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B CNG THNG
TRNG HCN TP.H CH MINH
CNG HA X HI CH NGHA VIT NAM
c lp T do Hnh phc
__________________
NHIM V N HC PHN
KHOA: CNG NGH HO HC
B MN: MY & THIT B
H V TN: V TRNG QUN MSSV:11254511 LP: DHHD7
1. Tn n:
Thit k thp mm chp chng luyn tch hn hp Etanol Nc
2. Nhim v n (yu cu v ni dung v s liu ban u)
2.1 S liu ban u: Lu lng hn hp u vo thp (kg/h): F = 1800 kg/h
Nng hn hp u (phn khi lng): = 33,5%
Nng sn phm nh (phn khi lng): = 90%
Nng sn phm y (phn khi lng): = 3 %
2.2 Yu cu v ni dung:
Quy trnh cng ngh
Cn bng vt cht v cn bng nng lng
Tnh ton thit b chnh v thit b ph
Tnh c kh
Bng v: quy trnh cng ngh v thit b chnh (A1)
3. Ngy giao nhim v n: ........................................................24/05/2014
4. Ngy hon thnh nhim v: .......................................................10/07/2014
5. H v tn ngi hng dn: Cao Thanh Nhn
Tp.H Ch Minh, ngy 24 thng 05 nm 2014
T TRNG B MN GIO VIN HNG DN (K v ghi r h tn) (K v ghi r h tn)
Trn Hoi c Cao Thanh Nhn
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC
LI M U
Cng ngh ha hc l mt trong nhng ngnh ng gp rt ln trong s pht
trin ca nn cng nghip nc ta. Trong ngnh sn xut ha cht cng nh s
dng sn phm ha hc, nhu cu s dng nguyn liu c tinh khit cao phi ph
hp vi qui trnh sn xut hoc nhu cu s dng.
Ngy nay, cc phng php c s dng nng cao tinh khit l: chng
ct, trch ly, c c, hp thu Ty theo c tnh sn phm m ta la chn phng
php thch hp. H Ethanol nc l 2 cu t tan ln hon ton, ta dng phng
php chng ct nng cao tinh khit cho Ethanol.
n mn hc Qu trnh v Thit b l mt mn hc mang tnh tng hp trong
qu trnh hc tp ca cc k s ho tng lai. Mn hc gip sinh vin gii quyt
nhim v tnh ton c th v: yu cu cng ngh, kt cu, gi thnh ca mt thit b
trong sn xut ho cht - thc phm. y l bc u tin sinh vin vn dng
nhng kin thc hc ca nhiu mn hc vo gii quyt nhng vn k thut
thc t mt cch tng hp.
Em chn thnh cm n Thy Cao Thanh Nhn v cc Qu Thy C b mn
My & Thit B gip em hon thnh n ny. Tuy nhin, trong qu trnh hon
thnh n vn khng trnh khi c sai st, em rt mong qu thy c gp , ch dn.
Em xin cm n Qu Thy C!
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC
NHN XT CA GIO VIN HNG DN
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Phn nh gi:
thc thc hin: ....................................................................................
Ni dung thc hin: ................................................................................
Hnh thc trnh by: ................................................................................
Tng hp kt qu: ..................................................................................
im bng s: ...................... im bng ch: ..................................
Tp. H Ch Minh, ngy ..... thng ..... nm 2014
Gio vin hng dn
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC
NHN XT CA GIO VIN PHN BIN
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Phn nh gi:
thc thc hin: ....................................................................................
Ni dung thc hin: ................................................................................
Hnh thc trnh by: ................................................................................
Tng hp kt qu: ..................................................................................
im bng s: ...................... im bng ch: ..................................
Tp. H Ch Minh, ngy ..... thng ..... nm 2014 Gio vin phn bin
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC
MC LC PHN 1: M U ....................................................................................... 1
I.L thuyt v chng luyn ........................................................................ 1
II.u, khuyt im ca phng php chng a chp: ............................ 2
III.Dy chuyn cng ngh: ........................ Error! Bookmark not defined.
PHN 2: TNH CNG NGH ...................................................................... 8
Chng 1: TNH S A .......................................................................... 9
1.1. Tnh lng hn hp: ....................................................................... 9
1.2 Xc nh s a ca thp ............................................................... 10
Chng 2: TNH NG KNH THIT B ............................................ 16
2.1. ng knh on luyn: ............................................................... 16
2.2. ng knh on chng: ............................................................. 20
Chng 3: CN BNG NHIT LNG ................................................ 24
3.1. Cn bng nhit lng ca thit b un nng hn hp u: .......... 24
3.2. Cn bng nhit lng ca thp chng luyn: .............................. 26
3.3. Cn bng nhit lng ca thit b ngng tu hi lu: .................... 28
3.4. Cn bng nhit lng ca thit b lm lnh: ................................ 28
Chng 4: TNH KT CU CA THP CHNG LUYN ..................... 30
4.1. Kt cu da phn luyn: ................................................................ 30
4.2. Kt cu a on chng : ............................................................. 33
PHN 3: TNH C KH THIT B CHNH ................................................. 37
I. Tnh thn thit b chnh: ....................................................................... 37
II. Tnh y v np thit b: ..................................................................... 40
III. Tnh b dy lp cch nhit: ............................................................... 40
IV. Tnh ng knh cc loi ng dn: ................................................... 42
V. Chn bch: .......................................................................................... 44
VI. Tnh ti trng ca thp: ..................................................................... 46
VII. Chn tai treo, chn : ..................................................................... 49
PHN 4: TNH THIT B PH ................................................................ 51
I. Tnh ton thit b ngng t hi lu: ..................................................... 51
II. Thit b gia nhit nhp liu: ................................................................. 55
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC
III. Ni un: ............................................................................................. 57
IV. Thit b lm lnh sn phm nh: ...................................................... 60
V. Tnh v chn bm: ............................................................................. 63
PHN 5: KT LUN .................................................................................. 68
Cc ti liu tham kho : ......................................................................... 68
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 1
PHN 1: M U
I. L thuyt v chng luyn.
Chng l phng php dng tch cc hn hp cht lng cng nh cc hn
hp kh lng thnh cc cu t ring bit da vo bay hi khc nhau ca cc cu
t trong hn hp, ngha l khi cng mt nhit th p sut hi ca cc cu t
khc nhau.
Khi chng ta thu c nhiu sn phm v thng bao nhiu cu t s c by
nhiu sn phm. i vi trng hp hn hp chng ch gm hai cu t th sn phm
nh gm cu t c bay hi ln v mt phn rt t cu t c bay hi b cn
sn phm y gm cu t c bay hi b v mt phn rt t cu t c bay hi
ln.
Trong sn xut c rt nhiu phng php chng nh chng n gin, chng
bng hi nc trc tip, chng chn khng v chng luyn. Ty thuc vo iu kin
sn c, tnh cht hn hp, yu cu v tinh khit sn phm m ta chn phng
php chng cho thch hp.
- Chng n gin dng tch cc hn hp gm cc cu t c bay hi rt
khc nhau. Phng php ny thng dng tch s b v lm sch cu t khi
tp cht.
- Chng bng hi nc trc tip dng tch cc hn hp gm cc cht kh bay
hi v tp cht khng bay hi, thng dng trong trng hp cht c tch khng
tan vo nc
- Chng chn khng dng trong trng hp cn h thp nhit si cu t. V
d nh trng hp cc cu t trong hn hp d b phn hy nhit cao hay
trng hp cc cu t c nhit si qu cao.
- Chng luyn l phng php ph bin nht tch hon ton hn hp cc
cu t d bay hi c tnh cht ha tan mt phn hoc ha tan hon ton vo nhau.
- Chng luyn p sut thp dng cho cc hn hp d b phn hy nhit
cao v hn hp c nhit si cao.
- Chng luyn p sut cao dng cho cc hn hp khng ha lng p sut
thng.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 2
- Chng luyn p sut thng (p sut kh quyn ) dng cho hn hp khng
thuc cc trng hp trn.
Ngi ta tin hnh chng luyn hn hp cn chng trong thp chng luyn,
thp gm nhiu a, trn mi a xy ra qu trnh chuyn khi gia pha lng v pha
hi. Hi i t di ln qua cc l ca a, lng i t trn xung theo cc ng chy
chuyn, nng cc cu t v nhit si mi a thay i theo chiu cao ca
thp. Do mt phn cu t d bay hi chuyn t pha lng vo pha hi v mt
phn t hn chuyn t pha hi vo pha lng, lp li nhiu ln bc hi v ngng t
nh th, hay ni mt cch khc, vi mt s a tng ng, cui cng trn nh
thp ta thu c cu t d bay hi dng nguyn cht v thp ta thu c cu t
kh bay hi dng nguyn cht.
Qu trnh chng luyn c thc hin trong thit b loi thp lm vic lin tc
hoc gin on.
y ta s thit k h thng chng luyn thp mm chp lm vic lin tc vi
hn hp chng l ru mtylic v nc. Khi chng luyn lin tc, hn hp u c
a vo thp a tip liu (nm phn gia thn thp) mt cch lin tc, sn
phm nh v sn phm y cng c ly ra lin tc.
II. u, khuyt im ca phng php chng a chp.
u im: Tch c sn phm c tinh khit cao, d khng ch qu trnh, b
mt tip xc pha tng i ln, tr lc khng cao.
Khuyt im: Tip xc pha khng lin tc, cu to phc tp.
II.1. Tnh cht l ha ca ru tylic.
Ethanol c cng thc phn t: CH3-CH2-OH, khi lng phn t: 46 vC
L cht lng c mi c trng, khng c, tan nhiu trong nc
Mt s thng s vt l v nhit ng ca Ethanol
+ Nhit si 760 (mmHg): 78.3oC.
+ Khi lng ring: d420 = 810 (Kg/m3)
Tnh cht ha hc
Tt c cc phn ng ho hc xy ra nhm hydroxyl (-OH) ca Ethanol l th
hin tnh cht ho hc ca n
Phn ng ca hydro trong nhm hydroxyl
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 3
CH3-CH2-OH CH3-CH2-O- + H+
Hng s phn ly ca Ethanol: , cho nn Ethanol l cht trung
tnh.
Tnh acid ca ru th hin qua phn ng vi kim loi kim, Natri hydrua
(NaH), Natri amid(NaNH2):
CH3-CH2-OH + NaH CH3-CH2-ONa + H2
Natri etylat
Do : tnh acid ca ru nh hn tnh acid ca nc,
nn khi mui Natri etylat tan trong nc s b thu phn thnh ru tr li.
Tc dng vi acid to ester: Ethanol c tnh baz tng ng vi nc. Khi
ru tc dng vi acid v c H2SO4, HNO3 v acid hu c u to ra ester.
CH3-CH2-OH + HO-SO3-H CH3-CH2O-SO3-H + H2O
CH3-CH2O-H + HO-CO-CH3 CH3-COO-C2H5 + H2O
Phn ng trn nhm hydroxyl:
Tc dng vi HX: CH3-CH2-OH + HX CH3-CH2-X + H2O
Tc dng vi Triclo Pht pho
CH3-CH2-OH + PCl3 CH3-CH2-Cl + POCl + HCl
Tc dng vi NH3: CH3-CH2-OH + NH3 C2H5-NH2 + H2O
Phn ng to eter v tch loi nc
2CH3-CH2-OH ( CH3-CH2)2O + H2O
CH3-CH2-OH CH2=CH2 + H2O
Phn ng hydro v oxy ho
CH3-CH2-OH CH3-CHO + H2
ng dng ca Ethanol c nhiu ng dng hn Methanol, n ng mt vai tr
quan trng trong nn kinh t quc dn. N l nguyn liu dng sn sut hn 150
181023
OHCHCHK
1410223
OHOHCHCH KK
Lnh
Al2O3
to
H2SO4
>150oC
H2SO4
>150oC
Cu 200-300
oC
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 4
mt hng khc nhau v c ng dng rng ri trong cc ngnh: cng nghip nng,
y t v dc, quc phng, giao thng vn ti, dt, ch bin g v nng nghip.
