spiroxamine 0.01 Sulcotrione 0.02 Sulfentrazone 0.02 Sulfoxaflor 0.01

Tebuconazole 0.01 Tebufenozide 0.01 Tebufenpyrad 0.01 Teflubenzuron 0.01 Tembotrione 0.01

Tepraloxydim 0.01 Terbufos 0.01 Terbufos-sulfone 0.01 Terbufos-sulfoxide 0.01 Tetraconazole 0.01

TFNA 0.01 TFNA-AM 0.01 TFNG 0.01 Thiabendazole 0.01 Thiacloprid 0.01

Thiamethoxam 0.01 Thidiazuron 0.01 Thiencarbazone-methyl 0.01 Thiobencarb 0.01 Thiocyclam 0.05

Thiodicarb 0.01 Thiofanox 0.01 Thiofanox-sulfone 0.01 Thiofanox-sulfoxide 0.01 Thiometon 0.01

Thiophanate-methyl 0.01 Thiram 0.01 Tolclofos-methyl 0.01 Tolfenpyrad 0.01 Tolylfluanid 0.01

Tolylfluanid (Sum) 0.01 Tralkoxydim 0.01 Triadimefon 0.01 Triadimenol 0.01 Triadimenol/Triadimefon (sum)0.01

Triapenthenol 0.01 Triazophos 0.01 Triazoxide 0.01 Tribenuron-methyl 0.01 Trichlorfon 0.01

Triclopyr 0.01 Tricyclazole 0.01 Tridemorph 0.01 Trifloxystrobin 0.01 Triflumizole 0.01

Triflumuron 0.01 Triflusulfuron-methyl 0.01 Triforine 0.01 Trimethycarb, 3,4,5- 0.01 Trinexapac-ethyl 0.01

Triticonazole 0.01 TRITOSULFURON 0.01 Uniconazole 0.01 Valifenalate 0.01 Vamidothion 0.01

Warfarin 0.01 Zoxamide 0.01

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Signed eletronically according to the "Medida Provisória 2.200-2" of 24/8/2001visit http://www.eurofins.com.br/assinaturadigital to download a verification key

SIGNATURE

José Belarmino Da Silva Neto and/or Lia Mara Palermi Do Prado De Carvalho and/or Gustavo Salerno

Business Unit Manager Technical Manager - Biology Technical Manager - Chemistry

EXPLANATORY NOTE

* = Below Limit of Quantification

This document can only be reproduced in full ; it only concerns the submitted sample.

Results have been obtained and reported in accordance with our general sales conditions available on request.

The tests identified by the two letters code SF are performed in laboratory SOFIA (Berlin).

The tests identified by the two letters code ZV are performed in laboratory Eurofins Lab Zeeuws-Vlaanderen.Only the signed hard copy or its duplicate is authentic

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