gmp supplementary water
TRANSCRIPT
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Project co-financed by
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Supplementary ModuleSupplementary Module
GMP Workshop Kuala Lumpur 14-16GMP Workshop Kuala Lumpur 14-16
Prepared by :Haryanto Susilo - IndonesiaSurachai Piyayodilokchai - ThailandStephanie Wong Choong Moy - Malaysia
Approved by :Asean Cosetic !MP Tea
GMP SUPPLEMENTARY TRAININGGMP SUPPLEMENTARY TRAININGMODULEMODULE
WAT"# $%# C%SM"TICWAT"# $%# C%SM"TIC&S"'&S"'
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Project co-financed by
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Implementing Agency Supplementary
Introduction
Water containants
Sources o( )aterWater treatent
Water puri*cation engineering
Water testing Inspection o( )ater treatent plants
#e(erences
C%+T"+T %$ P#"S"+TATI%+
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INTRODUCTION
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!o de"#ne the type o" $ater used as
the ma#n %omponent o" the
%osmet#% "ormula $#th the r#&ht'ual#ty $#th respe%t to the %hem#%al
and m#%ro(#olo%al %ontent to
prevent %ross %ontam#nat#on)
%,"CTI."
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Project co-financed by
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European Committeefor Standardization
Implementing Agency Supplementary
/ike any starting aterial0 )ater ust/ike any starting aterial0 )ater ustcon(or to !ood Manu(acturing Practicecon(or to !ood Manu(acturing Practice
It ust be 1potable2 and inially coplyIt ust be 1potable2 and inially coply
)ith the 3uality o( the national standard o()ith the 3uality o( the national standard o(drinking-)aterdrinking-)ater Systes ust be properly aintained toSystes ust be properly aintained to
avoid containantsavoid containants Speci*cations and periodic testing isSpeci*cations and periodic testing is
re3uiredre3uired Monitoring record is neededMonitoring record is needed
,ASIC P#I+CIP/"S
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Project co-financed by
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European Committeefor Standardization
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Types o( )ater used in cosetic processes are as (ollo)s:Types o( )ater used in cosetic processes are as (ollo)s:
$or product:$or product:
4545 Tap )ater con(oring to national standardTap )ater con(oring to national standard
6565 Puri*ed )ater 7Puri*ed )ater 7deionideioni8ed8ed,, reverse ososisreverse ososis9 (or9 (orcosetic productioncosetic production
$or cleaning:$or cleaning:
4545 So(tened )aterSo(tened )ater
$or rinsing: sae 3uality as (or the product$or rinsing: sae 3uality as (or the product
4545 Water (or *nal #inseWater (or *nal #inse$or sanitation:$or sanitation:
4545 SteaStea
WAT"# TP"
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Project co-financed by
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WATER
CONTAMINANTS
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Project co-financed by
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+o )ater is (ree (ro containants
Containant groups: Cheical copounds Physical copounds Solids !ases Micro-organiss 7algae0 proto8oa0 bacteria9
Mineral containants : Calciu and agnesiu
Iron and anganese Silicates Carbon dio;ide Hydrogen sul*de
WAT"# C%+TAMI+A+TS 749
Phosphates Copper Aluiniu Heavy etals +itrates
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WAT"# C%+TAMI+A+TS 769
Treatent depends on )ater
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T,I'IT
Turbidity ay coe (ro:
45 Silt0 clay0 and suspended aterials
65 Sall particles include BcolloidsB
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Waterhardness
classifcation
mg/L or ppmas CaCO
3
So(t -@
Moderate @4-46
Hard 464-4D
.ery hard E 4D
WAT"# HA#'+"SS
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Source o( ra) )aterSource o( ra) )ater
4545 #ain )ater#ain )ater
6565 Sur(ace or ground )aterSur(ace or ground )ater=5=5 Well or boreholeWell or borehole
>5>5 Municipal or civil F 1tapMunicipal or civil F 1tap
)ater2)ater2?5?5 Purchased in bulkPurchased in bulk
WAT"# S%C"S
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Well constructionWell construction
4545 Inspect e;posed parts o( the )ellInspect e;posed parts o( the )ell
6565 'epth o( )ell'epth o( )ell
Check:Check:
4545 +earby septic systes+earby septic systes
6565 Ha8ardous aterials usageHa8ardous aterials usage7pesticides0 (ertili8ers0 etc97pesticides0 (ertili8ers0 etc9
=5=5 11Potability2Potability2
>5>5 Well aintenanceWell aintenance
W"// WAT"#
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Project co-financed by
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STORAGE
OF WATER