S tm tt v tr ca Ethanol trong cc ngnh cng nghip
Phng php iu ch: c nhiu phng php iu ch Ethanol: hydrat ho
etylen vi xc tc H2SO4; thu phn dn xut halogen v ester ca Ethanol khi un
nng vi nc xc tc dung dch baz; hydro ha aldyhyt acetic; t cc hp cht c
kim
Trong cng nghip, iu ch Ethanol bng phng php ln men t ngun tinh
bt v r ng. Nhng nm gn y, nc ta cng ngh sn sut Ethanol ch
yu l s dng chng nm men Saccharomyses cerevisiae ln men tinh bt.
C6H6O6 2C2H5OH + 2CO2 + 28 Kcal
95% nguyn liu chuyn thnh Ethanol v CO2.
5% nguyn liu chuyn thnh sn phm ph: glyxrin, acid sucxinic, du fusel,
metylic v cc acid hu c (lactic, butylic).
II.2. Nc.
Trong iu kin bnh thng: nc l cht lng khng mu, khng mi, khng
v nhng khi nc dy s c mu xanh nht.
Khi ha rn n c th tn ti dng 5 dng tinh th khc nhau:
Nm men Zymaza
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 5
Khi lng phn t: 18 g/mol
Khi lng ring d4oC: 1 g/mol
Nhit nng chy: 0oC
Nhit si: 100oC
Nc l hp cht chim phn ln trn tri t (3/4 din tch tri t l nc
bin) v rt cn thit cho s sng. Nc l dung mi phn cc mnh, c kh nng
ho tan nhiu cht v l dung mi rt quan trng trong k thut ha hc.
II.3. Hn hp Ethanol Nc.
Bng 1: Thnh phn lng ( x ) hi (y) v nhit si ca hn hp Ethanol -
Nc 760 mmHg.
x(%phn
mol)
0 5 10 20 30 40 50 60 70 80 90
Y
(%phn
mol)
0 33,2 44,2 53,1 57,6 61,4 65,4 69,9 75,3 81,8 89,8
t(oC) 100 90,5 86,5 83,2 81,7 80,8 80 79,4 79 78,6 78,4
Hnh 1: Thnh phn lng ( x ) hi (y) v nhit si ca hn hp Ethanol -
Nc 760 mmHg.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 6
III. Quy trnh cng ngh.
Ethanol l mt cht lng tan v hn trong H2O, nhit si l 78,3oC
760mmHg, nhit si ca nc l 100oC 760mmHg: hi cch bit kh xa nn
phng php hiu qu thu Ethanol c tinh khit cao l phng php chng
ct.
Trong trng hp ny, ta khng th s dng phng php c c v cc cu
t u c kh nng bay hi, v khng s dng phng php trch ly cng nh
phng php hp th do phi a vo mt khoa mi tch, c th lm cho qu
trnh phc tp hn hay qu trnh tch khng c hon ton.
Hnh 2: S qui trnh cng ngh chng ct h Ethanol Nc
Ch thch cc k hiu trong qui trnh:
1. Bn cha nguyn liu.
2. Bm.
3. Bn cao v.
4. ng tun hon.
5. Lu lng k.
6. Thit b gia nhit nhp liu.
7. Thp chng ct.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 7
8. Ni un.
9. Thit b ngng t.
10 . Thit b phn tch hi lu.
11. Thit b lm lnh.
12. Bn cha sn phm nh.
13. Bn cha sn phm y.
14. By hi.
Thuyt minh qui trnh cng ngh:
Hn hp Ethanol nc c nng Ethanol 10% ( theo phn khi lng ),
nhit khong 28oC ti bnh cha nguyn liu (1) c bm (2) bm ln bn cao
v (3). T c a n thit b un si dng nhp liu (6). Sau , hn hp
c un si n nhit si v c a vo thp chng ct (7) a nhp liu.
Trn a nhp liu, cht lng c trn vi phn lng t on ct ca thp chy
xung. Trong thp, hi i t di ln gp cht lng t trn xung. y, c s tip
xc v trao i gia hai pha vi nhau. Pha lng chuyn ng trong phn chng cng
xung di cng gim nng cc cu t d bay hi v b pha hi to nn t ni
un (10) li cun cu t d bay hi. Nhit cng ln trn cng thp, nn khi hi i
qua cc a t di ln th cu t c nhit si cao l nc s ngng t li, cui
cng trn nh thp ta thu c hn hp c cu t Ethanol chim nhiu nht (c
nng 90% phn khi lng). Hi ny i vo thit b ngng t (9) v c ngng
t hon ton. Mt phn cht lng ngng t i qua thit b lm ngui sn phm nh
(11), c lm ngui n 35oC , ri c a qua bn cha sn phm nh (12).
Phn cn li ca cht lng ngng t c hon lu v thp a trn cng vi t s
hon lu ti u. Mt phn cu t c nhit si thp c bc hi, cn li cu t c
nhit si cao trong cht lng ngy cng tng. Cui cng, y thp ta thu c
hn hp lng hu ht l cc cu t kh bay hi (nc). Hn hp lng y c nng
Ethanol l 3% phn khi lng, cn li l nc. Dung dch lng y i ra khi
thp vo ni un (8). Trong ni un dung dch lng mt phn s bc hi cung cp li
cho thp tip tc lm vic, phn cn li ra khi ni un v a vo bn cha sn
phm y.
H thng lm vic lin tc cho ra sn phm nh l Ethanol, sn phm y
c thi b.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 8
PHN 2: TNH CNG NGH
Cc k hiu s dng trong qu trnh tnh ton:
GF: Lng hn hp u.
GD: Lng sn phm nh.
GW: Lng sn phm y.
: Nng phn khi lng ca cu t d bay hi trong hn hp u.
: Nng phn khi lng ca cu t d bay hi trong sn phm nh.
: Nng phn khi lng ca cu t d bay hi trong sn phm y.
xF: Nng phn mol cu t d bay hi trong hn hp u.
xD: Nng phn mol cu t d bay hi trong trong sn phm nh.
xW: Nng phn mol cu t d bay hi trong sn phm y.
Cu t d bay hi A: rutylic, cu t kh bay hi B: nc.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 9
Chng 1: CN BNG VT CHT
1.1. Tnh lng hn hp.
1.1.1. Nng phn mol.
Tnh F theo kmol/h:
(kmol/h)
i nng khi lng ra nng mol:
xA =
xF =
=
= 0.16 phn mol
xD =
=
= 0.78 phn mol
xW =
=
= 0.012 phn mol
1.1.2. Lu lng hn hp u v sn phm y.
Phng trnh cn bng vt liu cho ton thp:
F = D + W (Cng thc 3.52, trang 117, [3])
79.61 = W + D (1)
Vit cho cu t d bay hi:
F.xF = D.xD + W.xW (Cng thc 3.53, trang 117, [3])
(2)
T (1) v (2) suy ra:
{
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 10
Mt khc ta c:
D + W = 1800
0.9D + 0.03 W = 1800 x 0.335
{
Gi FM l phn t lng trung bnh ca hn hp u
FM = xF.ME + (1-xF).MN
= 0,16.46 + (1 0,16).18 = 22.48 (g)
1.2. Xc nh s a ca thp.
1.2.1. ng cong cn bng - th t-x-y theo thc nghim.
Gi x, y l nng mol phn ca thnh phn lng v hi ca ru tylic (tnh
theo phn mol)
t (0C) l nhit si ca hn hp hai cu t ( 760 mmHg).
x 0 5 10 20 30 40 50 60 70 80 90
y
0 33,2 44,2 53,1 57,6 61,4 65,4 69,9 75,3 81,8 89,8
t (oC) 100 90,5 86,5 83,2 81,7 80,8 80 79,4 79 78,6 78,4
Da vo bng s liu ny ta v th ng cong cn bng ca hn hp r
tylic v nc v th biu din ng cong si.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 11
Hnh 2: th ng cong cn bng ca hn hp ru tylic v nc.
Hnh 3: th biu din ng cong si.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 12
Theo th ng cn bng ta xc nh c y*F = 0,5 phn mol l nng
cu t d bay hi trong pha hi cn bng vi pha lng trong hn hp u ng gi tr
xF = 0,16.
Theo th ng cong si ta xc nh c nhit si ca hn hp u
tsF=84oC, ca sn phm nh tsD = 78
oC, ca sn phm y tsW= 97oC.
x y kg/h kmol/h Nhit
si (oC)
= 0.335 xF = 0.16 yF = 0.5 F = 1800
kg/h
F = 79.61
kmol/h 84oC
= 0.9 xD = 0.78 yD = 0.8 D = 631.0345
kg/h
D = 15.34
kmol/h 78oC
= 0.03 xW = 0.012 yW = 0.11 W = 1168.9655
kg/h
W = 64.27
kmol/h 97oC
Suy ra ch s hi lu ti thiu l:
Rxmin =
(Cng thc IX.24, trg 158, [2])
Rmin =
= 0.82
Ch s hi lu thch hp l:
R = 1.3Rmin + 0.3
= 1.3 X 0.82 + 0.3 = 1.37
xc nh s a l thuyt ca thp bng cch da vo phng trnh ng
nng lm vic ca on luyn v on chng.
Phng trnh lm vic ca on luyn
y =
(Cng thc IX.20, trang 144, [2])
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 13
y =
= 0.59x = 0.33
Phng trnh lm vic ca on chng:
y = RL
Rth
th
1.y +
RL th
L
1
.(Cng thc IX.22, trang 158, [2])
Vi: L =
y =
= 2.77x 0.02
V trn th 2 ng lm vic on chng v ng lm vic on ct ta c c
s mm l thuyt l: Nlt = 12 mm. S mm l thuyt on ct l 9.4 mm v on
chng l 2.6 mm.
1.2.2. Xc nh s a thc t.
S a thc t c xc nh theo cng thc:
Ntt = tb
ltN
(Cng thc IX.59, trang 170, [2])
Vi tb l hiu sut trung bnh ca thit b, l hm ca bay hi tng i
v nht ca hn hp = f(,).
=x
x
y
y
1.
1(Cng thc IX.61, trang 171, [2])
nht: lghh = n.lg1 + (1-n)lg2
n l nng cu t th nht
n -1 l nng cu t th hai
1, 2 l nht hai cu t.
( nht ca ru tylic theo nhit c tra bng dng cho ton
h.I.18, trg 93, [2], nht ca nc theo nhit c tra bng I.102, trang 94,
[2]).
= tb = .(3
11 + 2 + 3 ) (Cng thc IX.60, trang 171, [2])
Vi: 1 l hiu sut ng vi a trn cng
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 14
2 l hiu sut ng vi a tip liu
3 l hiu sut ng vi a cui cng
- ng vi a tip liu:
bay hi:
F =
= 5.25
nht:
Ti = 84oC ta c {
lgF = OHFOHCHF xx 23 lg).1(lg
= 0,16.lg0,4132 + (1 - 0,16).lg0,3395 = -0,4555
F = 0,3503 (Cp)
Tch F.F = 0,3503 X 5,25 = 1,8391.
Tra th hnh IX.11, trang 171, [2] ta c hiu sut ca a tip liu 2 = 42
%.
- ng vi a trn cng:
bay hi:
D =
= 1.1282
nht:
Ti = 78oC ta c {
lgD = OHDOHCHD xx 23 lg).1(lg
= 0,78.lg0,4506 + (1 - 0,78).lg0,3655 = - 0,3662
D = 0.4303 (Cp)
Tch D.D = 0,4303 . 1.1282 = 0,4855. Tra th hnh IX.11, trang 171, [2],
ta c hiu sut ca a trn cng 1 = 59 %.
- ng vi a cui cng:
bay hi:
W =
= 10.1760
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 15
nht:
Ti = 97oC ta c {
lgW = OHwOHCHw xx 23 lg).1(lg
= 0.012.lg0,3424 + (1 - 0,012).lg0,2930 = - 0,5323
W = 0,2935 (Cp)
Tch W.W = 0,2935 . 10.1760 = 2.9871. Tra th hnh IX.11, trang 171, [2], ta
c hiu sut ca a trn cng 3 = 38%.
