tma - linseis
TRANSCRIPT
TMA / DTMA
* Different furnaces (TMA PT1600)
TMA PT 1000 TMA PT 1600
5
二极管 或
真空
2
-90 -80 -70 -60 -50 -40 -30 -20 -10 0 10 20 30 40 50 60 70 80 90 100 110 120 130
5.0
4.8
4.5
4.3
4.0
3.8
3.5
3.3
3.0
2.8
2.5
2.3
2.0
1.8
1.5
1.3
1.0
0.8
0.5
0.3
0.0
-0.3
150
140
130
120
110
100
90
80
70
60
50
40
30
20
10
0
-10
Delta-L (1) [�m]
Temperature [°C]
E-Modulus (smoothed) [Log(N/mm )]
E-Modulus (smoothed) [PIR2-1]
Glass Point33.0°C
Delta-L (smoothed) [PIR2-1]Delta-L (1)[PIR2-1]
2
-1Y
Zoom 0
Linseis Data Evaluation
File Trace Evaluation Print Options ASCII-Export Help_ _ _ _ _ _ _
Function Group
TMA-Evaluation
Temperature profile infoSignal correction, X-smoothingY-smoothingDerivationExpansion coefficient ...E-Modulus calculationGlasspoint evaluationExtrapolationCurve aritmethicMean curveCollection fileDifferential measurement
Trace: DTA Sig
动态TMA模型
这个特性允许做材料的粘弹性行为研究，自动施加给
D-TMA探头一个特定的频率。
® ®
Linear Motor
LVDT
Sample
Furnace
Penetration
3 Point Bending Volumetric Expansion
Expansion
Side
E-Modulus
Front
Tension
7
-80 -70 -60 -50 -40 -30 -20 -10 0 10 20 30 40 50 60 70 80 90 100 110 120 130
4.84.64.44.24.03.83.63.43.23.02.82.62.42.22.01.81.61.41.21.00.80.60.40.20.0-0.2
36
34
32
30
28
26
24
22
20
18
16
14
12
10
8
6
4
2
0
-2
Delta-L (corrected) [�m]
Temperature (smoothed) [ °C]
E-Modulus [PIR3-1]
Glass Point-54.6°C
Delta-L [PIR3-1]
E-Modulus (smoothed) [Log(N/mm )]2
Offset-52.4°C
Onset-56.7°C Delta-L [PIR3-1]
-90 -80 -70 -60 -50 -40 -30 -20 -10 0 10 20 30 40 50 60 70 80 90 100 110 120 130
5.0
4.8
4.5
4.3
4.0
3.8
3.5
3.3
3.0
2.8
2.5
2.3
2.0
1.8
1.5
1.3
1.0
0.8
0.5
0.3
0.0
-0.3
150
140
130
120
110
100
90
80
70
60
50
40
30
20
10
0
-10
Delta-L (1) [�m]
Temperature [°C]
E-Modulus (smoothed) [Log(N/mm )]
E-Modulus [PIR2-1]
Glass Point33.0°C
Delta-L [PIR2-1]Delta-L (1)[PIR2-1]
2
-90 -80 -70 -60 -50 -40 -30 -20 -10 0 10 20 30 40 50 60 70 80 90 100 110 120 130
5.0
4.8
4.5
4.3
4.0
3.8
3.5
3.3
3.0
2.8
2.5
2.3
2.0
1.8
1.5
1.3
1.0
0.8
0.5
0.3
0.0
-0.3
150
140
130
120
110
100
90
80
70
60
50
40
30
20
10
0
-10
Delta-L (1) [�m]
Temperature [°C]
E-Modulus (smoothed) [Log(N/mm )]
E-Modulus [PIR2-1]
Glass Point33.0°C
Delta-L [PIR2-1]Delta-L (1)[PIR2-1]
2
7
200 220 240 260 280 300 320 340 360 380 400 420 440 460 480 500 520 540 560 580 600 620 640 660 680 700
80
70
60
50
40
30
20
10
0
-10
-20
-30
-40
-50
-60
50
45
40
35
30
25
20
15
10
5
0
-5
-10
-15
-20
Delta-L (2) [�m]
Temperature [°C]
DTA Signal (smoothed) [�V]
Delta-L(2)[BK-00-4]
DTA Signal [BK-00-3]Base Line [BK-00-3]
Point of Reaction576.1°C
Max/Min577.4°C 2.207�V
Onset575.2°C
0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90
FPM 2.4306 mm
95 100
EPDM 2.5267 mm
5%
N 10.0N 0.1N 10.0
0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90
FPM 2.4306 mm
95 100
EPDM 2.5267 mm
5%
N 10.0N 0.1N 10.0
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