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4545 May be re3uired prior to pre-treatentMay be re3uired prior to pre-treatent
6565 Check aterial o( constructionCheck aterial o( construction concrete0 steel are acceptable but checkconcrete0 steel are acceptable but check
corrosioncorrosion plastics or plastic linings ay leachplastics or plastic linings ay leach
=5=5 Check coverCheck cover to keep out insects0 birds and anialsto keep out insects0 birds and anials
>5>5 Check disin(ection practicesCheck disin(ection practices
#AW WAT"# ST%#A!"S
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THE WATER TREATMENTS
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Project co-financed by
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WAT"# T#"ATM"+T !&I'A+C"
The (ollo)ing should be onitored : Sources o( )ater Treatent procedures Water treatent e3uipent Monitoring records re3uired
Water treatent guidance All )ater-treatent systes should be
subGect to: planned aintenance veri*ed onitoring
Maintenance )ork should be
docuented
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Project co-financed by
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45 'isin(ection 7 i5e5 chlorination 9
65 $locculationcoagulation 7i5e5 by alu9
=5 $iltration through ulti-edia *lter
7gravel-sand-carbon9 to 4 icron
>5 $iltration through *lter si8e o( 4 icron
?5 #e-disin(ection 7i5e5 chlorination toeliinate gers9
P#"-T#"ATM"+T !&I'A+C"
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1$
Project co-financed by
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Activated-Carbon 7AC9 $iltration or ,isulphite
CH/%#I+" #"M%.A/
raw water in S trap to sewer
Water iskept
ir!"atin#
to waterso$tener% DI p"ant
artrie'"ter
( )iro)eters
ati*ate&ar+on'"ter
spra, +a""
+reak tank
air+reak to
&rain
entri$!#a" p!)p
air '"ter
-oatoperate&
*a"*e san&'"ter
e.ess water re,"e&$ro) &eioniser
NOTE /
45AC reoveschlorine butbacteria can thengro)
65AC *ltration can
reove organicipurities
=5,isulphite leavessulphate residuesbut is anti-icrobial
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Project co-financed by
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(r#ne and salt tank
(r#ne
*hard* $ater
#n
+eol#te $ater so"tener-e,%han&es-a and M& "or Na
dra#n
*so"t* $ater to de#on#ser(y pass valve
WAT"# S%$T"+"#
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Water treatent roo
";ternal ra) )aterstorage
WAT"# T#"ATM"+T C%MP/"
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Project co-financed by
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WATER
PURIFICATION
ENGINEERING
#everse ososis syste
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To e;aine the basic technology andre3uireents (or:
45Water treatent systes65Storage re3uireents
=5Sapling and testing
>5Microbial liits0 disin(ection
%,"CTI."S
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There should be:
proper pipe slope to avoid stagnation andcan be drained easilyJ
Proper *ttings K connections that can beeasily cleaned and saniti8edJ
constructed o( suitable aterials such aspolyethylene aterial0 stainless steel0 etc5
)ater circulation
non-return valves 7+#.9
WAT"# SST"M '"SI!+
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Project co-financed by
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$urther )ater treatent puri*cation stagesdo)nstrea o( the pre-treatent syste :
Pre - disin(ection - Locculation
$iltrationSo(tening colun'isin(ection'e-ioni8ation Syste#everse ososis plus deioni8ation
&. syste/ooping o( )ater
WAT"# PI$ICATI%+ STA!"S
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Project co-financed by
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There should be no dead legs
Water scours deadleg
I( '6? Kdistance isgreater than
?0 )e
havea dead legthat is too
long5
Deadleg section
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Project co-financed by
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=5 The )ater iscontainated as it passes
through the valve
65 In ,all valves0,acteria can gro))henthe valves are closed
45 ,utterLy valves are betterthan ,all valves
Stagnant
)aterinside valve
WAT"# SST"M '"SI!+ 769
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Project co-financed by
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Cationic column Anionic column
Hygienic pump
Outlets or storage
O!one generator
"V lig#t
HCl $aOH
%luates to
neutrali!ation
plant
Air &rea' to sewer
Drain line
(rom water so(tener
Waterust bekeptcirculating
)
2
*+,
-
)
2
*+,
-
.eturn to de/ioniser
Cartridge
(ilter , 0m
Cartridge
(ilter ) 0m
'"-I%+IN"# SCH"MATIC
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Project co-financed by
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'"-I%+IN"# %P"#ATI%+
0i"ter position Opene& *a"*es 1"ose& *a"*es
Services H %peration 40> 60=0?