Vy hiu sut trung bnh:
tb = 3
1(1 + 2 + 3) =
3
1(59 + 42 + 38) = 46.33(%)
S a thc t l:
Ntt =
= 25.8999 (mm)
Vy thc t phi chn 25.8999 a.
Tnh ring cho phn ct:
= 20.29 (mm)
Tnh ring cho phn chng:
= 5.61 (mm)
(yF , yP , yW c xc nh t th ng cn bng hnh 1)
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 16
Chng 2: TNH NG KNH THIT B
ng knh thp: (cng thc IX.89, trang 181, [2])
D = tb
tbV
.3600.
.4 , m
Hoc D = 0,0188.tbyy
tbg
).( , m
Trong : Vtb - Lng hi trung bnh i trong thp, m3/h
tb - Tc hi trung bnh i trong thp, m/s
gtb - Lng hi trung bnh i trong thp, kg/h
(y.y)tb - Tc hi trung bnh i trong thp, kg/m2.s
2.1. ng knh on luyn.
2.1.1. Lng hi trung bnh i trong on luyn gtb.
C th xem gn ng bng trung bnh cng lng hi i ra khi a trn cng
ca thp g v lng hi i vo di cng g1 ca on luyn:
gtb = 2
1ggd , kg/h
Trong , g = GR +GP = GP(RX+1) (cng thc IX.92, trang 181, [2]).
Vi GR: lng lng hi lu, kg/h
GP: lng sn phm nh, kg/h
RX: ch s hi lu
= > g = 631.0345.(1.37+1) = 1495.5518 kg/h
Lng hi i vo a u tin ca on luyn c xc nh theo h phng
trnh cho trang 182 S tay QTTB tp 2:
dd
PP
P
rgrg
xGxGyg
GGg
..
...
11
1111
11
Trong : x1 = = 0,335 (phn khi lng)
xP = = 0,90 (phn khi lng)
G1:lng lng a th nht on luyn
r: n nhit ha hi ca hn hp i ra khi nh thp
r1: n nhit ha hi ca hn hp i vo a th nht on luyn
r1= ra .y1 + (1-y1).rb
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 17
r= ra .y + (1-y).rb
ra, rb: n nhit ha hi ca ru tylic v nc.
y = = 0,90 phn khi lng.
*Tnh r1: hn hp u vo thp 84oC nn ta phi tnh ra, rb 84
oC.
(Theo bng I.212, trang 254, [1]) ta c:
60oC: ra1 = 879.9 kJ/kg
rb1 = 2359 kJ/kg
100oC: ra2 = 812.9 kJ/kg
rb2 = 2258.4 kJ/kg
Theo phng php ni suy ta tnh ra, rb 84oC:
ra84 = ra
60 + ( )
( ) ( ) = 839.7 kJ/kg = 200.6068 kcal/kg
rb84 = rb
60 + ( )
( ) ( ) = 2298.64 kJ/kg=551.5553 kcal/kg
Vy: r1 = ra.y1 +(1-y1).rb = 200.6068.y1 + (1-y1).551.5553
= 551.5553 350.9485y1
*Tnh r: hi i ra khi nh thp nhit 78oC, tng t nh trn:
ra78 = ra
60 + ( )
( ) ( )=1066.975kJ/kg = 254.9035 kcal/kg
rb67 = rb
60 + ( )
( ) ( ) = 2313.73 kJ/kg =552.7569 kcal/kg
Vy: r = ra.y + (1- y).rb = 254,9035.0,90 +(1-0,90).552,7569
= 284.6888 kcal/kg
Vy ta c h phng trnh :
{
( )
Gii h ta c :
{
- Lng hi trung bnh i trong on luyn:
gtb = hkgggd /4609,1382
2
37.12695518,1495
2
1
- Lng lng trung bnh i trong on luyn:
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 18
Gtb = hkgGRGGG XPR /4276,751
2
338,63837.1.0345,631
2
.
2
11
- Thnh phn hi cn bng i trn on luyn:
ytb = 758.02
6159.09.0
2
1
yyd
phn khi lng
= 0,5507 phn mol
- Phn t lng trung bnh ca hn hp hi:
tbM = ytb.MA +(1- ytb).MB = 0,5507.46 + (1-0,5507).18 = 33.4196 vC
2.1.2. Tc hi trung bnh i trong on luyn.
(yy)tb = 0,065[] . ytbxtbh .. , kg/m2. (Cng thc IX.105, trang 184, [2]).
xtb, ytb: Khi lng ring trung bnh ca pha lng v pha hi tnh theo nhit
trung bnh, kg/m3.
h: Khong cch cc a trong thp,m,vi gi tr h c chn theo ng knh
thp.
[] : H s tnh n sc cng b mt.
*Tnh [] nhit trung bnh:
Nhit trung bnh trong on luyn:
ttb = Ctt oPF 81
2
7884
2
Theo bng I.242, trang 300, [1] ta c sc cng b mt ca ru v nc:
80oC: a1 = 17.3 dyn/cm (tylic)
b1 = 62.6 dyn/cm (nc)
100oC: a2 = 15.5 dyn/cm (tylic)
b2 = 58.9 dyn/cm (nc)
8.112 aaa dyn/cm
7,312 bbb dyn/cm
Cttt 012 2080100
09,020
8,1
t
a dyn/cm.
185,020
7,3
t
b dyn/cm.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 19
Bng phng php ni suy ta tnh c sc cng b mt ca tylic v nc
81oC:
a81 = a1
80 + )8081(
t
a = 17,3 - 0,09.(81-80) = 17,21 dyn/cm
b81 = b1
80 +
)8081.(185,06.62)8081(
t
b 62.415 dyn/cm
Sc cng b mt ca hn hp:
bahh
111 (cng thc I.76, trang 299, [1])
49,13.
ba
bahh
dyn/cm
Ta thy hh < 20 dyn/cm nn chn [] = 0,8.
*Tnh khi lng ring trung bnh:
Khi lng ring ca tylic v nc: (Theo bng I.2, trang 9, [1])
- 800C: a1 = 735 kg/m3 (tylic)
b1 = 972 kg/m3 (nc)
- 1000C: a2 = 710 kg/m3 (tylic)
b2 = 958 kg/m3 (nc)
2512 aaa kg/m3
1412 bbb kg/m3
Ct 02080100
25.120
25
t
a kg/m3.
7,0
20
11
t
b kg/m3.
Theo phng php ni suy, tnh khi lng ring ca tylic v nc 81oC:
75.73325.1735)8081(80
1
81
t
aaa
kg/m3
3.971.7,097280818081
t
b
bb
kg/m
3
Khi lng ring ca hn hp (cng thc I.2, trang 5, [1]):
b
b
a
a
hh
xx
1
Vi xa, xb: Nng phn khi lng ca cc cu t trong hn hp
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 20
xa = 6175,02
335,090,0
phn khi lng
xb = 1-xa = 0,3825 phn khi lng
hh = 809.4745 kg/m3
xTB = hh = 809.4745 kg/m3
Khi lng ring ca pha hi: (cng thc I.3, trang 5, [1]):
0.
.273.
4,22 pT
pMyTB , p = p0 = 1atm
1506.181273
273.
4,22
33.4196
yTB
kg/m3
Vy tc trung bnh ca hi trong thp:
hhtbyy 587,11506,1.4745,809..8,0.065,0)( kg/m2.s
ng knh on luyn:
D = 0,0188.4
5382,0
.587,1
5692.1300
hh
Chn h = 0,35 (m) D = 0,7 m
2.2. ng knh on chng.
2.2.1. Lng hi trung bnh trong on chng gtb.
C th xem gn ng bng trung bnh cng lng hi i ra khi on chng gn
v lng hi i vo on chng g1:
gtb = 2
'' 1gg n , kg/h (Cng thc IX.96, trang 183, [2]).
V lng hi i ra khi on chng bng lng hi i vo on luyn nn:
gn = g1 = 1269.37 kg/h
Lung hi i vo an chng g1, lung lng G1 v hm lng lng x1 c
xc nh theo h phng trnh cho trang 182, S tay QTTB tp 2:
)3(
1111
)2(
111
)1(
11
.'.''.'
..''.'
''
rgrgrg
xGygxG
GgG
nn
www
w
Trong r1: n nhit ha hi ca hn hp hi i vo a th nht ca on
chng, c tnh theo cng thc:
r1= ra.y1 + (1-y1).rb
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 21
Vi y1 = yW l thnh phn cu t d bay hi (tylic) trong pha hi cn bng vi
pha lng trong sn phm y. Da vo th ng cn bng (H.1) ng vi
xW=0,012 ta c yW = 0,11 phn mol ng vi phn khi lng:
y1= 24,018.89,046.11,0
46.11,0
phn khi lng.
Theo th ng cong si (H.2) ta c sn phm y c nhit si l 97oC,
theo cc s liu 11,,,, baba rrtrr c phn tnh ton ng knh on luyn ta
c:
ra97 = ra
60 + )/(925,81737.675,19.879)6097( kgkJt
ra
= 195,4047 kcal/kg
rb97 = rb
60 + )/(945,226537.515,22359)6097( kgkJt
rb
= 458,3163 kcal/kg
r1 = ra97.y1 + (1-y1).rb
97
= 195,4047.0,24 + (1-0,24).541,341 = 458,3163 kcal/kg
Thay r1, g1, r1 vo (3):
g1.458,3163 = 1269,37.335,4052
g1 = 928,9508 kg/h
Thay vo (1):
G1 = 928,9508 + 1168,9655 = 2097,9163 kg/h
Thay vo (2):
2097,9163.x1= 928,9508.0,24 + 1168,9655.0,03
x1 = 0,123 phn khi lng
Vy lng hi trung bnh i trong on chng:
gtb = hkggg n /1604,1099
2
9508,92837,1269
2
'' 1
Lng lng trung bnh i trong on chng:
Gtb = hkgGG
/1272,13682
9163,2097338,638
2
'11
Thnh phn hi trung bnh i trong on chng:
ytb = 2
''1 nyy
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 22
Vi yn l hm lng trn a trn cng on chng xem bng hm lng hi a
th nht on luyn yn = y1 = 0,6159 phn khi lng.
ytb = 428,02
6159,024,0
(phn KL) = 0.2265 phn mol
Phn t lng trung bnh ca hn hp hi trong on chng:
'M hh = ytb.MA + (1-ytb).MB
=0,2265.46 + 0,77735.18 = 24,342 vC
2.2.2. Tc hi trung bnh trong on chng.
(yy)tb = 0,065[]. ytbxtbh '.'. ; kg/m2.s (Cng thc IX.105, trang 184, [2].
xtb, ytb: Khi lng ring trung bnh ca pha lng v pha hi tnh theo nhit
trung bnh, kg/m3.
h: Khong cch cc a trong on chng ,gi tr ca h chn theo ng knh
thp.
[]: H s tnh n sc cng b mt.
*Tnh [] nhit trung bnh on chng ttb = Ctt owF 5,90
2
9784
2
:
Tra sc cng b mt ca tylic v nc (bng I.242, trang 300, [1]), ta c :
a180 = 17,3 dyn/cm , a2
100 = 15,5 dyn/cm
b180 = 62,6 dyn/cm , b2
100 = 58,9 dyn/cm
Tnh tng t nh phn luyn:
cmdynt
aaa /355,165,10.09,03,17)805,90(
80
1
5,90
cmdynt
bbb /6575,605,12.185,06,62)805,90(
80
1
5,90
Sc cng b mt ca hn hp:
bahh
111
ba
bahh
.
hh = 12,8817 dyn/cm
*Tnh khi lng ring trung bnh pha lng:
Tra khi lng ring ca tylic v nc (bng I.2, trang 9, [1]) ta c:
a180 = 735 kg/m3 , a2
100 = 716 kg/m3
b180 = 972 kg/m3 , b2
100 = 958 kg/m3
Bng phng php ni suy ta c:
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 23
380
1
5,90/025,7255,10.95,0735)805,90( mkg
t
aaa
3801
5,90/65,9645,10.7,0972)805,90( mkg
t
bbb
Khi lng ring ca hn hp:
b
b
a
a
hh
xx
1
xa, xb: Phn khi lng trung bnh ca tylic v nc trong hn hp
xa = 1825,02
03,0335,0
2
wF xx (phn khi lng),
xb = 1- xa = 0,8175 (phn khi lung).
hh = 909,7748 kg/m3 = xt
Khi lng ring ca pha hi:
5,90273
273.
4,22
'
hhytbM
=
( ) = 0,8161 kg/m3
Vy tc trung bnh ca hi trong on chng:
hhtbyy 417,18161,0.7748,909.8,0.065,0)''(
ng knh on chng:
D = 0,0188.h
g
tbyy
tb
.417,1
1604,10990188,0
)''(
'
D =4
5,0
h , m
Chn h = 0,3 m D = 0,68 m.
V ng knh on chng v on ct khng chnh lch nhau nhiu nn ta ly
ng knh chung cho ton thp l D = 0,7m.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 24
Chng 3: CN BNG NHIT LNG
Gi QD1 l nhit lng do hi nc cung cp un si hn hp u.
Qf l nhit lng do hn hp u mang vo thit b un si hn hp.
QF l nhit lng do hn hp u mang ra khi thit b un si hn hp
u.
Qm l nhit lng do mt mt.
Qy l nhit lng do hi mang ra khi thp chng
QR l nhit lng do lng hi lu mang vo thp.
Qh l nhit lng do hi mang ra khi thit bi ngng t hi lu.
QD2 l nhit lng do hi t un si y thp mang vo.
3.1. Cn bng nhit lng ca thit b un nng hn hp u.
QD1 + Qf = QF + Qm (8)
3.1.1. Nhit lng do hi t mang vo QD1.
QD1 = D1.r1 (Cng thc IX.150, trang 196, [2])
D1: Lng hi t cn thit un si hn hp u, kg/h.
r1: n nhit ha hi ca hi nc, J/kg.
V nhit si ca hn hp u l 840C nn nhit ca hi nc phi cao,
chn 110,70C tng ng vi nc si p sut 1,5 at (bng I.97, trang 230, [1]).
Theo ton xc nh nhit ha hi trang 255, [2] ta c nhit ha hi ca nc
110,70C l r1 = 2232,18 kJ/kg.
3.1.2. Nhit lng do hn hp u mang vo thit b un si hn hp
u Qf.
Qf = F.Cf .tf (J/h). (Cng thc I X.151, trang 196, [2]).
Vi Cf: nhit dung ring ca hn hp u, J/kg.
tf: nhit u ca hn hp, xt 250C.
Ta c: Cf = .CA + (1 - ).CB
: nng phn khi lng trong hn hp u, = 0,335
CA, CB: nhit dung ring ca tylic v nc 250C .
*Nhit dung ring ca tylic 25oC:
Nhit dung ring ca tylic theo nhit :
CA20 = 2480 J/kg. , CA
40 = 2710 J/kg.
Nhit dung ring ca tylic 250C l:
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 25
CA25 = CA
20 + kgdoJCC AA /5,25375,.112480)2025(2040
2040
*Nhit dung ring ca nc 25oC:
Ta c nhit dung ring ca nc 250C l CB25 = 4178,8 J/kg.
Vy: Cf = 0,335.2537,5 + (1-0,335).4178,8 = 3629 J/kg.
Qf = 1800.3,629.25 = 163305 kJ/h
3.1.3. Nhit lng do hn hp u mang ra khi thit b un si QF.
QF = F.CF . tF , J/h (Cng thc IX.152, trang 196, [2].
Vi: CF: Nhit dung ring hn hp i ra thit b un si.
tF = 840C.
Ta c: CF = .CA + (1- ).CB
CA ,CB :Nhit dung ring ca tylic v nc 84oC.
Tra bng nhit dung ring v theo phng php ni suy ta c:
Nhit dung ring ca tylic 84oC:
CA80 = 3.22 kJ/kg. ; CA
100 = 3.52 kJ/kg.
kgdoJCC
C AAA /32804.20
322035203220)8084(
80100
80100
84
Nhit dung ring ca nc 84oC:
CB84 = 4198 J/kg.
CF = 0,335.3280 + 0,665.4198 = 3,8905 kJ/kg.
Vy QF = 1800.3,8905.84 = 588243,6 kJ/h.
3.1.4. Nhit lng tn hao ra mi trng xung quanh Qm.
Qm = 0,05.QD1
Thay vo (*):
QD1 + Qf = QF + 0,05.QD1
QD1 = 95,0
fF QQ
=
= 447303,7895 kJ/h
Qm = 0,05.447303,7895 = 22365,1895 kJ/h
3.1.5. Lng hi t cn dng un si hn hp u. QD1 = D1.r1
D1 = hKgr
QD /3888,20018,2232
7895,447303
1
1
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 26
3.2. Cn bng nhit lng ca thp chng luyn.
Phng trnh cn bng nhit ca thp chng luyn:
QF +QD2 + QR = Qh + QW + Qm (** )
3.2.1. Lng nhit do lng lng hi lu mang vo thp QR.
QR = CR.D.RX.tR J/h (Cng thc IX.158, trang 196, [2])
Vi : RX: ch s hi lu, RX = 1,37
D: lng sn phm nh, D = 631,0345 kg/h
tR: nhit lng hi lu, tR = tD = 78oC
CR: nhit dung ring ca lng hi lu
CR = .CA + (1 - ).CB
CA, CB :nhit dung ring ca tylic v nc 78oC
Tra bng nhit dung ring ca tylic v nc 60oC v 80oC, theo phng
php ni suy ta c:
CA60 = 2.97 kJ/kg. ; CA
80 = 3.22 kJ/kg.
CA78 = CA
60 + )6078(6080
6080
AA CC
= dokgkJ ./195,3)6078(20
97,222,397,2
CB60 = 4.19 kJ/kg. ; CB
80 = 4.19 kJ/kg.
CB78 = 4,19 kJ/kg.
CR = 0,9.3,195 + 0,1.4,19 = 3,2945 kJ/kg.
Vy: QR = 3,2945.631,0345.1,37.78 = 222155,8661 kJ/h
3.2.2. Nhit lng do sn phm y mang ra QW.
QW = GW.CW.tW, J/h (Cng thc IX, trang 197, [2])
Vi: GW: Lng sn phm y, GW = 1168,9655 kg/h
CW: Nhit dung ring ca sn phm y
tW: Nhit sn phm y , tW = 97oC.
CA80 = 3.22 kJ/kg. ; CA
100 = 3.52 kJ/kg.
Bng phng php ni suy ta c: CA97 = 3,475 kJ/kg.
CB80 = 4.19 kJ/kg. ; CB
100 = 4.23 kJ/kg.
Bng phng php ni suy ta c: CB97 = 4,224 kJ/kg.
CW = CA97. + CB
97(1- )
= 0,03.3,475 + 0,97.4,224 = 4,2015 kJ/kg.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 27
Vy nhit lng do sn phm y mang ra:
QW = 1168,9655.4,2015.97 = 476406,6292 kJ/h
3.2.3. Nhit lng do hi mang ra khi thp chng Qy.
Qy = P.(1+RX). , J/h (Cng thc IX.159, [2])
Vi: P: Lng sn phm nh, P = 631,0345 kg/h.
: Nhit lng ring ca hi nh thp, c tnh:
= A. + B.(1 - )
A, B: Nhit lng ring ca tylic v nc nh thp
: phn khi lng cu t d bay hi (tylic) trong sn
phm nh, = 0,90.
Nhit dung ring mt cu t c tnh theo:
= r + C.t
Vi: r: n nhit ha hi ca cu t .J/kg
C: Nhit dung ring ca cu t nhit t = tP = 78oC
Nhit dung ring ca tylic 78oC:
CA = 3,195 kJ/kg.
Nhit dung ring ca nc 78oC:
CB = 4,19 kJ/Kg.
( tnh phn tnh nhit lng do lng hi lu).
= (rA + CA.tP).aA + (rB + CB.tP).(1 - aA)
= rA. + rB.(1 - ) + [CA. + CB.(1 - )].tD
= r + [CA. + CB.(1 - )].tD
Vi r = rA. + rB.(1 - ) l n nhit ha hi ca hn hp, tnh phn tnh
ng knh on luyn:
r = 284,6888 kcal/kg = 1191,6504 kJ/kg
= 1191,6504 + (3,195.0,90 + 4,19.0,1).78
= 1448,6214 kJ/kg
Vy nhit lng do hi mang ra khi nh thp:
Qy = 631,0345.(1 + 1,37).1448,6214 = 2166488,292 kJ/h.
3.2.4. Nhit lng do hi t mang vo un si hn hp y thp QD.
Nhit lng tn hao Qm = 0,05.QD2 , thay vo (**), ta c:
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 28
95,0
)()(2
RFwy
D
QQQQQ
= 584,192894295,0
) 1222155,866 (588243,6) 6292,476406 22166488,29(
kJ/h
Do lng hi t s dng:
D2 = hkgr
QD /152,86418,2232
584,1928942
1
2
Lng nhit tn hao:
Qm = 0,05.QD2 = 0,05.1928942,584 = 96447,1292 kJ/h
3.3. Cn bng nhit lng ca thit b ngng tu hi lu.
Ta dng thit b trao i nhit ng chm ngng t hon ton sn phm nh.
P.(RX+1).r = Gn1.Cn.(t2 - t1) (Cng thc IX.164, [2])
Vi: P: Lng sn phm nh, P = D = 631,0345 kg/h
RX: Ch s hi lu, RX = 1,37
Gn1: Lng nc cn dng cho thit b ngng t hi lu.
t1, t2: nhit ca nc i vo v ra khi thit b ngng t hi lu,
chn t1 = 25oC, t2 = 45
oC.
Nhit trung bnh trong thit b ngng t hi lu: ttb= Ctt o35
2
21
Cn: Nhit dung ring ca nc nhit trung bnh 35oC
Cn = 4,1763 kJ/kg.
r: n nhit ha hi ca hi i ra khi nh thp, tnh trong phn
ng knh on luyn, r = 284,6888 kcal/kg = 1191,6504 kJ/kg.
Vy lng nc lnh cn dng cho thit b ngng t hi lu:
Gn1 = hkgttC
rRP
n
X /7677,21336)2545.(1763,4
6504,1191).137,1.(0345,631
).(
).1.(
12
3.4. Cn bng nhit lng ca thit b lm lnh.
Dng thit b trao i nhit ng chm.
P.CP.(t1-t2) = Gn2.Cn.(t2-t1) (Cng thc IX.167, trang 198, [2]).
Vi: Gn2: Lng nc lnh dng cho thit b, kg/h
CP: Nhit dung ring sn phm nh ngng t, J/kg.
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N HC PHN CNG NGH HA HC Trang 29
t1, t2: Nhit u v cui ca sn phm nh khi qua thit b lm lnh, t1 = 78
oC , t2 = 35oC .
t1,t2: Nhit vo v ra ca nc lm lnh, chn t1 = 25oC,
t2 = 45oC . ttb = 35
oC.
Cn: Nhit dung ring ca nc 35oC, Cn = 4,1763 kJ/kg
CP: Nhit dung ring sn phm nh ttb = C05,56
2
3578
.
Tnh nhit dung ring ca sn phm nh 56,5oC:
CP = .CA + (1 - ).CB
Tra bng I.154, trang 172, [1] ta c nhit dung ring ca ru tylic theo nhit :
CA40 = 2,71 kJ/kg., CA
60 = 2,97 kJ/kg.
CA56,5 = CA
40 + )405,56(4060
4060
AA CC
= 9245,2)405,56(4060
71,297,271,2
kJ/kg.
Nhit dung ring ca nc nhit 56,5oC:
CB56,5 = 4,1874 kJ/kg.
Vy: CP = 0,90.2,9245 + 0,10.4,1874 = 3,0508 J/kg.