,ack)ash 60= 40>0?
#insing 40? 60=0>
1ar+on 0i"ter 2a"*e Position
0i"ter position Opene& *a"*es 1"ose& *a"*es
Services H %peration @0O04 A0D04404604=04>
,ack)ash A0D04 @0O04404604=04>
Cation *lter regeneration A04604=04> @0D0O04044
,ack)ash A0D04 @04404604=04>
#insing @044 A0D0O0404404604=04>
1ation 0i"ter 2a"*e Position
0i"ter position Opene& *a"*es 1"ose& *a"*es
Services %peration 4?04D04O 4@040606406606=
,ack)ash 4@0404O 4?04D0606406606=
Anion *lter regeneration 4@06406606= 4@0404D04O
,ack)ash 4@0404O 4?0606406606=
#insing 4?06 4@0404D04O06406606=
Anion 0i"ter 2a"*e Position
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Project co-financed by
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raw water
Hig# pressure
Feedwater
under
pressure
.e
1ect
wate
r
Se
m
i/pe
rmea&
le
mem&
ran
e
2e
rmeate
wate
r
drain or recycle
3ow pressure
uri(ied water
#"."#S" %SM%SIS TH"%#
#everse ososis ay beused to:
puri*ed )ater
(eeding o( distillation unitsor ultra-*ltration units
)ater (or *nal rinse
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#% SCH"MATIC 'IA!#AM
DRINE TAN3
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.ran%h
.ran%h
2nd stage &u((er tan'
Cartridge
(ilter ) 0m
Second stage .O cartridge
First stage (iltrate (eeds second stage .O
wit# e4cess &ac' to )st stage &u((er tan'
)ststage
re1ectconcentrate
Air &rea'
to sewer
Second stage re1ect water goes &ac' to (irst stage &u((er tan'
Second stage .O water
meets #armacopoeia
standards Outlets or storage
)st stage &u((er tan'
Water (rom so(tener or de/ioniser
Water returns to )st stage &u((er tan'
Hygienic pump
First stage .O cartridge
Hig# pressure
pump
6-STA!"S #% SCH"MATIC
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???????????
1 S!
2 N/
ML!M/3 -LMN
M-5N-35!5/G
L!5
7G7 P5SS5 PMP
5 n#t10 m89h
P25M23!2LN2
-4N-2N!
53!2LN2
S/S
L P 7 P
FLFL
5-:-L LN
/ra#n
/ra#n
-P !3NK
-L3NNG LN
m
1;1
- ondu% t #v # t y
M eter
Na7 05 1+orally open2 and 1norally closed2
valves
I+SP"CTI%+ 7@9
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Project co-financed by
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#"$"#"+C"S
45 AS"A+ !uidelines (or Cosetic !MP 76=9
65 WH% "'M0 Suppleentary Training Modules on!ood Manu(acturing Practice0 Water (orPharaceutical &se0 Part 4060 and =5 7649
=5 WH%0 !uidelines (or drinking-)ater 3uality0 6ndedition0 volue 4 74OO=9
>5 WH%0 !uidelines (or drinking-)ater 3uality0 6ndedition0 volue 60 74OO@9
?5 WH%0 !uidelines (or drinking-)ater 3uality0 6ndedition0 .olue =J 74OO9
@5 WH%0 !uidelines (or drinking-)ater 3uality0 6ndedition0 Addendu to .olue 4 K 6 74OOD9
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E C itt