Lng nc lnh cn dng cho thit b lm lnh:
(
)
( )
( )
( ) = 991,0912 kg/h.
Nhit lng ca thit b lm lnh:
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 30
Chng 4: TNH KT CU CA THP CHNG LUYN
4.1. Kt cu a phn luyn.
4.1.1. Tnh ton.
Cc cng thc c gi tr sau c tra trang 236, [2]:
- ng knh ng hi ca chp: dh = 50 mm = 0,05 m
- S chp phn b trn a:
2
2
.1,0hd
Dn
Vi: D: ng knh trong ca thp, m.
dh: ng knh ng hi ca chp, m .
6,1905,0
7,0.1,0
2
n Chn n = 20 (chp ).
- Chiu cao chp pha trn ng dn hi:
h2 = 0,25.dh = 0,25.0,05 = 0,0125 m = 12,5 mm.
- ng knh chp:
22
).2( chhhch ddd
Vi ch: chiu dy chp, chn ch = 2,5 mm
Vy: 3303,74)5,2.250(50 22 chd mm
- Khong cch t mt da n chn chp:
S = 0 25 mm, chn S = 5 mm.
- Chiu cao mc cht lng trn khe chp:
h1 = 15 40 mm, chn h1 = 20 mm.
- Chiu cao khe chp:
x
yy
gb
.
..2
(Cng thc IX.215, trg 236, [2].
Vi: y = nd
V
h
y
...3600
.42
; Vy - lu lng hi i trong on luyn, m
3/h ;
- h s tr lc ca a chp, chn = 2;
x, y - khi lng ring trung bnh ca pha lng v hi, kg/m3. (
tnh phn tnh ng knh on luyn).
x = 809,4745 kg/m3; y = 1,1107 kg/m
3.
*Tnh Vy:
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N HC PHN CNG NGH HA HC Trang 31
Vy =ytb
tbg
Vi:gtb = Lng hi trung bnh i trong on luyn ( tnh phn tnh ng
knh on luyn). gtb = 1382,4609 kg/h
ytb - Khi lng ring trung bnh pha hi trong on luyn, kg/m3.
= 1244,6753 m3/h
y = 81,820.05,0..3600
6753,124442
m/s
Chiu cao ca khe chp:
b = m022,04745,809.81,9
1107,1.81,8.2 2 = 22 mm
S lng khe h ca mi chp:
).4
(
2
b
dd
ci hch
Vi: gtb - Lng hi trung bnh i trong on luyn, kg/h
c - Khong cch gia cc khe, chn c = 3 mm.
i = 480642,48)22.4
503303,74(
3
2
khe
- ng knh ng chy chuyn:
z
Gd
CX
Xc
....3600
.4
;
Vi: GX - Lu lng lng trung bnh i trong don luyn, kg/h. ( tnh phn
tnh ng knh on luyn).
GX = 751,4276 kg/h.
X - Khi lng ring trung bnh ca lng trong on luyn.
Z - S ng chy chuyn, chn z = 1.
C - Tc cht lng trong ng chy chuyn,
Chn C = 0,15 m/s.
Vy: mdC 0468,01.15,0.4745,809..3600
4276,751.4
= 46,8 m
- Khong cch t mp di ng chy chuyn n a:
S1 =0,25.dC = 0,25.0,0468 = 0,0117 (m) = 11,7 (mm).
- Chiu cao ng chy chuyn trn a:
hC = (h1 +b +S) - h
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N HC PHN CNG NGH HA HC Trang 32
Trong : h - chiu cao mc cht lng bn trn ng chy chuyn:
h = 3 2)..85,1.3600
(Cd
V
Vi: V - th tch cht lng chy qua
V = hmG
X
X /9283,04745,809
4276,751 3
h = m00965,0)0468.0..85,1.3600
9283,0(3 2
= 9,65 mm
hC = (20 + 22 + 5) 9,65 = 37,35 mm.
- Bc ti thiu ca chp trn a:
tmin = dch + 2.ch + l2
Vi: l2 = 12,5 + 0,25.dch l khong cch nh nht gia cc chp, thng ly
I2=35mm ta chn I2 = 35mm.
tmin = 74,3303 + 2.2,5 + 35 = 114,3303 mm
- Khong cch t tm ng chy chuyn n tm chp gn nht:
t1 = 122
ldd
chch
CC
Trong : C - B dy ng chy chuyn, thng ly C = 2 4, chn C = 3 mm
l1 - khong cch nh nht gia ng chy chuyn v chp,
chn l1 = 75 mm
Vy: t1 = mm07,141755,22
3303,743
2
8,46
4.1.2. Cc kt cu a phn luyn.
- ng knh ng hi: dh = 50 mm
- S chp: n = 20 chp
- ng knh chp: dch = 74,3303mm
- Chiu cao chp trn ng dn hi: h2 = 12,5 mm
- Khong cch t mt a n chn chp: S = 5 mm
- Chiu cao mc cht lng trn khe chp: h1 = 20 mm
- Chiu cao khe chp: b = 22 mm
- Khong cch gia cc khe: c = 3 mm
- S khe h ca mi chp: I = 48 khe
- ng knh ng chy chy chuyn: dC = 46,8 mm
- Chiu cao lp cht lng trn ng chy chuyn: h = 9,65 mm
- Khong cch t mp di ng chy chuyn n a: S1 = 11,7 mm
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N HC PHN CNG NGH HA HC Trang 33
- Chiu cao ng chy chuyn trn a: hC = 37,35 mm
- B dy ng chy chuyn: C = 3 mm
- B dy chp: ch = 2,5 mm
- Khong cch t tm ng chy chuyn n tm chp gn nht:
t1 = 141,07 mm
- Khong cch gia hai tm chp: tmin=114,3303 mm
- Khong cch nh nht gia hai chp: l2 = 35 mm
- Khong cch nh nht gia chp v ng chy chuyn: l1 = 75 mm
4.2. Kt cu a on chng.
4.2.1. Tnh ton.
Cc cng thc c gi tr sau c tra trang 236, [2]:
- ng knh ng hi ca chp, thng chn: 50; 75; 100; 125; 150 mm.
Ta chn: dh = 50 mm = 0,05 m.
- S chp phn b trn a:
2
2
.1,0hd
Dn
Vi: D : ng knh trong ca thp, tnh phn tnh ng knh thp,
D = 0,7 m.
dh: ng knh ng hi ca chp, m
6,1905,0
7,0.1,0
2
n (chp)
Chn n = 20 (chp )
- Chiu cao chp pha trn ng dn hi:
h2 = 0,25.dh = 0,25.0,05 = 0,0125 m = 12,5 mm.
- ng knh chp:
22
).2( chhhch ddd
Vi: ch: chiu dy chp, chn ch = 2,5 mm.
Vy: 3303,74)5,2.250(50 22 chd mm
- Khong cch t mt da n chn chp:
S = 0 25 mm, chn S = 5 mm.
- Chiu cao mc cht lng trn khe chp:
h1 = 15 40 mm, chn h1 = 20 mm
- Chiu cao khe chp:
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 34
x
yy
gb
.
..2
(Cng thc IX.215 trang 236, [2]).
Vi: y = nd
V
h
y
...3600
.42
; Vy -lu lng hi i trong on chng, m
3/h.
- H s tr lc ca a chp, chn = 2
x ,y - khi lng ring trung bnh ca pha lng v hi ,kg/m3. tnh
phn tnh ng knh on chng:
x = 909,7748 kg/m3; y = 0,7953 kg/m
3.
*Tnh Vy :
Vy =ytb
tbg
'
Vi:
l lu lng hi trung bnh i trong on chng.
= 1099,1604 kg/h.
ytb - khi lng ring trung bnh pha hi trong on chng , kg/m3.
Vy =
= 1382,07 m3/h
y = 78,920.05,0..3600
07,1382.42
m/s.
Chiu cao ca khe chp:
b = m017,07748,909.81,9
7953,0.78,9.2 2 = 17 mm.
- S lng khe h ca mi chp:
).4
(
2
b
dd
ci hch
Vi: c - Khong cch gia cc khe, chn c = 3 mm.
i = 4032,39)17.4
503303,74(
3
2
khe.
- ng knh ng chy chuyn:
z
Gd
CX
Xc
....3600
.4
;
Vi: GX - lu lng lng trung bnh i trong on chng, kg/h. tnh phn
tnh ng knh on chng. GX = 1368,1272 kg/h.
X - khi lng ring trung bnh ca lng trong on chng,
X = 935,17 kg/m3
z - s ng chy chuyn, chn z = 1.
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N HC PHN CNG NGH HA HC Trang 35
C - tc cht lng trong ng chy chuyn, chn C = 0,15 m/s.
Vy: mdC 06,01.15,0.7748,909..3600
1272,1368.4
= 60 mm.
- Khong cch t mp di ng chy chuyn n a:
S1 =0,25.dC = 0,25.0,06 = 0,015 (m) = 15 (mm).
- Chiu cao ng chy chuyn trn a:
hC = (h1 +b +S) - h.
Trong : h - chiu cao mc cht lng bn trn ng chy chuyn:
h = 3 2)..85,1.3600
(Cd
V
Vi: V - Th tch cht lng chy qua.
V = hmG
X
X /5038,17748,909
1272,1368 3
h = m0114,0)06.0..85,1.3600
5038,1(3 2
= 11,4 mm
hC = (20 + 11,34 + 5) - 11,9 = 24,44 mm.
- Bc ti thiu ca chp trn a:
tmin = dch + 2.ch + l2
Vi: l2 = 12,5 + 0,25.dch, l khong cch nh nht gia cc chp.
Ly l2 = 35 mm.
tmin = 74,3303 + 2.2,5 + 35 = 114,3303 mm.
- Khong cch t tm ng chy chuyn n tm chp gn nht:
t1 = 122
ldd
chch
CC
Trong : C - B dy ng chy chuyn, chn C = 3 mm.
l1 - Khong cch nh nht gia ng chy chuyn v chp.
Chn l1 = 75 mm.
Vy: t1 = mm6652,147755,22
3303,743
2
60
4.2.2. Cc kt cu a phn chng.
- ng knh ng hi: dh = 50 mm
- S chp: n = 20 chp
- ng knh chp: dch = 74,3303 mm
- Chiu cao chp trn ng dn hi: h2 = 12,5 mm
- Khong cch t mt a n chn chp: S = 5 mm
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 36
- Chiu cao mc cht lng trn khe chp: h1 = 20 mm
- Chiu cao khe chp: b = 17 mm
- Khong cch gia cc khe: c = 3 mm
- S khe h ca mi chp: i = 40 khe
- ng knh ng chy chy chuyn: dC = 60 mm
- Chiu cao lp cht lng trn ng chy chuyn: h = 11,4 mm
- Khong cch t mp di ng chy chuyn n a S1 = 15 mm
- Chiu cao ng chy chuyn trn a: hC = 30,6 mm
- B dy ng chy chuyn: C = 3 mm
- B dy chp: ch = 2,5 mm
- Khong cch t tm ng chy chuyn n tm chp gn nht:
t1 = 147,6652 mm
- Khong cch gia hai tm chp: tmin = 114,3303mm
- Khong cch nh nht gia hai chp: l2 = 35 mm
- Khong cch nh nht gia chp v ng chy chuyn l1 = 75 mm .
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 37
PHN 3: TNH C KH THIT B CHNH
I. Tnh thn thit b chnh.
Thp chng luyn p sut kh quyn P = 1,5 at = 1,47.105 N/m2 l p sut
thp v trung bnh nn chn thn thp hnh tr hn (theo trang 360, [2]).
Chiu dy thn hnh tr lm vic di p sut P (cng thc XIII.8, trang 360,
[2]).
CP
PDS t
][2
.. m
Trong : Dt - ng knh trong ca thp, m.
- H s bn ca thnh hnh tr theo phng dc.
C H s b sung do n mn, bo mn v dung sai v chiu dy, m.
[ ]- ng sut cho php ca vt liu.
Tra bng XIII.9, trang 364, [2], ta thy thp X18H10T ph hp vi thn hnh tr
hn c dng vi thit b lm vic p sut thp v trung bnh (
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N HC PHN CNG NGH HA HC Trang 38
(1) [ k] = 26
6
/10.69,2071.6,2
10.540mN
(2) [k] = 26
6
/10.67,1461.5,1
10.220mN
Ta chn gi tr b nht tnh tip [] = 146,67.106 N/m2
Tra bng XIII.8, trang 362, [2]vi kiu hn tay bng h quang in, hn gip mi
hai bn ta chn h s bn mi hn h = 0,95.
I.2. Tnh P.
Trong thp l hn hp lng - kh nn p sut lm vic bng tng s p sut Pmt
hi v p sut thy tnh Pt ca ct cht lng.
Pmt = 1,5 at = 147150 N/m2.
p sut thy lc ca ct cht lng c xc nh:
Pt = g.1.Ht , N/m2 (cng thc XIII.10, trang 360, [2]:
Trong : t - Khi lng ring ca cht lng, kg/m3
m bo kh nng chu ng ca thp khi gp trng hp lm vic bt
thng ta ly t l khi lng ring ln nht ca cht lng trong thp, ngha l
t=W.
Ti nhit si 97oC ta tra c :
;
Nng phn khi lng tng ng y thp l:
= 0,1825 (phn khi lng)
Khi lng ring ca hn hp:
0011054,01,960
8175,0
85,718
1825,01
b
b
a
a
hh
xx
hh = t = 904,6896 kg/m3 .
+ Ht - Chiu cao ct cht lng, m (ly chiu cao ln nht = chiu cao thp)
Ht = Ntt(h + ) + 0,8 , m
Vi: Ntt : S a thc t, Ntt = 25,8999 a
h : Khong cch gia cc a, h = 0,35 m
: B dy ca a, chn = 0,003 m
Ht = 25,8999.(0,35 + 0,003) + 0,8 = 9,9423 m
Vy: Pt = 9,81.904,6896.9,9423 = 88237,962 N/m2
P = Pmt + Pt = 147150 + 88237,962 = 235387,962 N/m2
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 39
Vi vt liu bn, ta c:
50944,59195,0.962,235387
10.67,146.
][ 6h
P
nn ta b qua P mu s khi tnh S.
I.3. Tnh C.
C = C1 + C2 + C3 m
Trong : C1 H s b sung do n mn, xut pht t iu kin n mn vt
liu ca mi trng. y ta ly C1 = 1 mm, tnh cho thi gian lm vic t 15 20
nm, vi n mn vt liu l 0,05 0,1 mm/nm.
C2 - i lng b sung do bo mn khi nguyn liu c ht rn
chuyn ng vi vn tc ln, y C2 c b qua .
C3 - i lng b sung do dung sai ca chiu dy tm vt liu, vi
vt liu X18H10T th C3 = 0,22 mm (tra bng XIII.9, trang 364, [2])
Vy C = 1 + 0,22 = 1,22 mm
Do
S = mmmCPDt 81,100181,010.22,1
95,0.10.67,146.2
962,235387.7,0
].[2
. 36
I.4. Kim tra ng sut theo p sut th.
).(2
)].([ 01
CS
PCSD
2,1
C (cng thc XIII.26, trang 365, [2]:
Po: p sut th, c tnh:
P0 = Pth + Pt
Pth: p sut th thy lc, theo bng XIII.5, trang 358, [2] th Pth = 1,5.P
Pth = 1,5.235387,962 = 353081,943 N/m2
Pt : p sut thy tnh ca nc
Pt = .g.Ht = 960,1. 9,81.9,9423 = 93642,358 N/m2.
Po = 353081,943 + 93642,358 = 446724,201 N/m2
Ta c: VT = 95,0).22,181,1.(2
201,446724)].22,181,1(7,0[
= 514071,5605 N/m2
VP =2,1
10.67,146 6 = 122,225.106 N/m2 > VT
Vy S = 1,81 mm l tha mn, tuy nhin chu c ti trng ca thp v
tng tnh bn vng ca thp ta chn b dy thp l S = 4 mm.
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SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 40
II. Tnh y v np thit b.
Thng thng ngi ta dng y v np elip vi thit b c thn hn thng
ng chu p sut trong ln hn 7.104 N/m2. Trong trng trng hp thit k thp
chng luyn lm vic p sut kh quyn nn ta s dng y v np c g c dng
elip c ng knh trong l 0,7 m. Chn vt liu ca y v np ging nh vt liu
ca thn thp. Theo hnh XIII.11, trang 381, [2], ta c:
Chiu cao phn li y:
hb = 0,25.Dt = 0,25.0,7 = 0,175 m.
Chn chiu cao ca g l 25 mm.
B dy y v np thit b (cng thc XIII.47, trg 385, [2]:
Ch
D
Pk
PDS
b
t
hk
t
.2
..]..[8,3
.
, m
Trong h - h s bn ca mi hn hng tm, tra bng XIII.8, trang 362, [2]
chn h = 0,95.
k - H s khng th nguyn, chn k = 1.
C - i lng b sung, C = 0,00122 m.
V 30944,591..][
hkP
nn b qua P mu s khi tnh S.
Vy: S = 00184,000122,0175,0295,011067,1468,3
962,2353877,06
2
m=1,84 mm
Do: S - C = 1,84 1,22 = 0,62 < 10 nn thm 2mm vo gi tri S tnh trn.
Vy: S = 3,7 mm, an ton ta chn S = 4 mm.
Kim tra ng sut theo p sut thy tnh:
iu kin tha mn:
).(...6,7
)].(.2[ 02
CShk
PCShD
bh
bt
2,1
c , N/m2 (Cng thc XIII.49, trang 386, [2].
)00122,0004,0.(175,0.95,0.1.6,7
201,446724)].00122,0004,0.(175,0.27,0[ 2 62442034,98 N/m2
66
10.225,1222,1
10.67,146
2,1c
N/m2 >
Vy b dy ca y v np thp S = 4mm l tha mn.
III. Tnh b dy lp cch nhit.
trnh tn tht nhit cho mi trng xung quanh, m bo cho qu trnh
chng luyn t hiu sut cao nht th ta phi trang b cho thp chng luyn mt lp
cch nhit.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 41
Chn vt liu cch nhit l bng thy tinh c h s dn nhit nh:
= 0,0372 W/m.
Ta gi thit nh sau:
- Nhit khng kh: tkk = 25oC.
- Nhit bn ngoi lp cch nhit: t = 50oC.
- Xem y l qu trnh nhit n nh qua vch phng.
- m bo kh nng cch nhit cho ton thp ta chn nhit lm vic
trong thp l 100oC.
Nhit ti ring ra mi trng xung quanh:
q = t. , W/m2
Trong : t - hiu s nhit gia tng bn ngoi ca thit b vi mi
trng: t = 50 - 25 = 25oC.
- h s cp nhit t b mt thit b ra ngoi mi trng.
= 4.98,1 t (cng thc V.75, trg 24, [2]:
= 4274,425.98,1 4 W/m2. .
q = 25. 4,427 = 110,685 W/m2
Hiu s nhit gia nhit trong thp v nhit mt ngoi thp:
t1 = 100 - 50 = 50oC .
Mt khc ta c:
t1 = q. r
Vi : r l nhit tr tng cng, m2./W. c tnh:
r = r1 + r2 + r3
Trong :
- r1: Nhit tr lp cn, r1 = 0,387.10-3 m2./W. (Tra bng V.1, trang 4, [2]).
- r2: Nhit tr thnh thit b, r2 = / = 4.10-3/16,3 = 0,2454.10-3 m2./W.
- r3: Nhit tr lp cch nhit dy , r3 = / = /0,0372 m2./W
Ta c: r = t1/q = 50/110,685 = 0,4517 m2./W
Suy ra: r3 = r - r1 - r2 = 0,4517 0,387.10-3 - 0,2454.10-3 = 0,4511 m2./W
= r3.0,0372 = 0,01678 m = 16,78 mm.
m bo cch nhit tt ta chn lp cch nhit c b dy 20 mm.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 42
IV. Tnh ng knh cc loi ng dn.
ng knh ng dn (cng thc II.36, trang 369, [1]):
..3600
.4VD , m
Vi: V : lu lng th tch, m3/h
: tc trung bnh ca cht lng v kh (cho bng II.2, trang 369,
[1]).
IV.1. ng knh ng dn hn hp u vo a tip liu.
Nhit si ca hn hp u vo thp l 840C (tra bng I.2, trang 9, [1]) ta c:
)8084(80100
801008084
aaaa
= 731,2 kg/m3
)8084(80100
801008084
bbbb
= 969,2 kg/m3
Khi lng ring ca hn hp:
B
B
a
A
hh
xx
1
a, b: Khi lng ring ca tylic v nc
xA, xB: Nng phn khi lng ca tylic v nc.
001144,02,969
665,0
2,731
335,01
hh
hh = 873,91 kg/m3
Lu lng th tch cht lng chy trong ng:
V = )/(06,291,873
1800 3 hmG
hh
F
Hn hp t chy vo thp nn chn vn tc cht lng i trong ng l = 0,20
m/s.
Vy ng knh ng dn l:
)(60)(06,0.3600.20,0
06,2.4mmmD
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 43
IV.2. ng knh ng dn t thit b ngng t hi lu v thp.
Nhit ca lng hi lu l 78oC, khi lng ring ca lng hi lu tnh tng t
nh trn ta c:
= 736,9 kg/m3 ;
= 971,75 kg/m3
75,971
1,0
9,736
9,01
hh
= 755,15 kg/m3
Lu lng th tch cht lng chy trong ng:
)/(145,115,755
0345,631.37,1. 3 hmGR
Vhh
PX
Hn hp t chy vo thp nn ta chn = 0,25 m/s
Vy ng knh ng dn l:
04,0.3600.25,0
145,1.4
D (m) = 40 (mm).
IV.3. ng knh ng dn hi ra khi nh thp.
Lng hi i ra khi nh thp g = 1495,5518 kg/h. tnh phn tnh ng
knh on luyn.
Phn t lng trung bnh ca hi i ra khi nh thp:
MTB = 46.0,8 + 18.0,2 = 40,4 vC
Khi lng ring ca hi ra khi nh thp 78oC l:
)/(4028,1)78273.(4,22
273. 3mkgMTB
(Cng thc I.3, trang 5, [1]).
Lu lng hi i trong ng:
V = )/(12,10664028,1
5518,1495 3 hmgd
Chn vn tc hi i trong ng l: = 20 m/s .
Vy ng knh ng dn hi l:
)(3,137)(1373,0.3600.20
12,1066.4mmmD
IV.4. ng knh ng dn sn phm y.
Khi lng ring ca sn phm y 97oC tnh phn tnh c kh thit b
chnh: hh = 950,53 kg/m3.
Sut lng sn phm y l: GW = 1168,9655 kg/h.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 44
Lu lng th tch:
V = )/(23,153,950
9655,1168 3 hmG
hh
Chn vn tc cht lng i trong ng l: = 0,26 m/s.
Vy ng knh ng dn sn phm y:
)(41)(041,0.3600.26,0
23,1.4mmmD
IV.5. ng knh ng dn vo y thp un si li.
Sut lng hi vo y thp l: = 928,9508 kg/h.
Vi: [ ( ) ]
( )
( )
( ) = 0,6944 kg/m3.
V =
= 1337,7748 m3/h.
Ta chn vn tc hi vo y thp l: w = 25 m/s.
D =
= 0,138 m = 138 m.
IV.6. ng knh dn cht lng y thp.
Sut lng cht lng vo ni un l: = 2097,9163 kg/h. tnh phn
ng knh on chng.
= 0,053 phn mol = 0,1251 phn khi lng.
= 921,2711 kg/m3
V =
= 2,2772 m3/h
Chn vn tc cht lng vo ni un l: = 0,2 m/s.
D =
= 0,0635 m = 63,5 mm.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 45
V. Chn bch.
Mt bch l b phn quan trng dng ni cc phn ca thit b cng nh ni
cc b phn khc vi thit b. V thp lm vic p sut kh quyn nn ta chn kiu
bch lin.
V.1. Bch ni thn thit b, np v y.
Theo bng IX.5, trang 170, [2] ng vi Dt = 700 mm, khong cch gia hai a
l 350 mm th s a gia hai mt bch lin tip l 4. Vi 25,8999 a ta c tt c l 8
b bch ni thn, np v y.
Theo bng XIII.27, trang 419, [2] ta chn bch kiu 4 ni cc on thn thp,
ni np v ni y. m bo bch chu c khi gp trng hp lm vic bt
thng ta chn p sut Py bng p sut th P0 tnh trong phn c kh thit b
chnh, Py 0,3.106 N/m2
S liu ca bch c cho bng sau:
Py.106
N/m2 Dt
(mm)
Kch thc ni (mm) Kiu bch
D Db D1 D0
Bulng 4
db z h h1
0,3 700 830 780 750 711 M20 24 20 3
Gia hai bch c mt lp lt b mt m bt kn m bo kn ca thp,
kch thc ca b mt m bt kn (Tra bng XIII.31, trang 433, [2]), ng vi
Dy=700 mm ta c D2 = 750 mm, D4 = 730 mm.
V.2. Bch ni ng dn vi thit b.
ni cc ng dn vi thn thit b ta dng kiu bch lin bng kim loi en.
Tra bng XIII.26 trang 409 S tay QTTB tp 2 ta c bng s liu sau:
Py.106
N/m2
Dy (mm)
Kch thc ni (mm) Kiu bch
Dn D D D1
Bulng 1
db z h
0,25 0,6
40 45 130 100 80 M12 4 14
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 46
Py.106
N/m2
Dy (mm)
Kch thc ni (mm) Kiu bch
Dn D D D1
Bulng 1
db z h
0,25 0,6
50 57 140 110 90 M12 4 14
0,25 0,6
70 76 160 130 110 M12 4 14
0,25 0,6
150 159 260 225 202 M16 8 16
ng dn c ni vi thit b thng qua mi ghp tho c, do ta phi
dng on ng ni, l on ng ngn c mt bch. Kch thc chiu di ng ni ta
chn bng XIII.32, trang 434, [2]:
Dy (mm) 40 50 70 100 150
l (mm) 100 100 110 120 130
VI. Tnh ti trng ca thp.
Khi lng ca thp bao gm tng khi lng ca thn thp, y, np, lp
cch nhit, cht lng trong thp, bch v a.
VI.1. Khi lng ca thn thp.
Tnh theo cng thc: ).(4
.. 221 tn DD
HG
, kg .
Trong : H: Chiu cao thp cha k y v np.
H = Ntt(h + )
+ h - Khong cch gia cc a, h = 0,35 m.
+ - B dy ca a, chn: = 0,003 m.
H = Ntt(h + ) = 25,8999.(0,35 + 0,003) = 9,1427 m.
: Khi lng ring ca thp X18H10T, = 7900 kg/m3
Dt : ng knh trong ca thp, Dt = 0,7 m.
Dn : ng knh ngoi ca thp
Dn = Dt + 2.S = 0,7 + 2.0,004 = 0,708 m.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 47
Vy: kgG 6514,638)7,0708,0(4
.7900.1427,9 221
VI.2. Khi lng ca y v np elip c g.
Tra bng XIII.11, trang 384, [2] ta c khi lng ca y v np elip c g
ng vi ng knh trong ca thp 0,7 m, chiu dy y v np 4 mm, chiu cao g
25 mm l:
G2 = 2.19 = 38 kg.
VI.3. Khi lng ca cht lng trong thp.
Xem cht lng chim y thp, ta s b qua khi lng ca cc ng chy
chuyn v cc chp.
G3 = V.hh (kg)
Trong : V - Th tch cht lng.
V = 5167,34
1427,9.7,0.
4
.. 22
HDt m3 .
hh : khi lng ring ca cht lng, ly khi lng ring ln nht,
hh = 904,6896 kg/m3. tnh phn tnh thn thit b chnh.
Vy: G3 = 3,5167.904,6896 = 3181,523 kg.
VI.4. Khi lng ca cc a.
n gin ta coi a l mt tm trn khng b khot l c chiu dy nn khi
lng ca 25,8999 a l:
G4 = 25,8999. D.4
t2.. = kg6024,2827900.003,0.7,0.
4.258999 2
VI.5. Khi lng lp cch nhit.
B dy lp cch nhit l 20 mm.
Khi lng bng thy tinh bao quanh thn thp, c phn g ca y v np:
m1 = )025,0.2).()02,0.((4
.22 HDD nn
= kg41)05,01427,9).(708,0728,0.(4
.200 22
Khi lng phn bng thy tinh ph y v np:
m2 = 2.Fy.0,02.
Ta c: Fy = hg.Dt.3,14 + 4 .(
)
Vi: a = b = Dt/2 = 0,35 m
C = hb = 0,175 m
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 48
hg = 0,025
Thay s vo ta c:
Fy = 0,025.0,7.3,14
+ 4. . (
)
= 0,5866 (m2)
m2 = 2.0,5866.0,02.200 = 4,6928 kg.
Vy khi lng lp bng cch nhit:
G5 = m1 + m2 = 41 + 4,6928 = 45,693 kg .
VI.6. Khi lng ca bch.
- Khi lng cc bch ni thn, np v y:
Mt cch gn ng ta c khi lng mt bch n (khng tnh n cc l khot
vn bulng nn b qua khi lng ca cc bulng):
m = kghDD 7445,227900.02,0.4
).711,083,0(..4
).( 222
0
2
Dng 8 b bch = 16 bch n, nn khi lng ton b 8 b bch l:
m1 = 16. m = 16.22,7445 = 363,912 kg.
Khi lng cc bch ni ng dn vi thn thp:
- Bch ni ng dn hn hp u vo thp:
kghDDm nd 42,17900.014,0).057,014,0(4
.)..(4
2222
Vy khi lng cp bch ny:
m2 = 2.1,42 = 2,84 kg
- Bch ni ng dn hi ra khi nh thp:
m3 = kg4,87900.016,0).159,026,0.(4
.2 22
- Bch ni ng dn dung dch y:
m4 = 2. kg58,27900.014,0).045,013,0.(4
22
- Bch ni ng dn lng hi lu:
m5 = 2. kg58,27900.014,0).045,013,0.(4
22
- Bch ni ng dn hi t:
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 49
m6 = 2. kg4,87900.016,0).159,026,0.(4
22
- Bch ni ng dn nc ngng:
m7 = m5 = 2,58 kg
Vy tng cc loi bch ni thn, np, y v ng dn:
G6 = m1 + m2 + m3 + m4 + m5 + m6 + m7
= 363,912 + 2,84 + 8,4 + 2,58 + 2,58 + 8,4 + 2,58
= 391,292 kg.
Tng khi lng ton thp:
G = G1 + G2 + G3 + G4 + G5 + G6
= 638,6514 + 38 + 3181,523 + 282,6024 + 45,693 + 391,292
= 4577,7618 kg.
VII. Chn tai treo, chn .
VII.1. Chn tai treo.
Ta dng 4 tai treo kiu VII, hnh XIII.21, trang 436, [2] do ti trng trn mt tai
treo:
G =
N9608,11226
4
81,9.7618,4577
Theo bng XIII.36, trang 438, [2] th ta chn tai treo c cc s liu sau:
Ti trng cho php trn mt tai treo: Gcp = 25 000 N > G
B mt : F = 173.10-4 m2
Ti trng cho php ln mt b mt :
qcp = 14500000173,0
25000
F
Gcp N/m2
Ti trng thc t ln mt b mt :
q = 2717,6489570173,0
9608,11226
F
G N/m2 < qcp = 1,45.10
6 mm.
L B B1 H S l a d
150 120 130 215 8 60 20 30
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 50
VII.2. Chn chn .
Ta chn chn kiu III, trang 436, [2] vi ti trng trn mt chn l
G=11226,9608 N nn ta chn chn c cc s liu sau:
Ti trng cho php trn mt chn: Gcp = 25 000 N > G
B mt : F = 444.10-4 m2
Ti trng cho php ln mt mt :
qcp =
= 2/5600000
000444,0
25000mN
Ti trng thc t ln mt chn :
q = 2/250000000444,0
9608,1126mN < qcp = 320 000 mm
L B B1 B2 H h s l d
250 180 215 290 350 185 16 90 27
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 51
PHN 4: TNH THIT B PH
I. Tnh ton thit b ngng t hi lu.
nng cao kh nng phn tch cc cu t trong qu trnh phn tch ta cn
to ra qu trnh tip xc gia pha lng v pha hi, diu ny c thc hin trong
thp. nng cao tinh khit ca sn phm nh v trnh hin tng kh a
nhng a trn cng ta cho mt phn sn phm nh hi lu tr li thp, iu ny
c thc hin nh thit b ngng t hi lu. y l ni xy ra qu trnh trao i
nhit gia hi i ra t nh thp vi nc lm lnh, lng nhit trao i y ng
bng nhit lng cn cung cp ha hi lng hi i ra khi nh thp. Trong iu
kin ny ta dng thit b ngng t kiu ng chm, h thng ny c u im l gn,
chc chn, t tn kim loi, b mt truyn nhit ln, d kim tra quan st, sa cha,
lm v sinh.
Trong thit b ny, tc nhn nng l hi i ra t nh thp (ru tylic) c
tinh khit cao nn ta cho i bn ngoi chm ng, cn tc nhn lm lnh l nc lnh
ta cho i bn trong cc ng d lm v sinh khi cc cht bn bm trong ng.
m bo truyn nhit trit , tit kim lng nc ta cho hai lu th chuyn ng
ngc chiu, hi i t trn xung, nc i t di ln .
y ta tnh ton thit b ngng t hon ton lng hi i ra khi thp.
Nhit ca hi l 78oC .
Nhit u ca nc c chn 25oC.
Nhit cui ca nc c chn 45oC, trnh hin tng cc mui d kt
ta v ng cn li trn b mt trong ng.
Trong phn cn bng nhit lng cho thp ta tnh lng nc cn thit
ngng t hon ton hi ra khi nh thp l: Gn2 = 991,0912 kg/h.
Lng nc lnh cn dng cho thit b ngng t hi lu Gn1 = 31336,7677.
Hiu s nhit trung bnh gia hai lu th chuyn ng ngc chiu c
xc nh theo cng thc V.8 trang 5 S tay QTTB tp 2:
2
1
21
lnt
t
ttt
, .
Trong t1 v t2 l hiu s nhit ln v nh ca hai lu th, . y ta
c:
t1 = 78 - 25 = 53 0C, t2 = 78 45 = 33
0C
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 52
Nn: Ct 0213,42
33
53ln
3353
Nhit trung bnh ca nc lm lnh c tnh theo cng thc V.21, trang 10,
[2]:
t = T1 - Cto787,35213,4278
I.1. i vi pha hi.
H s cp nhit c tnh theo cng thc V.100, trang 28, [2]:
1 = 41
32
..
....15,1
Ht
gr
, W/m2.
Trong : r: n nhit ngng, r = r = 284,6888 kcal/kg = 1191,65 J/kg ( tnh
phn tnh ng knh on luyn).
: Khi lng ring ca lng ngng, = 755,15 kg/m3.
H: Chiu cao ng, chn H = 2 m.
: H s dn nhit ca lng ngng, W/m., c xc nh theo
cng thc I.32, trang 123, [1]:
= 3...M
CA P
, W/m.
Vi: A H s ph thuc mc lin kt ca cht lng. A = 3,58.10-8,
v cht lng lin kt (nc, ru tylic).
CP : Nhit dung ring ng p ca cht lng, J/kg., xem cht
lng l ru tylic nn CP78 = 3,195 kJ/kg..
= 755,15 kg/m3 tnh trn.
M: Phn t lng trung bnh ca lng ngng.
M = 0,78.46 + (1-0,78).18 = 39,84 vc
Vy: = 2303,084,39
15,755.15,755.3195.10.58,3 38 ,W/m.
: nht ca lng ngng, = 0,4233.10-3 N.s/m2
Ta c:
= 0,591 Cp
= 0,435 Cp
= 0,4506.10-3 Ns/m2.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 53
ttt n 1 T1 :hiu s gia nhit ngng tn v nhit mt tng
tip xc vi hi ngng, tn = 78 0C, ly tT1 = 75
0C.
t1 = 30C .
Vy h s dn nhit:
1 = 0381,26942.3.10.4506,0
)2303,0.(81,9.)15,755.(1191650.15,1 4
3
32
(W/m2.)
Nhit ti ring v pha hi ngng t:
q1 = 1.t1 = 2694,0381.3 = 8082,1143 W/m2
I.2. i vi pha nc lm lnh.
H s cp nhit tnh theo cng thc V.33, trang 11, [2]:
d
Nu
.2
Trong : : H s dn nhit ca nc nhit trung bnh 35,7870C:
Ta c:
= 0,597 W/m..
= 0,642 W/m..
= 0,6332 W/m..
d: ng knh ng truyn nhit, chn d = 0,03 m.
Nu: Chun s Nuyxen, c tnh theo V.40 trang 14 S tay QTTB
tp 2.
Nu = 25,043,08,0
1 )Pr
Pr.(Pr.Re..021,0
t
Vi: Prt: Chun s Pran ca dng tnh theo nhit trung bnh ca
tng. V chnh lch nhit gia tng v dng nh nn 1Pr
Pr
t
.
Re: Chun s Renoydn, gi s nc chy ri vi Re = 104
Pr: Chun s Prant, tnh theo V.35 trang 12 S tay QTTB tp 2:
.Pr P
C
Vi: CP: Nhit dung ring ng p ca nc 35,7870C, ta c:
CP=4175,9825 J/kg.
: nht ca nc 35,7870C.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 54
Tra bng ta c: = 0,757.10-3 N.s/m2
: H s dn nhit ca nc 35,7870C, = 0,6332 W/m.
Pr = 56332,0
10.757,0.9825,4175 3
1: H s hiu chnh tnh n nh hng ca t s gia chiu di l
v ng knh d ca ng, theo bng V.2 th 1 = 1.
Nu = 0,021.1.(104)0,8.50,43 = 66,4931
Vy 2 = 4477,140303,0
6332,0.4931,66 W/m2.
Nhit ti ring v pha nc:
q2 = 2.t2
t2 l hiu s nhit gia nhit thnh bn trong tng ng vi nhit
trong dng nc, chn t2 = 50C.
q2 = 1403,4477.5 = 7015,5885 W/m2.
q =
2
21 qq(8082,1143 + 7015,5885)/2 = 7548,8514 W/m2
I.3. S ng truyn nhit v cch sp xp.
B mt truyn nhit:
F = q
rRP
q
Q X ).1.( m2
Vi: r - n nhit ngng t ca sn phm nh, r = 849750 J/kg
F = 7637,463600.8514,7548
849750).137,1.(0345,631
(m2)
S ng cn dng:
n = 2482.03,0.
7637,46
..
Hd
F(ng).
Ly s ng l 241 ng. Theo bng V.11, trang 48, [2], ng vi s ng l 241 v
sp xp theo hnh 6 cnh u th ta b tr 241 ng thnh 8 vng 6 cnh vi s ng
trn ng cho chnh ca hnh 6 cnh l 17 ng, s ng trong mi hnh vin phn
dy th nht l 4 ng v tng s ng trong cc hnh vin phn l 24 ng.
Theo cng thc V.140, trang 49, [2] th ng knh trong ca thit b c tnh:
D = t.(b -1) + 4.d , m
Vi: d: ng knh ngoi ca ng truyn nhit.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 55
d = 0,03 + 0,0015.2 = 0,033 m
t: Bc ng, t = 1,2.d = 0,0396 m
b: S ng trn ng cho chnh ca hnh 6 cnh, b = 17
D = 0,0396.(17 - 1) + 4.0,033 = 0,7656 m.
Chn D = 0,8 m.
Vy thit b ngng t c ng knh trong l 0,8 m, gm 241 ng xp theo hnh
lc gic u gm 8 vng. Mi ng di 2 m, ng knh trong 0,03 m, dy 0,0015 m.
II. Thit b gia nhit nhp liu.
- un si dung dch nhp liu a vo thp ta dng hi nc bo ha
c p sut tuyt i l 1,5 at
- ng i ca lu cht: Hi nc bo ha i ngoi ng cn dng nhp liu
i trong ng.
Dng nng: 110,7oC(hi bo ha) 110,11736oC (lng ngng)
Dng lnh: 84oC(lng si) 25oC (dung dch)
- Chnh lch nhit u vo: tv = 110,7 84 = 26,7oC
- Chnh lch nhit u ra: tr = 110,7 25 = 85,7oC
- Chnh lch nhit trung bnh:
- Lng hi cn cung cp, tnh phn cn bng nng lng.
D1 = 200,3888 kg/h
- Chn thit b c s ng n = 187 ng, ng knh ng 20x2mm, xp theo kiu
vng trn.
II.1. H s cp nhit t hi t n thnh ng.
H s cp nhit cho b mt ng ng c xc nh theo cng thc:
1 = 4
1
32
..
....15,1
Ht
gr
, W/m2. (Cng thc V.100, trang 28, [2])
Trong : r: n nhit ha hi, r = 2232,18 kJ/kg ( tnh phn cn bng
nng lng).
Chn t = 2oC.
: Khi lng ring ca nc 110,7oC l 949,975 kg/m3.
H: Chiu cao ng, chn H = 2 m.
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 56
: H s dn nhit, hi nc 110,7oC c = 0,684605 W/m..
: nht ca hi nc 110,7oC, = 254,715.10-6 N.s/m2
Vy h s cp nhit:
1 = 21,102142.2.10.254715,0
)684605,0.(81,9.)975,949.(2232180.15,1 4
3
32
(W/m2.)
II.2. H s cp nhit t thnh ng n dung dch nhp liu.
Nhit trung bnh ca dng lnh:
Ti nhit ny ta c cc thng s vt l nh sau:
{
(
)
( )
(
)
(
)
Trong : = 1541,0)405,54(20
004,0157,0 (kcal/m.h.
oC) = 0,1792 W/m.
Tnh chun s Reynold:
( [ ])
+ d - ng knh ng.
+ n - S ng.
lu th
chuyn ng dng.
Ch chy dng, ta p dng cng thc tnh Nu:
(
)
( [ ])
Chun s Pr c xc nh theo cng thc V.35, trg 12, [2]:
Chn (
)
l = 1 (tra bng V.2, trang 15, [2])
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 57
Vi: l Kch thc xc nh, l = d = 0,02 m.
H s dn n th tch. Tra bng ti nhit 54,5oC ta c:
=1,1953.10-3.
( ) = 251581,88
Nu = 0,15.1.259,850,33.10,60,43.251581,880,1.1 = 9
Suy ra h s cp nhit t thnh trong ng n dung dch:
( [ ])
( )
II.3. H s truyn nhit.
(
)
II.4. B mt truyn nhit.
( )
II.5. Chiu di thit b.
Chn s ng n = 187 ng.
( )
III. Ni un.
III.1. Chn thit b un si y thp.
Chn thit b un si y thp l ni un Kettle. t ni un ring bit vi thp.
Ni un tip nhn dng lng i ra bn di thp. Nh hi nc bo ha c nhit
cao hn nhit dng lng trn nn s gip ha hi mt phn lng y thp mc
ch to hi cho phn ny c iu kin i ln nh thp.
ng truyn nhit c lm bng thp X18H10T, kch thc ng 32 x 3:
ng knh ngoi: dn = 38 mm = 0,038 m
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 58
B dy ng: t = 3 mm = 0,003 m
ng knh trong: dt = 0,032 m
Hi t l hi nc 1,5 at i trong ng 32 x 3. Tra bng 1.251, trang 314,
[1]:
Nhit ha hi: OH2
r = rn = 2232,18 kJ/kg
Nhit si: OH2
t = tn = 110,7 oC
Dng sn phm ti y c nhit :
Trc khi vo ni un (lng): tS1 = 84 oC
Sau khi c un si (hi): tS2 = 97 oC
III.2. iu kin nhit ca qu trnh.
Dng nng : 110,7oC 110,7oC
Dng lnh : 84oC 97oC
Chnh lch nhit u vo : t1 = 110,7 84 = 26,7oC.
Chnh lch nhit u ra : t2 = 110,7 97 = 13,7oC.
= 19,4824oC
III.3. Nhit ti.
QD2 = 1928942,584 kJ/h ( tnh phn cn bng nhit lng).
III.4. Xc nh h s cp nhit ca dng lu cht i ngoi ng.
Xc nh chun s Renold khi hi ngng mt ngoi ng nm ngang:
(Cng thc V.58, trang 28, [2])
nhit 110,7oC ta c:
nht ca nc ngng, (N/m2).
KJ/kg (nhit ha hi)
Sn phm y l nc nn tnh h s cp nhit ta c cng thc:
t: Hiu s nhit . Chn t = 5.
p: p sut tuyt i trn mt thong. p = 1,5at = 147150 N/m2.
III.5. H s cp nhit ca hi t trong ng.
Ti nhit ca dng nng: 110,7oC ta c:
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 59
: Khi lng ring ca nc ngng = 949,975 kg/m3
*: Khi lng ring ca hi nc * = 1,11 kg/m3
= 0,0568N/m (Sc cn b mt).
Chun s Nuselt:
(
)
(
)
Chun s Reynolds:
Chn Ksb = 400 (W/m2.)
H s: C = 1,26; l/d = 50 225, chn l/d = 50.
Do ta c:
(
)
H s cp nhit t hi nc n thnh ng:
III.6. Xc nh h s truyn nhit.
( )
III.7. B mt truyn nhit.
III.8. Chiu di thit b.
Chn s ng n = 187 ng.
( )
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 60
IV. Thit b lm lnh sn phm nh.
ng i ca dng lu cht: Nc lm ngui i trong ng, sn phm nh i
ngoi ng.
Dng nng: 78oC 35oC
Dng lnh: 45oC 25oC
Chnh lch nhit u vo: tv = 78 45 = 33oC
Chnh lch nhit u ra: tr = 35 25 = 10oC
Chnh lch nhit trung bnh:
Chn ng tiu chun c ng knh l 25 x 2 mm, s ng n = 37.
IV.1. H s cp nhit t dung dch n thnh ng.
Nhit trung bnh ca dng nng: ttb2 = (78 + 35)/2 = 56,5oC.
Ti nhit ny ta c cc thng s dng nng nh sau:
{
H s cp nhit c tnh theo cng thc V.100, trang 28, [2]:
, W/m2.
Trong : r - n nhit ngng, r = 284,6888 kcal/kg = 1191,65 kJ/kg ( tnh
phn tnh ng knh on luyn).
Vy h s dn nhit:
( ) ( )
, W/m2.
IV.2. H s cp nhit t thnh ng n nc.
H s cp nhit tnh theo cng thc V.33, trang 11, [2]:
d
Nu
.2
-
SVTH: V Trng Qun MSSV: 11254511 Lp: HHD7 GVHD: Cao Thanh Nhn
N HC PHN CNG NGH HA HC Trang 61
Nhit trung bnh ca dng lnh: ttb1 = 35oC.
Ti nhit ny ta c cc thng s vt l dng lnh nh sau:
{
Lng nc cn gii nhit: Gn = 991,0912 kg/h. tnh phn cn bng nhit
lng.
d: ng knh ng truyn nhit, chn d = 0,03 m.
Nu: Chun s Nuyxen, c tnh theo V.40 trang 14 S tay QTTB
tp 2.
Nu = 25,043,08,01 )Pr
Pr.(Pr.Re..021,0
t
Vi: Prt: Chun s Prant ca dng tnh theo nhit trung bnh ca
tng.V chnh lch nhit gia tng v dng nh nn 1Pr